Pyrolysis Kinetics of Physical Components of Wood and Wood-Polymers Using Isoconversion Method

Two hardwood species, namely red oak and yellow-poplar, were separated into their bark, sapwood and heartwood components. The samples were tested for calorific value, specific gravity, proximate analysis, mineral composition, chemical composition, ultimate analysis, and thermo-chemical decomposition...

Full description

Bibliographic Details
Main Authors: John Zondlo, Wenjia Jin, Kaushlendra Singh
Format: Article
Language:English
Published: MDPI AG 2013-01-01
Series:Agriculture
Subjects:
Online Access:http://www.mdpi.com/2077-0472/3/1/12
_version_ 1829493181151969280
author John Zondlo
Wenjia Jin
Kaushlendra Singh
author_facet John Zondlo
Wenjia Jin
Kaushlendra Singh
author_sort John Zondlo
collection DOAJ
description Two hardwood species, namely red oak and yellow-poplar, were separated into their bark, sapwood and heartwood components. The samples were tested for calorific value, specific gravity, proximate analysis, mineral composition, chemical composition, ultimate analysis, and thermo-chemical decomposition behavior. In addition, the thermo-chemical decomposition behaviors of cellulose, xylan, and lignin polymers were also tested. Thermo-chemical decomposition behavior was assessed using a thermo-gravimetric (TGA) system by heating the sample from 50 °C to 700 °C at the heating rates of 10, 30 and 50 °C/min under nitrogen. The activation energy was calculated for various fractional conversion values using the isoconversion method. The results showed that char yields of lignin, cellulose and xylan were 41.43%, 4.45% and 1.89%, respectively, at the end of pyrolysis. Furthermore, cellulose, xylan and lignin decomposed dramatically in the temperature range of 320 °C to 360 °C, 150 °C to 230 °C and 100 °C to 410 °C, respectively, with decomposition peaks occurring at 340 °C, 200 °C and 340 °C, respectively. In addition, the maximum activation energy for cellulose was 381 kJ/mol at 360 °C and for xylan it was 348 kJ/mol at 210 °C.
first_indexed 2024-12-16T06:29:48Z
format Article
id doaj.art-86e1b95dce9547b3a9c4bd5b76a3724e
institution Directory Open Access Journal
issn 2077-0472
language English
last_indexed 2024-12-16T06:29:48Z
publishDate 2013-01-01
publisher MDPI AG
record_format Article
series Agriculture
spelling doaj.art-86e1b95dce9547b3a9c4bd5b76a3724e2022-12-21T22:40:55ZengMDPI AGAgriculture2077-04722013-01-0131123210.3390/agriculture3010012Pyrolysis Kinetics of Physical Components of Wood and Wood-Polymers Using Isoconversion MethodJohn ZondloWenjia JinKaushlendra SinghTwo hardwood species, namely red oak and yellow-poplar, were separated into their bark, sapwood and heartwood components. The samples were tested for calorific value, specific gravity, proximate analysis, mineral composition, chemical composition, ultimate analysis, and thermo-chemical decomposition behavior. In addition, the thermo-chemical decomposition behaviors of cellulose, xylan, and lignin polymers were also tested. Thermo-chemical decomposition behavior was assessed using a thermo-gravimetric (TGA) system by heating the sample from 50 °C to 700 °C at the heating rates of 10, 30 and 50 °C/min under nitrogen. The activation energy was calculated for various fractional conversion values using the isoconversion method. The results showed that char yields of lignin, cellulose and xylan were 41.43%, 4.45% and 1.89%, respectively, at the end of pyrolysis. Furthermore, cellulose, xylan and lignin decomposed dramatically in the temperature range of 320 °C to 360 °C, 150 °C to 230 °C and 100 °C to 410 °C, respectively, with decomposition peaks occurring at 340 °C, 200 °C and 340 °C, respectively. In addition, the maximum activation energy for cellulose was 381 kJ/mol at 360 °C and for xylan it was 348 kJ/mol at 210 °C.http://www.mdpi.com/2077-0472/3/1/12bioenergytorrefactionhardwood componentsactivation energy&#160
spellingShingle John Zondlo
Wenjia Jin
Kaushlendra Singh
Pyrolysis Kinetics of Physical Components of Wood and Wood-Polymers Using Isoconversion Method
Agriculture
bioenergy
torrefaction
hardwood components
activation energy&#160
title Pyrolysis Kinetics of Physical Components of Wood and Wood-Polymers Using Isoconversion Method
title_full Pyrolysis Kinetics of Physical Components of Wood and Wood-Polymers Using Isoconversion Method
title_fullStr Pyrolysis Kinetics of Physical Components of Wood and Wood-Polymers Using Isoconversion Method
title_full_unstemmed Pyrolysis Kinetics of Physical Components of Wood and Wood-Polymers Using Isoconversion Method
title_short Pyrolysis Kinetics of Physical Components of Wood and Wood-Polymers Using Isoconversion Method
title_sort pyrolysis kinetics of physical components of wood and wood polymers using isoconversion method
topic bioenergy
torrefaction
hardwood components
activation energy&#160
url http://www.mdpi.com/2077-0472/3/1/12
work_keys_str_mv AT johnzondlo pyrolysiskineticsofphysicalcomponentsofwoodandwoodpolymersusingisoconversionmethod
AT wenjiajin pyrolysiskineticsofphysicalcomponentsofwoodandwoodpolymersusingisoconversionmethod
AT kaushlendrasingh pyrolysiskineticsofphysicalcomponentsofwoodandwoodpolymersusingisoconversionmethod