Synthesis of nano-sized β-tricalcium phosphate via wet precipitation
Nano-size β-tricalcium phosphate powders with average grain size of 50 nm were prepared by the wet chemical precipitation method with calcium nitrate and diammonium hydrogen phosphate as calcium and phosphorus precursors, respectively. The pH of the system was maintained at 8 and 10.8 by adding of s...
| Main Authors: | , , |
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| Format: | Article |
| Language: | English |
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University of Novi Sad
2011-12-01
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| Series: | Processing and Application of Ceramics |
| Subjects: | |
| Online Access: | http://www.tf.uns.ac.rs/publikacije/PAC/pdf/PAC%2014%2003.pdf |
| _version_ | 1828379979847565312 |
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| author | Bahman Mirhadi Behzad Mehdikhani Nayereh Askari |
| author_facet | Bahman Mirhadi Behzad Mehdikhani Nayereh Askari |
| author_sort | Bahman Mirhadi |
| collection | DOAJ |
| description | Nano-size β-tricalcium phosphate powders with average grain size of 50 nm were prepared by the wet chemical precipitation method with calcium nitrate and diammonium hydrogen phosphate as calcium and phosphorus precursors, respectively. The pH of the system was maintained at 8 and 10.8 by adding of sodium hydroxide. Filtered cake was dried at 80°C and calcined at 700°C. The dried and calcined powders were characterized using X-ray diffractrometry (XRD), Fourier transform infrared spectroscopy (FTIR), inductively coupled plasma atomic emission spectroscopy (ICPAES) and scanning electron microscopy (SEM). |
| first_indexed | 2024-12-10T03:49:00Z |
| format | Article |
| id | doaj.art-87299e2d6f164d569e2862295834866a |
| institution | Directory Open Access Journal |
| issn | 1820-6131 |
| language | English |
| last_indexed | 2024-12-10T03:49:00Z |
| publishDate | 2011-12-01 |
| publisher | University of Novi Sad |
| record_format | Article |
| series | Processing and Application of Ceramics |
| spelling | doaj.art-87299e2d6f164d569e2862295834866a2022-12-22T02:03:18ZengUniversity of Novi SadProcessing and Application of Ceramics1820-61312011-12-0154193198Synthesis of nano-sized β-tricalcium phosphate via wet precipitationBahman MirhadiBehzad MehdikhaniNayereh AskariNano-size β-tricalcium phosphate powders with average grain size of 50 nm were prepared by the wet chemical precipitation method with calcium nitrate and diammonium hydrogen phosphate as calcium and phosphorus precursors, respectively. The pH of the system was maintained at 8 and 10.8 by adding of sodium hydroxide. Filtered cake was dried at 80°C and calcined at 700°C. The dried and calcined powders were characterized using X-ray diffractrometry (XRD), Fourier transform infrared spectroscopy (FTIR), inductively coupled plasma atomic emission spectroscopy (ICPAES) and scanning electron microscopy (SEM).http://www.tf.uns.ac.rs/publikacije/PAC/pdf/PAC%2014%2003.pdfBiomaterialβ-tricalcium phosphateWet chemical precipitationCharacterization |
| spellingShingle | Bahman Mirhadi Behzad Mehdikhani Nayereh Askari Synthesis of nano-sized β-tricalcium phosphate via wet precipitation Processing and Application of Ceramics Biomaterial β-tricalcium phosphate Wet chemical precipitation Characterization |
| title | Synthesis of nano-sized β-tricalcium phosphate via wet precipitation |
| title_full | Synthesis of nano-sized β-tricalcium phosphate via wet precipitation |
| title_fullStr | Synthesis of nano-sized β-tricalcium phosphate via wet precipitation |
| title_full_unstemmed | Synthesis of nano-sized β-tricalcium phosphate via wet precipitation |
| title_short | Synthesis of nano-sized β-tricalcium phosphate via wet precipitation |
| title_sort | synthesis of nano sized β tricalcium phosphate via wet precipitation |
| topic | Biomaterial β-tricalcium phosphate Wet chemical precipitation Characterization |
| url | http://www.tf.uns.ac.rs/publikacije/PAC/pdf/PAC%2014%2003.pdf |
| work_keys_str_mv | AT bahmanmirhadi synthesisofnanosizedbtricalciumphosphateviawetprecipitation AT behzadmehdikhani synthesisofnanosizedbtricalciumphosphateviawetprecipitation AT nayerehaskari synthesisofnanosizedbtricalciumphosphateviawetprecipitation |