Synthesis and Characterization of Sulfonated Anionic Hyperbranched Polyglycerol Oleate Surfactant Based on Oleic Fatty Acid Palm Oil
Surfactant is a palm oil-based product that was rapidly developed. One type of surfactant with several advantages is anionic surfactant, known for its good emulsion, detergency, and thermal stability. The synthesis of this surfactant involved three steps: first, the polymerization of glycerol with a...
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| Format: | Article |
| Language: | English |
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EDP Sciences
2024-01-01
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| Series: | E3S Web of Conferences |
| Online Access: | https://www.e3s-conferences.org/articles/e3sconf/pdf/2024/33/e3sconf_isac-iccme2023_08003.pdf |
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| author | Irawan Yan Ghozan Misri Meliana Yenny Kuslianti Elnike Prasetyaningrum Aji Rabbuka Muhammad Adiguna Afifah Dita Dwi |
| author_facet | Irawan Yan Ghozan Misri Meliana Yenny Kuslianti Elnike Prasetyaningrum Aji Rabbuka Muhammad Adiguna Afifah Dita Dwi |
| author_sort | Irawan Yan |
| collection | DOAJ |
| description | Surfactant is a palm oil-based product that was rapidly developed. One type of surfactant with several advantages is anionic surfactant, known for its good emulsion, detergency, and thermal stability. The synthesis of this surfactant involved three steps: first, the polymerization of glycerol with a variable KOH catalyst (1%-4% w/v); second, the esterification of the polyglycerol with oleic acid; and finally, the sulfonation of polyglycerol oleate with H2SO4. The molecular weight of the obtained polyglycerol was determined using the Ostwald method, and the polymerization process was confirmed with FTIR. Polyglycerol oleate was characterized by determining the acid number, ester number, ion number, and saponification number, and confirmed using FTIR and 1H-NMR. Sulfonated polyglycerol oleate was characterized using FTIR and 1H-NMR. |
| first_indexed | 2024-04-24T20:22:48Z |
| format | Article |
| id | doaj.art-8738e4dd765e4263bf5dc03e29341bf2 |
| institution | Directory Open Access Journal |
| issn | 2267-1242 |
| language | English |
| last_indexed | 2024-04-24T20:22:48Z |
| publishDate | 2024-01-01 |
| publisher | EDP Sciences |
| record_format | Article |
| series | E3S Web of Conferences |
| spelling | doaj.art-8738e4dd765e4263bf5dc03e29341bf22024-03-22T07:56:07ZengEDP SciencesE3S Web of Conferences2267-12422024-01-015030800310.1051/e3sconf/202450308003e3sconf_isac-iccme2023_08003Synthesis and Characterization of Sulfonated Anionic Hyperbranched Polyglycerol Oleate Surfactant Based on Oleic Fatty Acid Palm OilIrawan Yan0Ghozan Misri1Meliana Yenny2Kuslianti Elnike3Prasetyaningrum Aji4Rabbuka Muhammad Adiguna5Afifah Dita Dwi6Department of Chemical Engineering, Faculty of Engineering, University of IndonesiaResearch Center for Chemistry, National Research and Innovation Agency, KST Habibie SerpongResearch Center for Chemistry, National Research and Innovation Agency, KST Habibie SerpongFaculty of Math and Natural Sciences, University of Udayana,Jl. Raya Kampus UNUDDepartment of Chemical Engineering, Faculty of Engineering, Diponegoro UniversityResearch Center for Chemistry, National Research and Innovation Agency, KST Habibie SerpongResearch Center for Chemistry, National Research and Innovation Agency, KST Habibie SerpongSurfactant is a palm oil-based product that was rapidly developed. One type of surfactant with several advantages is anionic surfactant, known for its good emulsion, detergency, and thermal stability. The synthesis of this surfactant involved three steps: first, the polymerization of glycerol with a variable KOH catalyst (1%-4% w/v); second, the esterification of the polyglycerol with oleic acid; and finally, the sulfonation of polyglycerol oleate with H2SO4. The molecular weight of the obtained polyglycerol was determined using the Ostwald method, and the polymerization process was confirmed with FTIR. Polyglycerol oleate was characterized by determining the acid number, ester number, ion number, and saponification number, and confirmed using FTIR and 1H-NMR. Sulfonated polyglycerol oleate was characterized using FTIR and 1H-NMR.https://www.e3s-conferences.org/articles/e3sconf/pdf/2024/33/e3sconf_isac-iccme2023_08003.pdf |
| spellingShingle | Irawan Yan Ghozan Misri Meliana Yenny Kuslianti Elnike Prasetyaningrum Aji Rabbuka Muhammad Adiguna Afifah Dita Dwi Synthesis and Characterization of Sulfonated Anionic Hyperbranched Polyglycerol Oleate Surfactant Based on Oleic Fatty Acid Palm Oil E3S Web of Conferences |
| title | Synthesis and Characterization of Sulfonated Anionic Hyperbranched Polyglycerol Oleate Surfactant Based on Oleic Fatty Acid Palm Oil |
| title_full | Synthesis and Characterization of Sulfonated Anionic Hyperbranched Polyglycerol Oleate Surfactant Based on Oleic Fatty Acid Palm Oil |
| title_fullStr | Synthesis and Characterization of Sulfonated Anionic Hyperbranched Polyglycerol Oleate Surfactant Based on Oleic Fatty Acid Palm Oil |
| title_full_unstemmed | Synthesis and Characterization of Sulfonated Anionic Hyperbranched Polyglycerol Oleate Surfactant Based on Oleic Fatty Acid Palm Oil |
| title_short | Synthesis and Characterization of Sulfonated Anionic Hyperbranched Polyglycerol Oleate Surfactant Based on Oleic Fatty Acid Palm Oil |
| title_sort | synthesis and characterization of sulfonated anionic hyperbranched polyglycerol oleate surfactant based on oleic fatty acid palm oil |
| url | https://www.e3s-conferences.org/articles/e3sconf/pdf/2024/33/e3sconf_isac-iccme2023_08003.pdf |
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