Determination of organic acid and inorganic anion by suppressed electric conductance ion chromatography(离子色谱电导检测法测定酒中的有机酸和无机阴离子)

采用淋洗液发生器-抑制电导检测法,同时分离和检测16种无机阴离子和低分子量有机酸,建立了用亲水性阴离子交换分离柱,KOH为淋洗液等浓度泵作梯度淋洗的离子色谱分离方法.该方法具有良好的重现性、线性关系.除马来酸外,所有被测离子的检测限都在0. 16 mg/L以下.方法用于测定4种酒样品的分析,结果满意.样品测定的回收率在93. 52%到116. 08%之间,除富马酸外其它RSD都小于3.8%....

Full description

Bibliographic Details
Main Authors: WUFei-yan(吴飞燕), JIAZhi-shen(贾之慎), ZHUYan(朱岩)
Format: Article
Language:zho
Published: Zhejiang University Press 2006-05-01
Series:Zhejiang Daxue xuebao. Lixue ban
Subjects:
Online Access:https://doi.org/zjup/1008-9497.2006.33.3.312-315
_version_ 1797236299153801216
author WUFei-yan(吴飞燕)
JIAZhi-shen(贾之慎)
ZHUYan(朱岩)
author_facet WUFei-yan(吴飞燕)
JIAZhi-shen(贾之慎)
ZHUYan(朱岩)
author_sort WUFei-yan(吴飞燕)
collection DOAJ
description 采用淋洗液发生器-抑制电导检测法,同时分离和检测16种无机阴离子和低分子量有机酸,建立了用亲水性阴离子交换分离柱,KOH为淋洗液等浓度泵作梯度淋洗的离子色谱分离方法.该方法具有良好的重现性、线性关系.除马来酸外,所有被测离子的检测限都在0. 16 mg/L以下.方法用于测定4种酒样品的分析,结果满意.样品测定的回收率在93. 52%到116. 08%之间,除富马酸外其它RSD都小于3.8%.
first_indexed 2024-04-24T17:01:38Z
format Article
id doaj.art-87dcb32dda844c01989a69546f63c91a
institution Directory Open Access Journal
issn 1008-9497
language zho
last_indexed 2024-04-24T17:01:38Z
publishDate 2006-05-01
publisher Zhejiang University Press
record_format Article
series Zhejiang Daxue xuebao. Lixue ban
spelling doaj.art-87dcb32dda844c01989a69546f63c91a2024-03-29T01:58:23ZzhoZhejiang University PressZhejiang Daxue xuebao. Lixue ban1008-94972006-05-01333312315zjup/1008-9497.2006.33.3.312-315Determination of organic acid and inorganic anion by suppressed electric conductance ion chromatography(离子色谱电导检测法测定酒中的有机酸和无机阴离子)WUFei-yan(吴飞燕)0JIAZhi-shen(贾之慎)1ZHUYan(朱岩)2Department of Chemistry, Zhejiang University, Hangzhou 310027, China(浙江大学化学系,浙江 杭州 310027)Department of Chemistry, Zhejiang University, Hangzhou 310027, China(浙江大学化学系,浙江 杭州 310027)Department of Chemistry, Zhejiang University, Hangzhou 310027, China(浙江大学化学系,浙江 杭州 310027)采用淋洗液发生器-抑制电导检测法,同时分离和检测16种无机阴离子和低分子量有机酸,建立了用亲水性阴离子交换分离柱,KOH为淋洗液等浓度泵作梯度淋洗的离子色谱分离方法.该方法具有良好的重现性、线性关系.除马来酸外,所有被测离子的检测限都在0. 16 mg/L以下.方法用于测定4种酒样品的分析,结果满意.样品测定的回收率在93. 52%到116. 08%之间,除富马酸外其它RSD都小于3.8%.https://doi.org/zjup/1008-9497.2006.33.3.312-315淋洗液发生器离子色谱抑制电导有机酸
spellingShingle WUFei-yan(吴飞燕)
JIAZhi-shen(贾之慎)
ZHUYan(朱岩)
Determination of organic acid and inorganic anion by suppressed electric conductance ion chromatography(离子色谱电导检测法测定酒中的有机酸和无机阴离子)
Zhejiang Daxue xuebao. Lixue ban
淋洗液发生器
离子色谱
抑制电导
有机酸
title Determination of organic acid and inorganic anion by suppressed electric conductance ion chromatography(离子色谱电导检测法测定酒中的有机酸和无机阴离子)
title_full Determination of organic acid and inorganic anion by suppressed electric conductance ion chromatography(离子色谱电导检测法测定酒中的有机酸和无机阴离子)
title_fullStr Determination of organic acid and inorganic anion by suppressed electric conductance ion chromatography(离子色谱电导检测法测定酒中的有机酸和无机阴离子)
title_full_unstemmed Determination of organic acid and inorganic anion by suppressed electric conductance ion chromatography(离子色谱电导检测法测定酒中的有机酸和无机阴离子)
title_short Determination of organic acid and inorganic anion by suppressed electric conductance ion chromatography(离子色谱电导检测法测定酒中的有机酸和无机阴离子)
title_sort determination of organic acid and inorganic anion by suppressed electric conductance ion chromatography 离子色谱电导检测法测定酒中的有机酸和无机阴离子
topic 淋洗液发生器
离子色谱
抑制电导
有机酸
url https://doi.org/zjup/1008-9497.2006.33.3.312-315
work_keys_str_mv AT wufeiyanwúfēiyàn determinationoforganicacidandinorganicanionbysuppressedelectricconductanceionchromatographylízisèpǔdiàndǎojiǎncèfǎcèdìngjiǔzhōngdeyǒujīsuānhéwújīyīnlízi
AT jiazhishenjiǎzhīshèn determinationoforganicacidandinorganicanionbysuppressedelectricconductanceionchromatographylízisèpǔdiàndǎojiǎncèfǎcèdìngjiǔzhōngdeyǒujīsuānhéwújīyīnlízi
AT zhuyanzhūyán determinationoforganicacidandinorganicanionbysuppressedelectricconductanceionchromatographylízisèpǔdiàndǎojiǎncèfǎcèdìngjiǔzhōngdeyǒujīsuānhéwújīyīnlízi