Green synthesis of multifunctional MgO@AgO/Ag2O nanocomposite for photocatalytic degradation of methylene blue and toluidine blue
Introduction: In this paper, MgO@AgO/Ag2O nanoparticles were greenly synthesized, the current idea is to replace the harmful chemical technique with an ecofriendly synthesis of metal oxide nanoparticles (NPs) utilizing biogenic sources.Methods: The current investigation was conducted to create silve...
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Frontiers Media S.A.
2022-12-01
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author | Younes Zidane Younes Zidane Salah E. Laouini Salah E. Laouini Abderrhmane Bouafia Abderrhmane Bouafia Souhaila Meneceur Souhaila Meneceur Mohammed L. Tedjani Mohammed L. Tedjani Sohad A. Alshareef Hanadi A. Almukhlifi Khansaa Al-Essa Ethar M. Al-Essa Mohammed M. Rahman Osama Madkhali Farid Menaa |
author_facet | Younes Zidane Younes Zidane Salah E. Laouini Salah E. Laouini Abderrhmane Bouafia Abderrhmane Bouafia Souhaila Meneceur Souhaila Meneceur Mohammed L. Tedjani Mohammed L. Tedjani Sohad A. Alshareef Hanadi A. Almukhlifi Khansaa Al-Essa Ethar M. Al-Essa Mohammed M. Rahman Osama Madkhali Farid Menaa |
author_sort | Younes Zidane |
collection | DOAJ |
description | Introduction: In this paper, MgO@AgO/Ag2O nanoparticles were greenly synthesized, the current idea is to replace the harmful chemical technique with an ecofriendly synthesis of metal oxide nanoparticles (NPs) utilizing biogenic sources.Methods: The current investigation was conducted to create silver oxide NPs decorated by MgO NPs (namely, MgO@AgO/Ag2O nanocom-posite) using the leaves extract of Purslane (Portulaca Oleracea) as the reducing and capping agent. The nanopowder was investigated by means of X-ray diffraction, scanning electron mi-croscope, BET surface area, Fourier transform infrared, and UV-vis spectrophotom-eter studies. XRD studies reveal the monophasic nature of these highly crystalline silver nano-particles. SEM studies the shape and morphology of the synthesis AgO/Ag2O and MgO@AgO/Ag2O NPs. The presence of magnesium and oxygen was further confirmed by EDS profile.Results and discussion: The surface area was found to be 9.1787 m2/g and 7.7166 m2/g, respectively. FTIR analysis showed the presence of specific functional groups. UV-vis spectrophotometer studies show the absorption band at 450 nm due to surface plasmon resonance. The results have also indicated the high performance of the greenly synthesized AgO/Ag2O NPs and MgO@AgO/Ag2O NPs for photocatalytic activity dye degradation (methylene blue and toluidine blue). |
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spelling | doaj.art-8897c9cf1f074311b7a9979c799a81512022-12-22T03:53:54ZengFrontiers Media S.A.Frontiers in Chemistry2296-26462022-12-011010.3389/fchem.2022.10835961083596Green synthesis of multifunctional MgO@AgO/Ag2O nanocomposite for photocatalytic degradation of methylene blue and toluidine blueYounes Zidane0Younes Zidane1Salah E. Laouini2Salah E. Laouini3Abderrhmane Bouafia4Abderrhmane Bouafia5Souhaila Meneceur6Souhaila Meneceur7Mohammed L. Tedjani8Mohammed L. Tedjani9Sohad A. Alshareef10Hanadi A. Almukhlifi11Khansaa Al-Essa12Ethar M. Al-Essa13Mohammed M. Rahman14Osama Madkhali15Farid Menaa16Department of Process Engineering, Faculty of Technology, University of El Oued, El-Oued, AlgeriaLaboratory of Biotechnology Biomaterial and Condensed Matter, Faculty of Technology, University of El Oued, El-Oued, AlgeriaDepartment of Process Engineering, Faculty of Technology, University of El Oued, El-Oued, AlgeriaLaboratory of Biotechnology Biomaterial and Condensed Matter, Faculty of Technology, University of El Oued, El-Oued, AlgeriaDepartment of Process Engineering, Faculty of Technology, University of El Oued, El-Oued, AlgeriaLaboratory of Biotechnology Biomaterial and Condensed Matter, Faculty of Technology, University of El Oued, El-Oued, AlgeriaDepartment of Process Engineering, Faculty of Technology, University of El Oued, El-Oued, AlgeriaLaboratory of Biotechnology Biomaterial and Condensed Matter, Faculty of Technology, University of El Oued, El-Oued, AlgeriaDepartment of Process Engineering, Faculty of Technology, University of El Oued, El-Oued, AlgeriaLaboratory of Biotechnology Biomaterial and Condensed Matter, Faculty of Technology, University of El Oued, El-Oued, AlgeriaDepartment of Chemistry, Faculty of Science, University of Tabuk, Tabuk, Saudi ArabiaDepartment of Chemistry, Faculty of Science, University of Tabuk, Tabuk, Saudi ArabiaDepartment of Chemistry, Jerash University, Jerash, JordanDepartment of Civil Engineering, Isra University, Amman, JordanCenter of Excellence for Advanced Materials Research (CEAMR) and Chemistry Department, Faculty of Science, King Abdulaziz University, Jeddah, Saudi ArabiaDepartment of Physics, College of Science, Jazan University, Jazan, Saudi ArabiaDepartment of Biomedical and Environmental Engineering (BEE), Fluorotronics, Inc.-California Innovations Corporation, San Diego, CA, United StatesIntroduction: In this paper, MgO@AgO/Ag2O nanoparticles were greenly synthesized, the current idea is to replace the harmful chemical technique with an ecofriendly synthesis of metal oxide nanoparticles (NPs) utilizing biogenic sources.Methods: The current investigation was conducted to create silver oxide NPs decorated by MgO NPs (namely, MgO@AgO/Ag2O nanocom-posite) using the leaves extract of Purslane (Portulaca Oleracea) as the reducing and capping agent. The nanopowder was investigated by means of X-ray diffraction, scanning electron mi-croscope, BET surface area, Fourier transform infrared, and UV-vis spectrophotom-eter studies. XRD studies reveal the monophasic nature of these highly crystalline silver nano-particles. SEM studies the shape and morphology of the synthesis AgO/Ag2O and MgO@AgO/Ag2O NPs. The presence of magnesium and oxygen was further confirmed by EDS profile.Results and discussion: The surface area was found to be 9.1787 m2/g and 7.7166 m2/g, respectively. FTIR analysis showed the presence of specific functional groups. UV-vis spectrophotometer studies show the absorption band at 450 nm due to surface plasmon resonance. The results have also indicated the high performance of the greenly synthesized AgO/Ag2O NPs and MgO@AgO/Ag2O NPs for photocatalytic activity dye degradation (methylene blue and toluidine blue).https://www.frontiersin.org/articles/10.3389/fchem.2022.1083596/fullMgO@AgO/Ag2O NPsgreen synthesisPortulaca oleraceaphotocatalysismethylene bluetoluidine blue |
spellingShingle | Younes Zidane Younes Zidane Salah E. Laouini Salah E. Laouini Abderrhmane Bouafia Abderrhmane Bouafia Souhaila Meneceur Souhaila Meneceur Mohammed L. Tedjani Mohammed L. Tedjani Sohad A. Alshareef Hanadi A. Almukhlifi Khansaa Al-Essa Ethar M. Al-Essa Mohammed M. Rahman Osama Madkhali Farid Menaa Green synthesis of multifunctional MgO@AgO/Ag2O nanocomposite for photocatalytic degradation of methylene blue and toluidine blue Frontiers in Chemistry MgO@AgO/Ag2O NPs green synthesis Portulaca oleracea photocatalysis methylene blue toluidine blue |
title | Green synthesis of multifunctional MgO@AgO/Ag2O nanocomposite for photocatalytic degradation of methylene blue and toluidine blue |
title_full | Green synthesis of multifunctional MgO@AgO/Ag2O nanocomposite for photocatalytic degradation of methylene blue and toluidine blue |
title_fullStr | Green synthesis of multifunctional MgO@AgO/Ag2O nanocomposite for photocatalytic degradation of methylene blue and toluidine blue |
title_full_unstemmed | Green synthesis of multifunctional MgO@AgO/Ag2O nanocomposite for photocatalytic degradation of methylene blue and toluidine blue |
title_short | Green synthesis of multifunctional MgO@AgO/Ag2O nanocomposite for photocatalytic degradation of methylene blue and toluidine blue |
title_sort | green synthesis of multifunctional mgo ago ag2o nanocomposite for photocatalytic degradation of methylene blue and toluidine blue |
topic | MgO@AgO/Ag2O NPs green synthesis Portulaca oleracea photocatalysis methylene blue toluidine blue |
url | https://www.frontiersin.org/articles/10.3389/fchem.2022.1083596/full |
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