Optimization of the bioactive compounds content in raspberry during freeze-drying using response surface method

The production of high-quality freeze-dried raspberry was studied by response surface method. Two independent variables, temperature (X1) and time (X2) were determined as the most important factors affecting the final product quality estimated by the responses: total phenol (Y1), total anth...

Full description

Bibliographic Details
Main Authors: Tumbas-Šaponjac Vesna T., Ćetković Gordana S., Stajčić Slađana M., Vulić Jelena J., Čanadanović-Brunet Jasna M., Đilas Sonja M.
Format: Article
Language:English
Published: Association of the Chemical Engineers of Serbia 2015-01-01
Series:Chemical Industry and Chemical Engineering Quarterly
Subjects:
Online Access:http://www.doiserbia.nb.rs/img/doi/1451-9372/2015/1451-93721400005T.pdf
_version_ 1819133535282266112
author Tumbas-Šaponjac Vesna T.
Ćetković Gordana S.
Stajčić Slađana M.
Vulić Jelena J.
Čanadanović-Brunet Jasna M.
Đilas Sonja M.
author_facet Tumbas-Šaponjac Vesna T.
Ćetković Gordana S.
Stajčić Slađana M.
Vulić Jelena J.
Čanadanović-Brunet Jasna M.
Đilas Sonja M.
author_sort Tumbas-Šaponjac Vesna T.
collection DOAJ
description The production of high-quality freeze-dried raspberry was studied by response surface method. Two independent variables, temperature (X1) and time (X2) were determined as the most important factors affecting the final product quality estimated by the responses: total phenol (Y1), total anthocyanin (Y2), vitamin C (Y3) and total bioactive compounds (Y4) content. A two-factor central composite design was used for freeze-drying experiments. The second order polynomial models obtained were found to be significant (p<0.05) for all responses. The statistical analysis of experimental data indicated that only quadratic time variable (X22) had significant (p<0.05) effect on all responses. The optimal conditions for all responses combined were found to be: -31 ºC and 35 h. The experimental values of all responses obtained under optimal conditions were in good agreement with predicted values which enables the use of the proposed mathematical models for optimization of investigated process. [Projekat Ministarstav nauke Republike Srbije, br. TR31044]
first_indexed 2024-12-22T09:48:50Z
format Article
id doaj.art-89f02d29a27549f2bd8afbad222bef14
institution Directory Open Access Journal
issn 1451-9372
2217-7434
language English
last_indexed 2024-12-22T09:48:50Z
publishDate 2015-01-01
publisher Association of the Chemical Engineers of Serbia
record_format Article
series Chemical Industry and Chemical Engineering Quarterly
spelling doaj.art-89f02d29a27549f2bd8afbad222bef142022-12-21T18:30:27ZengAssociation of the Chemical Engineers of SerbiaChemical Industry and Chemical Engineering Quarterly1451-93722217-74342015-01-01211-1536110.2298/CICEQ131201005T1451-93721400005TOptimization of the bioactive compounds content in raspberry during freeze-drying using response surface methodTumbas-Šaponjac Vesna T.0Ćetković Gordana S.1Stajčić Slađana M.2Vulić Jelena J.3Čanadanović-Brunet Jasna M.4Đilas Sonja M.5Faculty of Technology, Novi SadFaculty of Technology, Novi SadFaculty of Technology, Novi SadFaculty of Technology, Novi SadFaculty of Technology, Novi SadFaculty of Technology, Novi SadThe production of high-quality freeze-dried raspberry was studied by response surface method. Two independent variables, temperature (X1) and time (X2) were determined as the most important factors affecting the final product quality estimated by the responses: total phenol (Y1), total anthocyanin (Y2), vitamin C (Y3) and total bioactive compounds (Y4) content. A two-factor central composite design was used for freeze-drying experiments. The second order polynomial models obtained were found to be significant (p<0.05) for all responses. The statistical analysis of experimental data indicated that only quadratic time variable (X22) had significant (p<0.05) effect on all responses. The optimal conditions for all responses combined were found to be: -31 ºC and 35 h. The experimental values of all responses obtained under optimal conditions were in good agreement with predicted values which enables the use of the proposed mathematical models for optimization of investigated process. [Projekat Ministarstav nauke Republike Srbije, br. TR31044]http://www.doiserbia.nb.rs/img/doi/1451-9372/2015/1451-93721400005T.pdffreeze-dryingresponse surface methodologytotal phenolstotal anthocyaninsvitamin C
spellingShingle Tumbas-Šaponjac Vesna T.
Ćetković Gordana S.
Stajčić Slađana M.
Vulić Jelena J.
Čanadanović-Brunet Jasna M.
Đilas Sonja M.
Optimization of the bioactive compounds content in raspberry during freeze-drying using response surface method
Chemical Industry and Chemical Engineering Quarterly
freeze-drying
response surface methodology
total phenols
total anthocyanins
vitamin C
title Optimization of the bioactive compounds content in raspberry during freeze-drying using response surface method
title_full Optimization of the bioactive compounds content in raspberry during freeze-drying using response surface method
title_fullStr Optimization of the bioactive compounds content in raspberry during freeze-drying using response surface method
title_full_unstemmed Optimization of the bioactive compounds content in raspberry during freeze-drying using response surface method
title_short Optimization of the bioactive compounds content in raspberry during freeze-drying using response surface method
title_sort optimization of the bioactive compounds content in raspberry during freeze drying using response surface method
topic freeze-drying
response surface methodology
total phenols
total anthocyanins
vitamin C
url http://www.doiserbia.nb.rs/img/doi/1451-9372/2015/1451-93721400005T.pdf
work_keys_str_mv AT tumbassaponjacvesnat optimizationofthebioactivecompoundscontentinraspberryduringfreezedryingusingresponsesurfacemethod
AT cetkovicgordanas optimizationofthebioactivecompoundscontentinraspberryduringfreezedryingusingresponsesurfacemethod
AT stajcicslađanam optimizationofthebioactivecompoundscontentinraspberryduringfreezedryingusingresponsesurfacemethod
AT vulicjelenaj optimizationofthebioactivecompoundscontentinraspberryduringfreezedryingusingresponsesurfacemethod
AT canadanovicbrunetjasnam optimizationofthebioactivecompoundscontentinraspberryduringfreezedryingusingresponsesurfacemethod
AT đilassonjam optimizationofthebioactivecompoundscontentinraspberryduringfreezedryingusingresponsesurfacemethod