Simultaneous determination of four bioactive compounds in Korean rice wine (makgeolli) by solvent extraction coupled with gas chromatography-mass spectrometry
Makgeolli is a traditional Korean rice wine reported to have anticancer, anti-inflammatory, and antioxidant effects. We developed an approach involving solvent extraction coupled with gas chromatography-mass spectrometry to determine four bioactive compounds, farnesol (FOH), squalene (SQ), and newly...
| Main Authors: | , , , , |
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| Format: | Article |
| Language: | English |
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Taylor & Francis Group
2018-01-01
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| Series: | International Journal of Food Properties |
| Subjects: | |
| Online Access: | http://dx.doi.org/10.1080/10942912.2017.1414841 |
| _version_ | 1818278615894196224 |
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| author | Jangho Lee Yunyeol Lee Jaeho Ha Miyoung Yoo Hae Won Jang |
| author_facet | Jangho Lee Yunyeol Lee Jaeho Ha Miyoung Yoo Hae Won Jang |
| author_sort | Jangho Lee |
| collection | DOAJ |
| description | Makgeolli is a traditional Korean rice wine reported to have anticancer, anti-inflammatory, and antioxidant effects. We developed an approach involving solvent extraction coupled with gas chromatography-mass spectrometry to determine four bioactive compounds, farnesol (FOH), squalene (SQ), and newly identified 4-vinyl guaiacol (4-VG) and 2,4-di-tert-butylphenol (DTBP), in makgeolli. The method was validated with the linearity, limit of detection, limit of quantification, intra- and inter-day precision, and accuracy. The validated method was then applied to several makgeolli, beer, and wine samples. 4-VG and DTBP were identified in all beverages, but FOH and SQ were only identified in makgeolli. |
| first_indexed | 2024-12-12T23:20:16Z |
| format | Article |
| id | doaj.art-8a0863818f48438687f326a7d7f1a638 |
| institution | Directory Open Access Journal |
| issn | 1094-2912 1532-2386 |
| language | English |
| last_indexed | 2024-12-12T23:20:16Z |
| publishDate | 2018-01-01 |
| publisher | Taylor & Francis Group |
| record_format | Article |
| series | International Journal of Food Properties |
| spelling | doaj.art-8a0863818f48438687f326a7d7f1a6382022-12-22T00:08:19ZengTaylor & Francis GroupInternational Journal of Food Properties1094-29121532-23862018-01-0121113914610.1080/10942912.2017.14148411414841Simultaneous determination of four bioactive compounds in Korean rice wine (makgeolli) by solvent extraction coupled with gas chromatography-mass spectrometryJangho Lee0Yunyeol Lee1Jaeho Ha2Miyoung Yoo3Hae Won Jang4Korea Food Research InstituteKorea Food Research InstituteKorea Food Research InstituteKorea Food Research InstituteKorea Food Research InstituteMakgeolli is a traditional Korean rice wine reported to have anticancer, anti-inflammatory, and antioxidant effects. We developed an approach involving solvent extraction coupled with gas chromatography-mass spectrometry to determine four bioactive compounds, farnesol (FOH), squalene (SQ), and newly identified 4-vinyl guaiacol (4-VG) and 2,4-di-tert-butylphenol (DTBP), in makgeolli. The method was validated with the linearity, limit of detection, limit of quantification, intra- and inter-day precision, and accuracy. The validated method was then applied to several makgeolli, beer, and wine samples. 4-VG and DTBP were identified in all beverages, but FOH and SQ were only identified in makgeolli.http://dx.doi.org/10.1080/10942912.2017.1414841MakgeolliSolvent extractionGas chromatography-mass spectrometryVolatilesBioactive compounds |
| spellingShingle | Jangho Lee Yunyeol Lee Jaeho Ha Miyoung Yoo Hae Won Jang Simultaneous determination of four bioactive compounds in Korean rice wine (makgeolli) by solvent extraction coupled with gas chromatography-mass spectrometry International Journal of Food Properties Makgeolli Solvent extraction Gas chromatography-mass spectrometry Volatiles Bioactive compounds |
| title | Simultaneous determination of four bioactive compounds in Korean rice wine (makgeolli) by solvent extraction coupled with gas chromatography-mass spectrometry |
| title_full | Simultaneous determination of four bioactive compounds in Korean rice wine (makgeolli) by solvent extraction coupled with gas chromatography-mass spectrometry |
| title_fullStr | Simultaneous determination of four bioactive compounds in Korean rice wine (makgeolli) by solvent extraction coupled with gas chromatography-mass spectrometry |
| title_full_unstemmed | Simultaneous determination of four bioactive compounds in Korean rice wine (makgeolli) by solvent extraction coupled with gas chromatography-mass spectrometry |
| title_short | Simultaneous determination of four bioactive compounds in Korean rice wine (makgeolli) by solvent extraction coupled with gas chromatography-mass spectrometry |
| title_sort | simultaneous determination of four bioactive compounds in korean rice wine makgeolli by solvent extraction coupled with gas chromatography mass spectrometry |
| topic | Makgeolli Solvent extraction Gas chromatography-mass spectrometry Volatiles Bioactive compounds |
| url | http://dx.doi.org/10.1080/10942912.2017.1414841 |
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