Electrochemical and Structural Behavior of Bi Doped ZnO Materials Obtained with Solvothermal Synthesis Method

In this study, Bi-doped ZnO and undoped ZnO nanomaterials have been synthesized by the solvothermal reaction method. The effect of Bi doping on the structural and electrochemical properties has been investigated by X-ray diffractions (XRD), X-ray photoelectron spectroscopy (XPS) and, scanning electr...

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Main Authors: Hamide Kavak, Nazmi Sedefoğlu
Format: Article
Language:English
Published: Suleyman Demirel University 2021-05-01
Series:Süleyman Demirel Üniversitesi Fen-Edebiyat Fakültesi Fen Dergisi
Subjects:
Online Access:https://dergipark.org.tr/tr/pub/sdufeffd/issue/62394/886309
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author Hamide Kavak
Nazmi Sedefoğlu
author_facet Hamide Kavak
Nazmi Sedefoğlu
author_sort Hamide Kavak
collection DOAJ
description In this study, Bi-doped ZnO and undoped ZnO nanomaterials have been synthesized by the solvothermal reaction method. The effect of Bi doping on the structural and electrochemical properties has been investigated by X-ray diffractions (XRD), X-ray photoelectron spectroscopy (XPS) and, scanning electron microscopy (SEM). As seen from X-ray diffraction spectra performed on the bulk material, it has been clearly observed that both Bi doping changed the preferred orientation of the nanopowder as (101) and Bi+3 ions were expectedly entered the lattice. Furthermore, this result has been supported by photoelectron spectra. Scanning electron microscopy images have shown the shapes and distributions of nanostructures of the samples. As a result, it is thought that Bi doping is suitable for obtaining p-type conductivity in ZnO materials for the experimental processes we applied to samples in the study.
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spelling doaj.art-8a46264e38af41719ded4481b6b86f3e2023-02-15T16:15:45ZengSuleyman Demirel UniversitySüleyman Demirel Üniversitesi Fen-Edebiyat Fakültesi Fen Dergisi1306-75752021-05-0116114715610.29233/sdufeffd.8863091113Electrochemical and Structural Behavior of Bi Doped ZnO Materials Obtained with Solvothermal Synthesis MethodHamide Kavak0Nazmi Sedefoğlu1CUKUROVA UNIVERSITYOSMANIYE KORKUT ATA UNIVERSITYIn this study, Bi-doped ZnO and undoped ZnO nanomaterials have been synthesized by the solvothermal reaction method. The effect of Bi doping on the structural and electrochemical properties has been investigated by X-ray diffractions (XRD), X-ray photoelectron spectroscopy (XPS) and, scanning electron microscopy (SEM). As seen from X-ray diffraction spectra performed on the bulk material, it has been clearly observed that both Bi doping changed the preferred orientation of the nanopowder as (101) and Bi+3 ions were expectedly entered the lattice. Furthermore, this result has been supported by photoelectron spectra. Scanning electron microscopy images have shown the shapes and distributions of nanostructures of the samples. As a result, it is thought that Bi doping is suitable for obtaining p-type conductivity in ZnO materials for the experimental processes we applied to samples in the study.https://dergipark.org.tr/tr/pub/sdufeffd/issue/62394/886309zno:bibi dopingsolvothermal synthesis
spellingShingle Hamide Kavak
Nazmi Sedefoğlu
Electrochemical and Structural Behavior of Bi Doped ZnO Materials Obtained with Solvothermal Synthesis Method
Süleyman Demirel Üniversitesi Fen-Edebiyat Fakültesi Fen Dergisi
zno:bi
bi doping
solvothermal synthesis
title Electrochemical and Structural Behavior of Bi Doped ZnO Materials Obtained with Solvothermal Synthesis Method
title_full Electrochemical and Structural Behavior of Bi Doped ZnO Materials Obtained with Solvothermal Synthesis Method
title_fullStr Electrochemical and Structural Behavior of Bi Doped ZnO Materials Obtained with Solvothermal Synthesis Method
title_full_unstemmed Electrochemical and Structural Behavior of Bi Doped ZnO Materials Obtained with Solvothermal Synthesis Method
title_short Electrochemical and Structural Behavior of Bi Doped ZnO Materials Obtained with Solvothermal Synthesis Method
title_sort electrochemical and structural behavior of bi doped zno materials obtained with solvothermal synthesis method
topic zno:bi
bi doping
solvothermal synthesis
url https://dergipark.org.tr/tr/pub/sdufeffd/issue/62394/886309
work_keys_str_mv AT hamidekavak electrochemicalandstructuralbehaviorofbidopedznomaterialsobtainedwithsolvothermalsynthesismethod
AT nazmisedefoglu electrochemicalandstructuralbehaviorofbidopedznomaterialsobtainedwithsolvothermalsynthesismethod