Crystal structure of 2,2′-{[(2-nitrobenzyl)azanediyl]bis(propane-3,1-diyl)}bis[1H-isoindole-1,3(2H)-dione]

The structure of the title compound, C29H26N4O6, exhibits a folded conformation with the three arms all on the same side of the tertiary N atom. The two phthalimide units make a dihedral angle of 12.18 (12)° and the dihedral angles between the benzyl plane and the phthalimide units are 68.08 (7) and...

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Main Authors: Ryne Holmberg, Vanessa Franz, Kristen M. Moser, Ricardo Solano, Curtis Moore, Arnold L. Rheingold, Gary L. N. Smith
Format: Article
Language:English
Published: International Union of Crystallography 2021-02-01
Series:Acta Crystallographica Section E: Crystallographic Communications
Subjects:
Online Access:http://scripts.iucr.org/cgi-bin/paper?S2056989020016771
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author Ryne Holmberg
Vanessa Franz
Kristen M. Moser
Ricardo Solano
Curtis Moore
Arnold L. Rheingold
Gary L. N. Smith
author_facet Ryne Holmberg
Vanessa Franz
Kristen M. Moser
Ricardo Solano
Curtis Moore
Arnold L. Rheingold
Gary L. N. Smith
author_sort Ryne Holmberg
collection DOAJ
description The structure of the title compound, C29H26N4O6, exhibits a folded conformation with the three arms all on the same side of the tertiary N atom. The two phthalimide units make a dihedral angle of 12.18 (12)° and the dihedral angles between the benzyl plane and the phthalimide units are 68.08 (7) and 67.71 (7)°. The crystal packing features π–π interactions.
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spelling doaj.art-8cfdcd4dd3f54d11950ea1b43f8666022022-12-22T04:06:29ZengInternational Union of CrystallographyActa Crystallographica Section E: Crystallographic Communications2056-98902021-02-01772838510.1107/S2056989020016771zn2003Crystal structure of 2,2′-{[(2-nitrobenzyl)azanediyl]bis(propane-3,1-diyl)}bis[1H-isoindole-1,3(2H)-dione]Ryne Holmberg0Vanessa Franz1Kristen M. Moser2Ricardo Solano3Curtis Moore4Arnold L. Rheingold5Gary L. N. Smith6Department of Chemistry, Point Loma Nazarene University, San Diego, CA 92106, USADepartment of Chemistry, Point Loma Nazarene University, San Diego, CA 92106, USADepartment of Chemistry, Point Loma Nazarene University, San Diego, CA 92106, USADepartment of Chemistry, Point Loma Nazarene University, San Diego, CA 92106, USACrystallography Facility, The Ohio State University, Columbus, OH 43210, USADepartment of Chemistry, University of California-San Diego, La Jolla, CA 92093, USADepartment of Chemistry, San Diego Miramar College, San Diego, CA 92126, USAThe structure of the title compound, C29H26N4O6, exhibits a folded conformation with the three arms all on the same side of the tertiary N atom. The two phthalimide units make a dihedral angle of 12.18 (12)° and the dihedral angles between the benzyl plane and the phthalimide units are 68.08 (7) and 67.71 (7)°. The crystal packing features π–π interactions.http://scripts.iucr.org/cgi-bin/paper?S2056989020016771crystal structurephthalimidesπ–π interactionstripodal ligand
spellingShingle Ryne Holmberg
Vanessa Franz
Kristen M. Moser
Ricardo Solano
Curtis Moore
Arnold L. Rheingold
Gary L. N. Smith
Crystal structure of 2,2′-{[(2-nitrobenzyl)azanediyl]bis(propane-3,1-diyl)}bis[1H-isoindole-1,3(2H)-dione]
Acta Crystallographica Section E: Crystallographic Communications
crystal structure
phthalimides
π–π interactions
tripodal ligand
title Crystal structure of 2,2′-{[(2-nitrobenzyl)azanediyl]bis(propane-3,1-diyl)}bis[1H-isoindole-1,3(2H)-dione]
title_full Crystal structure of 2,2′-{[(2-nitrobenzyl)azanediyl]bis(propane-3,1-diyl)}bis[1H-isoindole-1,3(2H)-dione]
title_fullStr Crystal structure of 2,2′-{[(2-nitrobenzyl)azanediyl]bis(propane-3,1-diyl)}bis[1H-isoindole-1,3(2H)-dione]
title_full_unstemmed Crystal structure of 2,2′-{[(2-nitrobenzyl)azanediyl]bis(propane-3,1-diyl)}bis[1H-isoindole-1,3(2H)-dione]
title_short Crystal structure of 2,2′-{[(2-nitrobenzyl)azanediyl]bis(propane-3,1-diyl)}bis[1H-isoindole-1,3(2H)-dione]
title_sort crystal structure of 2 2 2 nitrobenzyl azanediyl bis propane 3 1 diyl bis 1h isoindole 1 3 2h dione
topic crystal structure
phthalimides
π–π interactions
tripodal ligand
url http://scripts.iucr.org/cgi-bin/paper?S2056989020016771
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