6-Benzyl-3,4-dimethoxy-10-methylpyrido[2′,1′:2,3]imidazo[4,5-c]isoquinolin-5(6H)-one
Pyrido[2′,1′:2,3]imidazo[4,5-c]isoquinolin-5(6H)-ones such as the title compound, C24H21N3O3, can be obtained in a few minutes in a microwave-assisted three-component reaction from 2-aminopyridines, isocyanides and 2-carboxybenzaldehydes. In the title compound, the pyrido...
| Main Authors: | , , , |
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| Format: | Article |
| Language: | English |
| Published: |
International Union of Crystallography
2009-10-01
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| Series: | Acta Crystallographica Section E |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S1600536809035806 |
| _version_ | 1818297610660741120 |
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| author | Kathrin Meindl Daniel Stern Fadime Mert-Balci Uwe Beifuss |
| author_facet | Kathrin Meindl Daniel Stern Fadime Mert-Balci Uwe Beifuss |
| author_sort | Kathrin Meindl |
| collection | DOAJ |
| description | Pyrido[2′,1′:2,3]imidazo[4,5-c]isoquinolin-5(6H)-ones such as the title compound, C24H21N3O3, can be obtained in a few minutes in a microwave-assisted three-component reaction from 2-aminopyridines, isocyanides and 2-carboxybenzaldehydes. In the title compound, the pyrido[2′,1′:2,3]imidazo[4,5-c]isoquinolin-5(6H)-one ring system is almost planar (mean deviation 0.068 Å). The dihedral angle between the benzyl ring and the pyrido[2′,1′:2,3]imidazo[4,5-c]isoquinolin-5(6H)-one ring system is 78.2°. The crystal structure is stabilized by intermolecular C—H...O and C—H...N hydrogen bonds. |
| first_indexed | 2024-12-13T04:22:10Z |
| format | Article |
| id | doaj.art-8d5a25321a284405834592814a199372 |
| institution | Directory Open Access Journal |
| issn | 1600-5368 |
| language | English |
| last_indexed | 2024-12-13T04:22:10Z |
| publishDate | 2009-10-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | Acta Crystallographica Section E |
| spelling | doaj.art-8d5a25321a284405834592814a1993722022-12-21T23:59:45ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682009-10-016510o2464o246510.1107/S16005368090358066-Benzyl-3,4-dimethoxy-10-methylpyrido[2′,1′:2,3]imidazo[4,5-c]isoquinolin-5(6H)-oneKathrin MeindlDaniel SternFadime Mert-BalciUwe BeifussPyrido[2′,1′:2,3]imidazo[4,5-c]isoquinolin-5(6H)-ones such as the title compound, C24H21N3O3, can be obtained in a few minutes in a microwave-assisted three-component reaction from 2-aminopyridines, isocyanides and 2-carboxybenzaldehydes. In the title compound, the pyrido[2′,1′:2,3]imidazo[4,5-c]isoquinolin-5(6H)-one ring system is almost planar (mean deviation 0.068 Å). The dihedral angle between the benzyl ring and the pyrido[2′,1′:2,3]imidazo[4,5-c]isoquinolin-5(6H)-one ring system is 78.2°. The crystal structure is stabilized by intermolecular C—H...O and C—H...N hydrogen bonds.http://scripts.iucr.org/cgi-bin/paper?S1600536809035806 |
| spellingShingle | Kathrin Meindl Daniel Stern Fadime Mert-Balci Uwe Beifuss 6-Benzyl-3,4-dimethoxy-10-methylpyrido[2′,1′:2,3]imidazo[4,5-c]isoquinolin-5(6H)-one Acta Crystallographica Section E |
| title | 6-Benzyl-3,4-dimethoxy-10-methylpyrido[2′,1′:2,3]imidazo[4,5-c]isoquinolin-5(6H)-one |
| title_full | 6-Benzyl-3,4-dimethoxy-10-methylpyrido[2′,1′:2,3]imidazo[4,5-c]isoquinolin-5(6H)-one |
| title_fullStr | 6-Benzyl-3,4-dimethoxy-10-methylpyrido[2′,1′:2,3]imidazo[4,5-c]isoquinolin-5(6H)-one |
| title_full_unstemmed | 6-Benzyl-3,4-dimethoxy-10-methylpyrido[2′,1′:2,3]imidazo[4,5-c]isoquinolin-5(6H)-one |
| title_short | 6-Benzyl-3,4-dimethoxy-10-methylpyrido[2′,1′:2,3]imidazo[4,5-c]isoquinolin-5(6H)-one |
| title_sort | 6 benzyl 3 4 dimethoxy 10 methylpyrido 2 amp 8242 1 amp 8242 2 3 imidazo 4 5 c isoquinolin 5 6h one |
| url | http://scripts.iucr.org/cgi-bin/paper?S1600536809035806 |
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