Electro-spinning of highly-aligned polyacrylonitrile nano-fibres with continuous spooling
Abstract This paper reports on a new configuration for producing highly-aligned electro-spun fibres that can be produced on a static substrate or one where it is hauled off and spooled continuously to enable the production of continuous lengths. The fixture consists of a Vee-shaped polytetrafluoreth...
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Format: | Article |
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Nature Portfolio
2021-11-01
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Series: | Scientific Reports |
Online Access: | https://doi.org/10.1038/s41598-021-99890-w |
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author | Siheng Shao Tao Ma Gerard F. Fernando |
author_facet | Siheng Shao Tao Ma Gerard F. Fernando |
author_sort | Siheng Shao |
collection | DOAJ |
description | Abstract This paper reports on a new configuration for producing highly-aligned electro-spun fibres that can be produced on a static substrate or one where it is hauled off and spooled continuously to enable the production of continuous lengths. The fixture consists of a Vee-shaped polytetrafluorethylene shield at 60° with a 1 cm wide integral rectangular base that is mounted on a copper disk with a 10 cm diameter. Specified concentrations of polyacrylonitrile in dimethyl sulfoxide were electro-spun on to a strip of cellulose paper. In the static setup, approximately 91% of the fibres were deposited to within 3°. When the spooling rig was used, a tape of the cellulose paper was hauled off at 0.07 mm/min, 78% of the fibres were aligned to within 3°. Simulations of the conventional and Vee-shield electro-spinning setups were undertaken and they provided corroboration for the experimental observations with regard to the mechanism responsible for fibre alignment. The feasibility of using this technique to produce 0°/− 45°/+ 45° stacked layers of aligned fibre preform is demonstrated. |
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issn | 2045-2322 |
language | English |
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publishDate | 2021-11-01 |
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spelling | doaj.art-8d89a01f1d6f4dfc81cca5ad754dba752022-12-22T04:03:47ZengNature PortfolioScientific Reports2045-23222021-11-0111111410.1038/s41598-021-99890-wElectro-spinning of highly-aligned polyacrylonitrile nano-fibres with continuous spoolingSiheng Shao0Tao Ma1Gerard F. Fernando2Sensors and Composites Group, School of Metallurgy and Materials, University of BirminghamSensors and Composites Group, School of Metallurgy and Materials, University of BirminghamSensors and Composites Group, School of Metallurgy and Materials, University of BirminghamAbstract This paper reports on a new configuration for producing highly-aligned electro-spun fibres that can be produced on a static substrate or one where it is hauled off and spooled continuously to enable the production of continuous lengths. The fixture consists of a Vee-shaped polytetrafluorethylene shield at 60° with a 1 cm wide integral rectangular base that is mounted on a copper disk with a 10 cm diameter. Specified concentrations of polyacrylonitrile in dimethyl sulfoxide were electro-spun on to a strip of cellulose paper. In the static setup, approximately 91% of the fibres were deposited to within 3°. When the spooling rig was used, a tape of the cellulose paper was hauled off at 0.07 mm/min, 78% of the fibres were aligned to within 3°. Simulations of the conventional and Vee-shield electro-spinning setups were undertaken and they provided corroboration for the experimental observations with regard to the mechanism responsible for fibre alignment. The feasibility of using this technique to produce 0°/− 45°/+ 45° stacked layers of aligned fibre preform is demonstrated.https://doi.org/10.1038/s41598-021-99890-w |
spellingShingle | Siheng Shao Tao Ma Gerard F. Fernando Electro-spinning of highly-aligned polyacrylonitrile nano-fibres with continuous spooling Scientific Reports |
title | Electro-spinning of highly-aligned polyacrylonitrile nano-fibres with continuous spooling |
title_full | Electro-spinning of highly-aligned polyacrylonitrile nano-fibres with continuous spooling |
title_fullStr | Electro-spinning of highly-aligned polyacrylonitrile nano-fibres with continuous spooling |
title_full_unstemmed | Electro-spinning of highly-aligned polyacrylonitrile nano-fibres with continuous spooling |
title_short | Electro-spinning of highly-aligned polyacrylonitrile nano-fibres with continuous spooling |
title_sort | electro spinning of highly aligned polyacrylonitrile nano fibres with continuous spooling |
url | https://doi.org/10.1038/s41598-021-99890-w |
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