Easy and New Chemical Synthesis of Stable Nano Sliver using Propylene Glycol and Glycerin as Reducing Agents

In this present work we have synthesized stable silvernanoparticles (Ag-NPs) by chemical reduction with aqueous solutions ofsilver nitrate (i) propylene glycol (ii) glycerin as reducing agents and guargum as a stabilizer. The reaction were done at room temperature and atpH=8. Systematic characteriza...

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Main Authors: Abdulah Mohammed, Sarab Mahmood
Format: Article
Language:English
Published: Unviversity of Technology- Iraq 2018-12-01
Series:Engineering and Technology Journal
Subjects:
Online Access:https://etj.uotechnology.edu.iq/article_175478_60e9a57016fcc2ed13f675437c7276b1.pdf
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author Abdulah Mohammed
Sarab Mahmood
author_facet Abdulah Mohammed
Sarab Mahmood
author_sort Abdulah Mohammed
collection DOAJ
description In this present work we have synthesized stable silvernanoparticles (Ag-NPs) by chemical reduction with aqueous solutions ofsilver nitrate (i) propylene glycol (ii) glycerin as reducing agents and guargum as a stabilizer. The reaction were done at room temperature and atpH=8. Systematic characterizations of the Ag-NPs were done using UV-Vis,zeta potential analysis, X-Ray diffraction (XRD), AFM and SEM whichreveal stable Ag-NPs. These measurements indicate that the particles aremostly spherical in shape. The UV-Vis spectra of the result solution of Ag-NPs show an absorption peak at 412 nm and 424 nm for using propyleneglycol and for using glycerin respectively. These color occurring due toSurface Plasmon Resonance (SPR). The SEM measurements gave a particlesize of 40 -70 nm. Nano silver showed stability for long periods of time tomore than nine months, and this can be an economical and effective way forwide scale synthesis of Ag-NPs which applicable for various medicaltherapies.
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spelling doaj.art-8dc28ea6543543489731d69a12a4b64c2024-02-04T17:20:11ZengUnviversity of Technology- IraqEngineering and Technology Journal1681-69002412-07582018-12-01362B13113510.30684/etj.36.2B.7175478Easy and New Chemical Synthesis of Stable Nano Sliver using Propylene Glycol and Glycerin as Reducing AgentsAbdulah Mohammed0Sarab Mahmood1Department of Chemistry, College of Science, University of Anbar, Anbar, Iraq.Department of Chemistry, College of Science, University of Anbar, Anbar, Iraq.In this present work we have synthesized stable silvernanoparticles (Ag-NPs) by chemical reduction with aqueous solutions ofsilver nitrate (i) propylene glycol (ii) glycerin as reducing agents and guargum as a stabilizer. The reaction were done at room temperature and atpH=8. Systematic characterizations of the Ag-NPs were done using UV-Vis,zeta potential analysis, X-Ray diffraction (XRD), AFM and SEM whichreveal stable Ag-NPs. These measurements indicate that the particles aremostly spherical in shape. The UV-Vis spectra of the result solution of Ag-NPs show an absorption peak at 412 nm and 424 nm for using propyleneglycol and for using glycerin respectively. These color occurring due toSurface Plasmon Resonance (SPR). The SEM measurements gave a particlesize of 40 -70 nm. Nano silver showed stability for long periods of time tomore than nine months, and this can be an economical and effective way forwide scale synthesis of Ag-NPs which applicable for various medicaltherapies.https://etj.uotechnology.edu.iq/article_175478_60e9a57016fcc2ed13f675437c7276b1.pdfsilver nanoparticlessurface plasmon resonance (spr)scanning electron microscope (sem)
spellingShingle Abdulah Mohammed
Sarab Mahmood
Easy and New Chemical Synthesis of Stable Nano Sliver using Propylene Glycol and Glycerin as Reducing Agents
Engineering and Technology Journal
silver nanoparticles
surface plasmon resonance (spr)
scanning electron microscope (sem)
title Easy and New Chemical Synthesis of Stable Nano Sliver using Propylene Glycol and Glycerin as Reducing Agents
title_full Easy and New Chemical Synthesis of Stable Nano Sliver using Propylene Glycol and Glycerin as Reducing Agents
title_fullStr Easy and New Chemical Synthesis of Stable Nano Sliver using Propylene Glycol and Glycerin as Reducing Agents
title_full_unstemmed Easy and New Chemical Synthesis of Stable Nano Sliver using Propylene Glycol and Glycerin as Reducing Agents
title_short Easy and New Chemical Synthesis of Stable Nano Sliver using Propylene Glycol and Glycerin as Reducing Agents
title_sort easy and new chemical synthesis of stable nano sliver using propylene glycol and glycerin as reducing agents
topic silver nanoparticles
surface plasmon resonance (spr)
scanning electron microscope (sem)
url https://etj.uotechnology.edu.iq/article_175478_60e9a57016fcc2ed13f675437c7276b1.pdf
work_keys_str_mv AT abdulahmohammed easyandnewchemicalsynthesisofstablenanosliverusingpropyleneglycolandglycerinasreducingagents
AT sarabmahmood easyandnewchemicalsynthesisofstablenanosliverusingpropyleneglycolandglycerinasreducingagents