Use of chitin as a template for the preparation of mesostructured ZSM-5

Abstract In this work, mesostructured ZSM-5 zeolite was prepared using chitin as a new template to produce mesoporosity. Different amounts of chitin were used for the synthesis of ZSM-5 in order to verify its influence on the formation of mesopores. All samples were prepared by conventional hydrothe...

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Main Authors: F. C. Drumm, J. S. de Oliveira, M. S. P. Enders, E. I. Müller, E. A. Urquieta-González, G. L. Dotto, E. L. Foletto, S. L. Jahn
Format: Article
Language:English
Published: Associação Brasileira de Cerâmica
Series:Cerâmica
Subjects:
Online Access:http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0366-69132018000200214&lng=en&tlng=en
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author F. C. Drumm
J. S. de Oliveira
M. S. P. Enders
E. I. Müller
E. A. Urquieta-González
G. L. Dotto
E. L. Foletto
S. L. Jahn
author_facet F. C. Drumm
J. S. de Oliveira
M. S. P. Enders
E. I. Müller
E. A. Urquieta-González
G. L. Dotto
E. L. Foletto
S. L. Jahn
author_sort F. C. Drumm
collection DOAJ
description Abstract In this work, mesostructured ZSM-5 zeolite was prepared using chitin as a new template to produce mesoporosity. Different amounts of chitin were used for the synthesis of ZSM-5 in order to verify its influence on the formation of mesopores. All samples were prepared by conventional hydrothermal process. For comparison purposes, ZSM-5 zeolite has also been synthesized without a presence of chitin. The samples were characterized by X-ray diffraction, scanning electron microscopy and N2 adsorption techniques. Experimental results showed that the mesopores volume of the obtained samples increased with increasing amount of chitin in the reaction mixture. Therefore, chitin showed to be a promising template for obtaining the ZSM-5 with mesoporous property.
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spelling doaj.art-8ef1c823a62945c1a6e3f335482a71552022-12-22T03:43:10ZengAssociação Brasileira de CerâmicaCerâmica1678-45536437021421810.1590/0366-69132018643702271S0366-69132018000200214Use of chitin as a template for the preparation of mesostructured ZSM-5F. C. DrummJ. S. de OliveiraM. S. P. EndersE. I. MüllerE. A. Urquieta-GonzálezG. L. DottoE. L. FolettoS. L. JahnAbstract In this work, mesostructured ZSM-5 zeolite was prepared using chitin as a new template to produce mesoporosity. Different amounts of chitin were used for the synthesis of ZSM-5 in order to verify its influence on the formation of mesopores. All samples were prepared by conventional hydrothermal process. For comparison purposes, ZSM-5 zeolite has also been synthesized without a presence of chitin. The samples were characterized by X-ray diffraction, scanning electron microscopy and N2 adsorption techniques. Experimental results showed that the mesopores volume of the obtained samples increased with increasing amount of chitin in the reaction mixture. Therefore, chitin showed to be a promising template for obtaining the ZSM-5 with mesoporous property.http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0366-69132018000200214&lng=en&tlng=enZSM-5 mesoporosasíntesequitina
spellingShingle F. C. Drumm
J. S. de Oliveira
M. S. P. Enders
E. I. Müller
E. A. Urquieta-González
G. L. Dotto
E. L. Foletto
S. L. Jahn
Use of chitin as a template for the preparation of mesostructured ZSM-5
Cerâmica
ZSM-5 mesoporosa
síntese
quitina
title Use of chitin as a template for the preparation of mesostructured ZSM-5
title_full Use of chitin as a template for the preparation of mesostructured ZSM-5
title_fullStr Use of chitin as a template for the preparation of mesostructured ZSM-5
title_full_unstemmed Use of chitin as a template for the preparation of mesostructured ZSM-5
title_short Use of chitin as a template for the preparation of mesostructured ZSM-5
title_sort use of chitin as a template for the preparation of mesostructured zsm 5
topic ZSM-5 mesoporosa
síntese
quitina
url http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0366-69132018000200214&lng=en&tlng=en
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