Citric acid supported on melamine-based COP [CA@MIP] in metal-free on-water synthesis of quinazolinones
A metal-free, efficient, and eco-friendly on-water protocol for the synthesis of quinazolinone derivatives via a tandem one-pot three-component reaction using a novel, efficient, and recyclable heterogeneous catalyst, [CA@MIP] – melamine-based covalent organic polymer supported citric acid, has been...
| Main Authors: | , |
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| Format: | Article |
| Language: | English |
| Published: |
Elsevier
2023-01-01
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| Series: | Tetrahedron Green Chem |
| Subjects: | |
| Online Access: | http://www.sciencedirect.com/science/article/pii/S2773223123000018 |
| _version_ | 1797342111536775168 |
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| author | Atif Mustafa Zeba N. Siddiqui |
| author_facet | Atif Mustafa Zeba N. Siddiqui |
| author_sort | Atif Mustafa |
| collection | DOAJ |
| description | A metal-free, efficient, and eco-friendly on-water protocol for the synthesis of quinazolinone derivatives via a tandem one-pot three-component reaction using a novel, efficient, and recyclable heterogeneous catalyst, [CA@MIP] – melamine-based covalent organic polymer supported citric acid, has been described. The catalyst has been synthesized by a simple procedure and is well characterized by numerous spectroscopic techniques such as Fourier Transform Infrared (FTIR), Scanning Electron Microscope (SEM), Powder X-ray diffraction (PXRD), Brunauer-Emmett-Teller (BET), Energy Dispersive X-ray (EDX), and Thermal Gravimetric (TG) analyses. [CA@MIP] showed excellent catalytic potential offering quinazolinones in excellent yields (>85%) in a short reaction time period and was reusable for up to five successive runs. |
| first_indexed | 2024-03-08T10:28:41Z |
| format | Article |
| id | doaj.art-8f13df4cb68a4f809c268d1815d4636a |
| institution | Directory Open Access Journal |
| issn | 2773-2231 |
| language | English |
| last_indexed | 2024-03-08T10:28:41Z |
| publishDate | 2023-01-01 |
| publisher | Elsevier |
| record_format | Article |
| series | Tetrahedron Green Chem |
| spelling | doaj.art-8f13df4cb68a4f809c268d1815d4636a2024-01-27T07:02:55ZengElsevierTetrahedron Green Chem2773-22312023-01-011100002Citric acid supported on melamine-based COP [CA@MIP] in metal-free on-water synthesis of quinazolinonesAtif Mustafa0Zeba N. Siddiqui1Green Chemistry Laboratory, Organic Chemistry Division, Department of Chemistry, Aligarh Muslim University, Aligarh, 202002, IndiaCorresponding author.; Green Chemistry Laboratory, Organic Chemistry Division, Department of Chemistry, Aligarh Muslim University, Aligarh, 202002, IndiaA metal-free, efficient, and eco-friendly on-water protocol for the synthesis of quinazolinone derivatives via a tandem one-pot three-component reaction using a novel, efficient, and recyclable heterogeneous catalyst, [CA@MIP] – melamine-based covalent organic polymer supported citric acid, has been described. The catalyst has been synthesized by a simple procedure and is well characterized by numerous spectroscopic techniques such as Fourier Transform Infrared (FTIR), Scanning Electron Microscope (SEM), Powder X-ray diffraction (PXRD), Brunauer-Emmett-Teller (BET), Energy Dispersive X-ray (EDX), and Thermal Gravimetric (TG) analyses. [CA@MIP] showed excellent catalytic potential offering quinazolinones in excellent yields (>85%) in a short reaction time period and was reusable for up to five successive runs.http://www.sciencedirect.com/science/article/pii/S2773223123000018QuinazolinonesHeterogeneous catalysisWaterCitric acidHeterocyclesCovalent Organic Polymer |
| spellingShingle | Atif Mustafa Zeba N. Siddiqui Citric acid supported on melamine-based COP [CA@MIP] in metal-free on-water synthesis of quinazolinones Tetrahedron Green Chem Quinazolinones Heterogeneous catalysis Water Citric acid Heterocycles Covalent Organic Polymer |
| title | Citric acid supported on melamine-based COP [CA@MIP] in metal-free on-water synthesis of quinazolinones |
| title_full | Citric acid supported on melamine-based COP [CA@MIP] in metal-free on-water synthesis of quinazolinones |
| title_fullStr | Citric acid supported on melamine-based COP [CA@MIP] in metal-free on-water synthesis of quinazolinones |
| title_full_unstemmed | Citric acid supported on melamine-based COP [CA@MIP] in metal-free on-water synthesis of quinazolinones |
| title_short | Citric acid supported on melamine-based COP [CA@MIP] in metal-free on-water synthesis of quinazolinones |
| title_sort | citric acid supported on melamine based cop ca mip in metal free on water synthesis of quinazolinones |
| topic | Quinazolinones Heterogeneous catalysis Water Citric acid Heterocycles Covalent Organic Polymer |
| url | http://www.sciencedirect.com/science/article/pii/S2773223123000018 |
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