ZrB2-CNTs Nanocomposites Fabricated by Spark Plasma Sintering

ZrB2-based nanocomposites with and without carbon nanotubes (CNTs) as reinforcement were prepared at 1600 °C by spark plasma sintering. The effects of CNTs on the microstructure and mechanical properties of nano-ZrB2 matrix composites were studied. The results indicated that adding CNTs can inhibit...

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Main Authors: Hua Jin, Songhe Meng, Weihua Xie, Chenghai Xu, Jiahong Niu
Format: Article
Language:English
Published: MDPI AG 2016-11-01
Series:Materials
Subjects:
Online Access:http://www.mdpi.com/1996-1944/9/12/967
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author Hua Jin
Songhe Meng
Weihua Xie
Chenghai Xu
Jiahong Niu
author_facet Hua Jin
Songhe Meng
Weihua Xie
Chenghai Xu
Jiahong Niu
author_sort Hua Jin
collection DOAJ
description ZrB2-based nanocomposites with and without carbon nanotubes (CNTs) as reinforcement were prepared at 1600 °C by spark plasma sintering. The effects of CNTs on the microstructure and mechanical properties of nano-ZrB2 matrix composites were studied. The results indicated that adding CNTs can inhibit the abnormal grain growth of ZrB2 grains and improve the fracture toughness of the composites. The toughness mechanisms were crack deflection, crack bridging, debonding, and pull-out of CNTs. The experimental results of the nanograined ZrB2-CNTs composites were compared with those of the micro-grained ZrB2-CNTs composites. Due to the small size and surface effects, the nanograined ZrB2-CNTs composites exhibited stronger mechanical properties: the hardness, flexural strength and fracture toughness were 18.7 ± 0.2 GPa, 1016 ± 75 MPa, and 8.5 ± 0.4 MPa·m1/2, respectively.
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spelling doaj.art-8f746e25840e42a7b069388aed30d8172022-12-22T03:07:09ZengMDPI AGMaterials1996-19442016-11-0191296710.3390/ma9120967ma9120967ZrB2-CNTs Nanocomposites Fabricated by Spark Plasma SinteringHua Jin0Songhe Meng1Weihua Xie2Chenghai Xu3Jiahong Niu4National Key Laboratory of Science and Technology on Advanced Composites in Special Environments, Harbin Institute of Technology, Harbin 150001, ChinaNational Key Laboratory of Science and Technology on Advanced Composites in Special Environments, Harbin Institute of Technology, Harbin 150001, ChinaNational Key Laboratory of Science and Technology on Advanced Composites in Special Environments, Harbin Institute of Technology, Harbin 150001, ChinaNational Key Laboratory of Science and Technology on Advanced Composites in Special Environments, Harbin Institute of Technology, Harbin 150001, ChinaNational Key Laboratory of Science and Technology on Advanced Composites in Special Environments, Harbin Institute of Technology, Harbin 150001, ChinaZrB2-based nanocomposites with and without carbon nanotubes (CNTs) as reinforcement were prepared at 1600 °C by spark plasma sintering. The effects of CNTs on the microstructure and mechanical properties of nano-ZrB2 matrix composites were studied. The results indicated that adding CNTs can inhibit the abnormal grain growth of ZrB2 grains and improve the fracture toughness of the composites. The toughness mechanisms were crack deflection, crack bridging, debonding, and pull-out of CNTs. The experimental results of the nanograined ZrB2-CNTs composites were compared with those of the micro-grained ZrB2-CNTs composites. Due to the small size and surface effects, the nanograined ZrB2-CNTs composites exhibited stronger mechanical properties: the hardness, flexural strength and fracture toughness were 18.7 ± 0.2 GPa, 1016 ± 75 MPa, and 8.5 ± 0.4 MPa·m1/2, respectively.http://www.mdpi.com/1996-1944/9/12/967nanocompositescarbon nanotubes (CNTs)ZrB2fracture toughnessstrength
spellingShingle Hua Jin
Songhe Meng
Weihua Xie
Chenghai Xu
Jiahong Niu
ZrB2-CNTs Nanocomposites Fabricated by Spark Plasma Sintering
Materials
nanocomposites
carbon nanotubes (CNTs)
ZrB2
fracture toughness
strength
title ZrB2-CNTs Nanocomposites Fabricated by Spark Plasma Sintering
title_full ZrB2-CNTs Nanocomposites Fabricated by Spark Plasma Sintering
title_fullStr ZrB2-CNTs Nanocomposites Fabricated by Spark Plasma Sintering
title_full_unstemmed ZrB2-CNTs Nanocomposites Fabricated by Spark Plasma Sintering
title_short ZrB2-CNTs Nanocomposites Fabricated by Spark Plasma Sintering
title_sort zrb2 cnts nanocomposites fabricated by spark plasma sintering
topic nanocomposites
carbon nanotubes (CNTs)
ZrB2
fracture toughness
strength
url http://www.mdpi.com/1996-1944/9/12/967
work_keys_str_mv AT huajin zrb2cntsnanocompositesfabricatedbysparkplasmasintering
AT songhemeng zrb2cntsnanocompositesfabricatedbysparkplasmasintering
AT weihuaxie zrb2cntsnanocompositesfabricatedbysparkplasmasintering
AT chenghaixu zrb2cntsnanocompositesfabricatedbysparkplasmasintering
AT jiahongniu zrb2cntsnanocompositesfabricatedbysparkplasmasintering