Silver(I) Recovery by Ion Flotation Process from Aqueous Solutions in Cells with Spargers

Extractive metallurgy has recently turned its attention to waste treatment for the recovery of precious metals through innovative metallurgical processes, such as ion flotation. This work studied the influence of several chemical and physical factors, such as the concentration of xanthate [x], froth...

Full description

Bibliographic Details
Main Authors: Laura P. Ángeles Palazuelos, Mizraim U. Flores Guerrero, Miguel Pérez Labra, Iván A. Reyes Domínguez, Ramiro Escudero García, Francisco Patiño Cardona, Francisco R. Barrientos Hernández, Julio C. Juárez Tapia, Martín Reyes Pérez
Format: Article
Language:English
Published: MDPI AG 2023-04-01
Series:Minerals
Subjects:
Online Access:https://www.mdpi.com/2075-163X/13/4/572
_version_ 1797604178503139328
author Laura P. Ángeles Palazuelos
Mizraim U. Flores Guerrero
Miguel Pérez Labra
Iván A. Reyes Domínguez
Ramiro Escudero García
Francisco Patiño Cardona
Francisco R. Barrientos Hernández
Julio C. Juárez Tapia
Martín Reyes Pérez
author_facet Laura P. Ángeles Palazuelos
Mizraim U. Flores Guerrero
Miguel Pérez Labra
Iván A. Reyes Domínguez
Ramiro Escudero García
Francisco Patiño Cardona
Francisco R. Barrientos Hernández
Julio C. Juárez Tapia
Martín Reyes Pérez
author_sort Laura P. Ángeles Palazuelos
collection DOAJ
description Extractive metallurgy has recently turned its attention to waste treatment for the recovery of precious metals through innovative metallurgical processes, such as ion flotation. This work studied the influence of several chemical and physical factors, such as the concentration of xanthate [x], frother agent [e], dithiophosphate [xl], pH, superficial gas velocity Jg, percentage of gas holdup Eg, bubble diameter (Db) calculated with the drift flux model, and the type of sparger, in the efficiency of silver(I) recovery by the ion flotation technique in sub-aerated cells. The results obtained indicate a 90.7% <i>v</i>/<i>v</i> recovery of silver(I) under conditions of 3.77 × 10<sup>−4</sup> M [x], 1.25 × 10<sup>−4</sup> M [e], Jg 0.5 cm/s, Jl 0.19 cm/s, Eg of 4.1% <i>v</i>/<i>v</i>, and Optimal Db of 0.11 cm, with a rigid bubble generator, achieving an apparent flotation kinetics of 4.16 1/min. The use of combinations [x]–[xl] achieve a silver(I) recovery of 86.9% with a Jg of 1.0 cm/s. The best recovery efficiencies achieved 93% <i>w</i>/<i>w</i> silver(I) are with pH 8.0, [e] of 1.25 × 10<sup>−4</sup>, Jl of 0.19 (cm/s) and a rigid sparger compared to a flexible one.
first_indexed 2024-03-11T04:42:42Z
format Article
id doaj.art-9021c1299ffb4c728bc5b0be581fed36
institution Directory Open Access Journal
issn 2075-163X
language English
last_indexed 2024-03-11T04:42:42Z
publishDate 2023-04-01
publisher MDPI AG
record_format Article
series Minerals
spelling doaj.art-9021c1299ffb4c728bc5b0be581fed362023-11-17T20:36:35ZengMDPI AGMinerals2075-163X2023-04-0113457210.3390/min13040572Silver(I) Recovery by Ion Flotation Process from Aqueous Solutions in Cells with SpargersLaura P. Ángeles Palazuelos0Mizraim U. Flores Guerrero1Miguel Pérez Labra2Iván A. Reyes Domínguez3Ramiro Escudero García4Francisco Patiño Cardona5Francisco R. Barrientos Hernández6Julio C. Juárez Tapia7Martín Reyes Pérez8Area Academica de Ciencias de la Tierra y Materiales, Universidad Autónoma del Estado de Hidalgo, Mineral de la Reforma 42186, MexicoArea de Electromecanica Industrial, Universidad Tecnológica de Tulancingo, Tulancingo 43642, MexicoArea Academica de Ciencias de la Tierra y Materiales, Universidad Autónoma del Estado de Hidalgo, Mineral de la Reforma 42186, MexicoInstituto de Metalurgia, Universidad Autónoma de San Luis Potosí, San Luis Potosí 78210, MexicoInstituto de Investigaciones Metalúrgicas, Universidad Michoacana de San Nicolás de Hidalgo, Morelia 58030, MexicoIngenieria en Energia, Universidad Politécnica Metropolitana de Hidalgo, Tolcayuca 43860, MexicoArea Academica de Ciencias de la Tierra y Materiales, Universidad Autónoma del Estado de Hidalgo, Mineral de la Reforma 42186, MexicoArea Academica de Ciencias de la Tierra y Materiales, Universidad Autónoma del Estado de Hidalgo, Mineral de la Reforma 42186, MexicoArea Academica de Ciencias de la Tierra y Materiales, Universidad Autónoma del Estado de Hidalgo, Mineral de la Reforma 42186, MexicoExtractive metallurgy has recently turned its attention to waste treatment for the recovery of precious metals through innovative metallurgical processes, such as ion flotation. This work studied the influence of several chemical and physical factors, such as the concentration of xanthate [x], frother agent [e], dithiophosphate [xl], pH, superficial gas velocity Jg, percentage of gas holdup Eg, bubble diameter (Db) calculated with the drift flux model, and the type of sparger, in the efficiency of silver(I) recovery by the ion flotation technique in sub-aerated cells. The results obtained indicate a 90.7% <i>v</i>/<i>v</i> recovery of silver(I) under conditions of 3.77 × 10<sup>−4</sup> M [x], 1.25 × 10<sup>−4</sup> M [e], Jg 0.5 cm/s, Jl 0.19 cm/s, Eg of 4.1% <i>v</i>/<i>v</i>, and Optimal Db of 0.11 cm, with a rigid bubble generator, achieving an apparent flotation kinetics of 4.16 1/min. The use of combinations [x]–[xl] achieve a silver(I) recovery of 86.9% with a Jg of 1.0 cm/s. The best recovery efficiencies achieved 93% <i>w</i>/<i>w</i> silver(I) are with pH 8.0, [e] of 1.25 × 10<sup>−4</sup>, Jl of 0.19 (cm/s) and a rigid sparger compared to a flexible one.https://www.mdpi.com/2075-163X/13/4/572silverion flotationgas holdupxanthatedrift flux model
spellingShingle Laura P. Ángeles Palazuelos
Mizraim U. Flores Guerrero
Miguel Pérez Labra
Iván A. Reyes Domínguez
Ramiro Escudero García
Francisco Patiño Cardona
Francisco R. Barrientos Hernández
Julio C. Juárez Tapia
Martín Reyes Pérez
Silver(I) Recovery by Ion Flotation Process from Aqueous Solutions in Cells with Spargers
Minerals
silver
ion flotation
gas holdup
xanthate
drift flux model
title Silver(I) Recovery by Ion Flotation Process from Aqueous Solutions in Cells with Spargers
title_full Silver(I) Recovery by Ion Flotation Process from Aqueous Solutions in Cells with Spargers
title_fullStr Silver(I) Recovery by Ion Flotation Process from Aqueous Solutions in Cells with Spargers
title_full_unstemmed Silver(I) Recovery by Ion Flotation Process from Aqueous Solutions in Cells with Spargers
title_short Silver(I) Recovery by Ion Flotation Process from Aqueous Solutions in Cells with Spargers
title_sort silver i recovery by ion flotation process from aqueous solutions in cells with spargers
topic silver
ion flotation
gas holdup
xanthate
drift flux model
url https://www.mdpi.com/2075-163X/13/4/572
work_keys_str_mv AT laurapangelespalazuelos silverirecoverybyionflotationprocessfromaqueoussolutionsincellswithspargers
AT mizraimufloresguerrero silverirecoverybyionflotationprocessfromaqueoussolutionsincellswithspargers
AT miguelperezlabra silverirecoverybyionflotationprocessfromaqueoussolutionsincellswithspargers
AT ivanareyesdominguez silverirecoverybyionflotationprocessfromaqueoussolutionsincellswithspargers
AT ramiroescuderogarcia silverirecoverybyionflotationprocessfromaqueoussolutionsincellswithspargers
AT franciscopatinocardona silverirecoverybyionflotationprocessfromaqueoussolutionsincellswithspargers
AT franciscorbarrientoshernandez silverirecoverybyionflotationprocessfromaqueoussolutionsincellswithspargers
AT juliocjuareztapia silverirecoverybyionflotationprocessfromaqueoussolutionsincellswithspargers
AT martinreyesperez silverirecoverybyionflotationprocessfromaqueoussolutionsincellswithspargers