Analytical strategies based on untargeted and targeted metabolomics for the accurate authentication of organic milk from Jersey and Yak
Organic milk has a high risk of food fraud as it can easily be adulterated with non-organic milk. This study aimed to identify metabolite markers for assessing the authenticity of organic milk from Jersey and Yak. In the untargeted strategy, ultra-high performance liquid chromatography-Q Exactive HF...
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Format: | Article |
Language: | English |
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Elsevier
2023-10-01
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Series: | Food Chemistry: X |
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Online Access: | http://www.sciencedirect.com/science/article/pii/S2590157523002298 |
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author | Min Kang Hongxia Wang Chuxin Chen Ran Suo Jianfeng Sun Quanhong Yue Yaqiong Liu |
author_facet | Min Kang Hongxia Wang Chuxin Chen Ran Suo Jianfeng Sun Quanhong Yue Yaqiong Liu |
author_sort | Min Kang |
collection | DOAJ |
description | Organic milk has a high risk of food fraud as it can easily be adulterated with non-organic milk. This study aimed to identify metabolite markers for assessing the authenticity of organic milk from Jersey and Yak. In the untargeted strategy, ultra-high performance liquid chromatography-Q Exactive HF-X mass spectrometer coupled with chemometrics analysis was used to screen and identify tentative markers of organic milk from Jersey and Yak. In the targeted strategy, a quick and easy method of ultra-performance liquid chromatography–tandem mass spectrometry (UPLC-MS/MS) was developed to quantify three markers. The peptide of Thr-Ala-Val and D-biotin were determined to be metabolite markers for distinguishing organic and non-organic Jersey milk, whereas trimethylamine N-oxide was determined to be a metabolite marker for distinguishing organic and non-organic Yak milk. These findings provide critical information to facilitate assessments of organic milk authenticity. |
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format | Article |
id | doaj.art-90311cb421e84857b2d2979da35a30cf |
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issn | 2590-1575 |
language | English |
last_indexed | 2024-03-11T22:31:02Z |
publishDate | 2023-10-01 |
publisher | Elsevier |
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series | Food Chemistry: X |
spelling | doaj.art-90311cb421e84857b2d2979da35a30cf2023-09-23T05:12:16ZengElsevierFood Chemistry: X2590-15752023-10-0119100786Analytical strategies based on untargeted and targeted metabolomics for the accurate authentication of organic milk from Jersey and YakMin Kang0Hongxia Wang1Chuxin Chen2Ran Suo3Jianfeng Sun4Quanhong Yue5Yaqiong Liu6College of Food Science and Technology, Hebei Agricultural University, 289th Lingyusi Street, Lianchi District, Baoding 071000, ChinaCollege of Food Science and Technology, Hebei Agricultural University, 289th Lingyusi Street, Lianchi District, Baoding 071000, ChinaCollege of Food Science and Technology, Hebei Agricultural University, 289th Lingyusi Street, Lianchi District, Baoding 071000, ChinaCorresponding authors.; College of Food Science and Technology, Hebei Agricultural University, 289th Lingyusi Street, Lianchi District, Baoding 071000, ChinaCorresponding authors.; College of Food Science and Technology, Hebei Agricultural University, 289th Lingyusi Street, Lianchi District, Baoding 071000, ChinaCollege of Food Science and Technology, Hebei Agricultural University, 289th Lingyusi Street, Lianchi District, Baoding 071000, ChinaCollege of Food Science and Technology, Hebei Agricultural University, 289th Lingyusi Street, Lianchi District, Baoding 071000, ChinaOrganic milk has a high risk of food fraud as it can easily be adulterated with non-organic milk. This study aimed to identify metabolite markers for assessing the authenticity of organic milk from Jersey and Yak. In the untargeted strategy, ultra-high performance liquid chromatography-Q Exactive HF-X mass spectrometer coupled with chemometrics analysis was used to screen and identify tentative markers of organic milk from Jersey and Yak. In the targeted strategy, a quick and easy method of ultra-performance liquid chromatography–tandem mass spectrometry (UPLC-MS/MS) was developed to quantify three markers. The peptide of Thr-Ala-Val and D-biotin were determined to be metabolite markers for distinguishing organic and non-organic Jersey milk, whereas trimethylamine N-oxide was determined to be a metabolite marker for distinguishing organic and non-organic Yak milk. These findings provide critical information to facilitate assessments of organic milk authenticity.http://www.sciencedirect.com/science/article/pii/S2590157523002298AuthenticityJersey milkMetabolomicYak milk |
spellingShingle | Min Kang Hongxia Wang Chuxin Chen Ran Suo Jianfeng Sun Quanhong Yue Yaqiong Liu Analytical strategies based on untargeted and targeted metabolomics for the accurate authentication of organic milk from Jersey and Yak Food Chemistry: X Authenticity Jersey milk Metabolomic Yak milk |
title | Analytical strategies based on untargeted and targeted metabolomics for the accurate authentication of organic milk from Jersey and Yak |
title_full | Analytical strategies based on untargeted and targeted metabolomics for the accurate authentication of organic milk from Jersey and Yak |
title_fullStr | Analytical strategies based on untargeted and targeted metabolomics for the accurate authentication of organic milk from Jersey and Yak |
title_full_unstemmed | Analytical strategies based on untargeted and targeted metabolomics for the accurate authentication of organic milk from Jersey and Yak |
title_short | Analytical strategies based on untargeted and targeted metabolomics for the accurate authentication of organic milk from Jersey and Yak |
title_sort | analytical strategies based on untargeted and targeted metabolomics for the accurate authentication of organic milk from jersey and yak |
topic | Authenticity Jersey milk Metabolomic Yak milk |
url | http://www.sciencedirect.com/science/article/pii/S2590157523002298 |
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