Correlating Volatile Lipid Oxidation Compounds with Consumer Sensory Data in Dairy Based Powders during Storage

Lipid oxidation (LO) is a recognised problem in dairy powders due to the formation of volatile odour compounds that can negatively impact sensory perception. Three commercial dairy powders, fat-filled whole milk powder (FFWMP), skim milk powder (SMP), and infant milk formula (IMF), stored under diff...

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Main Authors: Holly J. Clarke, Maurice G. O’Sullivan, Joseph P. Kerry, Kieran N. Kilcawley
Format: Article
Language:English
Published: MDPI AG 2020-04-01
Series:Antioxidants
Subjects:
Online Access:https://www.mdpi.com/2076-3921/9/4/338
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author Holly J. Clarke
Maurice G. O’Sullivan
Joseph P. Kerry
Kieran N. Kilcawley
author_facet Holly J. Clarke
Maurice G. O’Sullivan
Joseph P. Kerry
Kieran N. Kilcawley
author_sort Holly J. Clarke
collection DOAJ
description Lipid oxidation (LO) is a recognised problem in dairy powders due to the formation of volatile odour compounds that can negatively impact sensory perception. Three commercial dairy powders, fat-filled whole milk powder (FFWMP), skim milk powder (SMP), and infant milk formula (IMF), stored under different conditions (21 °C, 37 °C, or 25 °C with 50% humidity), were evaluated by consumer acceptance studies, ranked descriptive sensory analysis, and LO volatile profiling using headspace solid phase microextraction gas chromatography mass spectrometry (HS-SPME GCMS) over 16 weeks. Significant (<i>p</i> = 0.001) differences in the concentration of LO compounds and sensory perception were evident between sample types in the different storage conditions. The sensory acceptance scores for FFWMP and SMP remained stable throughout storage in all conditions, despite the increased perception of some LO products. The IMF sample was perceived negatively in each storage condition and at each time point. Overall increases in hexanal, heptanal, and pentanal correlated with “painty”, “oxidised”, “cooked”, and “caramelised” attributes in all samples. The concentration of some LO volatiles in the IMF was far in excess of those in FFWMP and SMP. High levels of LO volatiles in IMF were presumably due to the addition of polyunsaturated fatty acids (PUFA) in the formulation.
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spelling doaj.art-90ebbeda2aec4e53996f790156d3cf692023-11-19T22:13:37ZengMDPI AGAntioxidants2076-39212020-04-019433810.3390/antiox9040338Correlating Volatile Lipid Oxidation Compounds with Consumer Sensory Data in Dairy Based Powders during StorageHolly J. Clarke0Maurice G. O’Sullivan1Joseph P. Kerry2Kieran N. Kilcawley3Food Quality and Sensory Science, Teagasc Food Research Centre, Moorepark, Fermoy, P61 C996 Co. Cork, IrelandSensory Group, School of Food and Nutritional Sciences, University College Cork, T12 R229 Cork, IrelandFood Packaging Group, School of Food and Nutritional Sciences, University College Cork, T12 R229 Cork, IrelandFood Quality and Sensory Science, Teagasc Food Research Centre, Moorepark, Fermoy, P61 C996 Co. Cork, IrelandLipid oxidation (LO) is a recognised problem in dairy powders due to the formation of volatile odour compounds that can negatively impact sensory perception. Three commercial dairy powders, fat-filled whole milk powder (FFWMP), skim milk powder (SMP), and infant milk formula (IMF), stored under different conditions (21 °C, 37 °C, or 25 °C with 50% humidity), were evaluated by consumer acceptance studies, ranked descriptive sensory analysis, and LO volatile profiling using headspace solid phase microextraction gas chromatography mass spectrometry (HS-SPME GCMS) over 16 weeks. Significant (<i>p</i> = 0.001) differences in the concentration of LO compounds and sensory perception were evident between sample types in the different storage conditions. The sensory acceptance scores for FFWMP and SMP remained stable throughout storage in all conditions, despite the increased perception of some LO products. The IMF sample was perceived negatively in each storage condition and at each time point. Overall increases in hexanal, heptanal, and pentanal correlated with “painty”, “oxidised”, “cooked”, and “caramelised” attributes in all samples. The concentration of some LO volatiles in the IMF was far in excess of those in FFWMP and SMP. High levels of LO volatiles in IMF were presumably due to the addition of polyunsaturated fatty acids (PUFA) in the formulation.https://www.mdpi.com/2076-3921/9/4/338dairy powderinfant milk formulalipid oxidationfatty acidsensoryflavour
spellingShingle Holly J. Clarke
Maurice G. O’Sullivan
Joseph P. Kerry
Kieran N. Kilcawley
Correlating Volatile Lipid Oxidation Compounds with Consumer Sensory Data in Dairy Based Powders during Storage
Antioxidants
dairy powder
infant milk formula
lipid oxidation
fatty acid
sensory
flavour
title Correlating Volatile Lipid Oxidation Compounds with Consumer Sensory Data in Dairy Based Powders during Storage
title_full Correlating Volatile Lipid Oxidation Compounds with Consumer Sensory Data in Dairy Based Powders during Storage
title_fullStr Correlating Volatile Lipid Oxidation Compounds with Consumer Sensory Data in Dairy Based Powders during Storage
title_full_unstemmed Correlating Volatile Lipid Oxidation Compounds with Consumer Sensory Data in Dairy Based Powders during Storage
title_short Correlating Volatile Lipid Oxidation Compounds with Consumer Sensory Data in Dairy Based Powders during Storage
title_sort correlating volatile lipid oxidation compounds with consumer sensory data in dairy based powders during storage
topic dairy powder
infant milk formula
lipid oxidation
fatty acid
sensory
flavour
url https://www.mdpi.com/2076-3921/9/4/338
work_keys_str_mv AT hollyjclarke correlatingvolatilelipidoxidationcompoundswithconsumersensorydataindairybasedpowdersduringstorage
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AT josephpkerry correlatingvolatilelipidoxidationcompoundswithconsumersensorydataindairybasedpowdersduringstorage
AT kierannkilcawley correlatingvolatilelipidoxidationcompoundswithconsumersensorydataindairybasedpowdersduringstorage