Analysis of the Statistical Comparability of the Hardness and Wear of Polymeric Materials for Orthodontic Applications

Background: Clinical success depends on the contact strength and wear resistance of medical devices made of polymer materials. The scientific goal resulted from the problem of using different methods of surface evaluation of materials used in the production of orthodontic appliances. The purpose of...

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Main Authors: Ivo Domagała, Krzysztof Przystupa, Marcel Firlej, Daniel Pieniak, Leszek Gil, Anna Borucka, Ireneusz Naworol, Barbara Biedziak, Mariana Levkiv
Format: Article
Language:English
Published: MDPI AG 2021-05-01
Series:Materials
Subjects:
Online Access:https://www.mdpi.com/1996-1944/14/11/2925
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author Ivo Domagała
Krzysztof Przystupa
Marcel Firlej
Daniel Pieniak
Leszek Gil
Anna Borucka
Ireneusz Naworol
Barbara Biedziak
Mariana Levkiv
author_facet Ivo Domagała
Krzysztof Przystupa
Marcel Firlej
Daniel Pieniak
Leszek Gil
Anna Borucka
Ireneusz Naworol
Barbara Biedziak
Mariana Levkiv
author_sort Ivo Domagała
collection DOAJ
description Background: Clinical success depends on the contact strength and wear resistance of medical devices made of polymer materials. The scientific goal resulted from the problem of using different methods of surface evaluation of materials used in the production of orthodontic appliances. The purpose of the work was an experimental comparative assessment of indentation hardness and scratch hardness and the sliding wear of four selected polymeric materials used in the manufacture of orthodontic appliances. Methods: Four commercial materials were compared. Shore hardness tests and a scratch test with a Rockwell indenter were performed. A sliding wear test was performed using the ball-on-disc method. Statistical PCA and correlation analyses were performed. Results: The results of scratch hardness measurements using a contact profilometer correlated with the Shore hardness to a greater extent than measurements made using an optical microscope. PCA showed that Shore hardness explains 45% of the total variance in all the results across the materials. Conclusions: The scratch hardness method allows for a more explicit ranking of orthodontic polymeric materials when measurements are made with a profilometer. The ranking of sliding wear resistance should be made separately.
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spelling doaj.art-911e49be4ca24eeea05f29bb312455d72023-11-21T21:54:01ZengMDPI AGMaterials1996-19442021-05-011411292510.3390/ma14112925Analysis of the Statistical Comparability of the Hardness and Wear of Polymeric Materials for Orthodontic ApplicationsIvo Domagała0Krzysztof Przystupa1Marcel Firlej2Daniel Pieniak3Leszek Gil4Anna Borucka5Ireneusz Naworol6Barbara Biedziak7Mariana Levkiv8Department of Craniofacial Anomalies, University of Medical Sciences, 70 Bukowska Street, 60-812 Poznań, PolandDepartment of Automation, Lublin University of Technology, 36 Nadbystrzycka Street, 20-618 Lublin, PolandDepartment of Craniofacial Anomalies, University of Medical Sciences, 70 Bukowska Street, 60-812 Poznań, PolandDepartment of Mechanics and Machine Building, University of Economics and Innovations in Lublin, 4 Projektowa Street, 20-209 Lublin, PolandDepartment of Mechanics and Machine Building, University of Economics and Innovations in Lublin, 4 Projektowa Street, 20-209 Lublin, PolandFaculty of Security, Logistics and Management, Military University of Technology, 2 gen. S. Kaliskiego Street, 00-908 Warsaw, PolandFaculty of Safety Engineering and Civil Protection, The Main School of Fire Service, 52/54 Slowackiego Street, 01-629 Warsaw, PolandDepartment of Craniofacial Anomalies, University of Medical Sciences, 70 Bukowska Street, 60-812 Poznań, PolandDepartment of Dental Therapy, I.Horbachevsky Ternopil National Medical University, 1 Maidan Voli, 46000 Ternopil, UkraineBackground: Clinical success depends on the contact strength and wear resistance of medical devices made of polymer materials. The scientific goal resulted from the problem of using different methods of surface evaluation of materials used in the production of orthodontic appliances. The purpose of the work was an experimental comparative assessment of indentation hardness and scratch hardness and the sliding wear of four selected polymeric materials used in the manufacture of orthodontic appliances. Methods: Four commercial materials were compared. Shore hardness tests and a scratch test with a Rockwell indenter were performed. A sliding wear test was performed using the ball-on-disc method. Statistical PCA and correlation analyses were performed. Results: The results of scratch hardness measurements using a contact profilometer correlated with the Shore hardness to a greater extent than measurements made using an optical microscope. PCA showed that Shore hardness explains 45% of the total variance in all the results across the materials. Conclusions: The scratch hardness method allows for a more explicit ranking of orthodontic polymeric materials when measurements are made with a profilometer. The ranking of sliding wear resistance should be made separately.https://www.mdpi.com/1996-1944/14/11/2925microhardnessscratch resistancesliding wearthermocyclingdental biomaterials
spellingShingle Ivo Domagała
Krzysztof Przystupa
Marcel Firlej
Daniel Pieniak
Leszek Gil
Anna Borucka
Ireneusz Naworol
Barbara Biedziak
Mariana Levkiv
Analysis of the Statistical Comparability of the Hardness and Wear of Polymeric Materials for Orthodontic Applications
Materials
microhardness
scratch resistance
sliding wear
thermocycling
dental biomaterials
title Analysis of the Statistical Comparability of the Hardness and Wear of Polymeric Materials for Orthodontic Applications
title_full Analysis of the Statistical Comparability of the Hardness and Wear of Polymeric Materials for Orthodontic Applications
title_fullStr Analysis of the Statistical Comparability of the Hardness and Wear of Polymeric Materials for Orthodontic Applications
title_full_unstemmed Analysis of the Statistical Comparability of the Hardness and Wear of Polymeric Materials for Orthodontic Applications
title_short Analysis of the Statistical Comparability of the Hardness and Wear of Polymeric Materials for Orthodontic Applications
title_sort analysis of the statistical comparability of the hardness and wear of polymeric materials for orthodontic applications
topic microhardness
scratch resistance
sliding wear
thermocycling
dental biomaterials
url https://www.mdpi.com/1996-1944/14/11/2925
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