Correlation between the Dendritic Structure and Lattice Parameter of γ′-Phase in Single-Crystalline Turbine Blades Made of Superalloys

The dendritic structure and the distribution of the γ′-phase lattice parameter (a<sub>γ′</sub>) along selected lines of the longitudinal section in a model single-crystalline blade made of CMSX-4<sup>®</sup> nickel-based superalloy were studied. It was established that there...

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Main Authors: Jacek Krawczyk, Włodzimierz Bogdanowicz
Format: Article
Language:English
Published: MDPI AG 2022-01-01
Series:Materials
Subjects:
Online Access:https://www.mdpi.com/1996-1944/15/3/781
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author Jacek Krawczyk
Włodzimierz Bogdanowicz
author_facet Jacek Krawczyk
Włodzimierz Bogdanowicz
author_sort Jacek Krawczyk
collection DOAJ
description The dendritic structure and the distribution of the γ′-phase lattice parameter (a<sub>γ′</sub>) along selected lines of the longitudinal section in a model single-crystalline blade made of CMSX-4<sup>®</sup> nickel-based superalloy were studied. It was established that there is a correlation between the value of the a<sub>γ′</sub> and the predomination of initial or ending fragments of the secondary dendrite arms. It is most noticed for the areas where the dendrite growth conditions are similar to steady. They are located in the center and near the root’s selector extension (SE) area. The correlation has been related to the dendritic segregation mechanism. It was shown that in the single-crystalline blades obtained by the directional crystallization using a spiral selector, the “walls” of the primary dendrite arms that grow at a low angle to the blade axis are created. It was found for the first time that the value of the lattice parameter a<sub>γ′</sub> is decreased near such “walls”. Additionally, it was found that competitive growth of the dendrites may occur at a distance of even several millimeters from the bottom surface of the root. The first-time applied X-ray diffraction measurements of a<sub>γ′</sub> made in a single-pass along the line allow the analysis of the dendritic segregation in the whole blade cast.
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spelling doaj.art-913b25f411e74fab9ecb32e057568f502023-11-23T16:57:02ZengMDPI AGMaterials1996-19442022-01-0115378110.3390/ma15030781Correlation between the Dendritic Structure and Lattice Parameter of γ′-Phase in Single-Crystalline Turbine Blades Made of SuperalloysJacek Krawczyk0Włodzimierz Bogdanowicz1Institute of Materials Engineering, University of Silesia in Katowice, 1a 75 Pułku Piechoty St., 41-500 Chorzów, PolandInstitute of Materials Engineering, University of Silesia in Katowice, 1a 75 Pułku Piechoty St., 41-500 Chorzów, PolandThe dendritic structure and the distribution of the γ′-phase lattice parameter (a<sub>γ′</sub>) along selected lines of the longitudinal section in a model single-crystalline blade made of CMSX-4<sup>®</sup> nickel-based superalloy were studied. It was established that there is a correlation between the value of the a<sub>γ′</sub> and the predomination of initial or ending fragments of the secondary dendrite arms. It is most noticed for the areas where the dendrite growth conditions are similar to steady. They are located in the center and near the root’s selector extension (SE) area. The correlation has been related to the dendritic segregation mechanism. It was shown that in the single-crystalline blades obtained by the directional crystallization using a spiral selector, the “walls” of the primary dendrite arms that grow at a low angle to the blade axis are created. It was found for the first time that the value of the lattice parameter a<sub>γ′</sub> is decreased near such “walls”. Additionally, it was found that competitive growth of the dendrites may occur at a distance of even several millimeters from the bottom surface of the root. The first-time applied X-ray diffraction measurements of a<sub>γ′</sub> made in a single-pass along the line allow the analysis of the dendritic segregation in the whole blade cast.https://www.mdpi.com/1996-1944/15/3/781nickel-based superalloyX-ray diffractionlattice parameterdendritic array
spellingShingle Jacek Krawczyk
Włodzimierz Bogdanowicz
Correlation between the Dendritic Structure and Lattice Parameter of γ′-Phase in Single-Crystalline Turbine Blades Made of Superalloys
Materials
nickel-based superalloy
X-ray diffraction
lattice parameter
dendritic array
title Correlation between the Dendritic Structure and Lattice Parameter of γ′-Phase in Single-Crystalline Turbine Blades Made of Superalloys
title_full Correlation between the Dendritic Structure and Lattice Parameter of γ′-Phase in Single-Crystalline Turbine Blades Made of Superalloys
title_fullStr Correlation between the Dendritic Structure and Lattice Parameter of γ′-Phase in Single-Crystalline Turbine Blades Made of Superalloys
title_full_unstemmed Correlation between the Dendritic Structure and Lattice Parameter of γ′-Phase in Single-Crystalline Turbine Blades Made of Superalloys
title_short Correlation between the Dendritic Structure and Lattice Parameter of γ′-Phase in Single-Crystalline Turbine Blades Made of Superalloys
title_sort correlation between the dendritic structure and lattice parameter of γ phase in single crystalline turbine blades made of superalloys
topic nickel-based superalloy
X-ray diffraction
lattice parameter
dendritic array
url https://www.mdpi.com/1996-1944/15/3/781
work_keys_str_mv AT jacekkrawczyk correlationbetweenthedendriticstructureandlatticeparameterofgphaseinsinglecrystallineturbinebladesmadeofsuperalloys
AT włodzimierzbogdanowicz correlationbetweenthedendriticstructureandlatticeparameterofgphaseinsinglecrystallineturbinebladesmadeofsuperalloys