Crystal structure of 2-methylpiperazine-1,4-diium bis(hydrogen maleate)
In the title salt, C5H14N22+·2C4H3O4−, the asymmetric unit contains two independent 2-methylpiperazinium dications, which comprise a racemic pair, and four hydrogen maleate monoanions. In the roughly planar hydrogen maleate anions, intramolecular O—H...O hydrogen bonds generate S(7) rings. In the cr...
| Main Authors: | , , , |
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| Format: | Article |
| Language: | English |
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International Union of Crystallography
2015-03-01
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| Series: | Acta Crystallographica Section E: Crystallographic Communications |
| Subjects: | |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S2056989015003102 |
| _version_ | 1798031687136837632 |
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| author | Intissar Wecharine Arto Valkonen Mohamed Rzaigui Wajda Smirani Sta |
| author_facet | Intissar Wecharine Arto Valkonen Mohamed Rzaigui Wajda Smirani Sta |
| author_sort | Intissar Wecharine |
| collection | DOAJ |
| description | In the title salt, C5H14N22+·2C4H3O4−, the asymmetric unit contains two independent 2-methylpiperazinium dications, which comprise a racemic pair, and four hydrogen maleate monoanions. In the roughly planar hydrogen maleate anions, intramolecular O—H...O hydrogen bonds generate S(7) rings. In the crystal, the four independent anions are linked to the 2-methylpiperazinium cations through N—H...O hydrogen bonds, forming two-dimensional layered structures lying parallel to (001). |
| first_indexed | 2024-04-11T20:01:29Z |
| format | Article |
| id | doaj.art-91a624858b254e68b7bce4a63c86a0fb |
| institution | Directory Open Access Journal |
| issn | 2056-9890 |
| language | English |
| last_indexed | 2024-04-11T20:01:29Z |
| publishDate | 2015-03-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | Acta Crystallographica Section E: Crystallographic Communications |
| spelling | doaj.art-91a624858b254e68b7bce4a63c86a0fb2022-12-22T04:05:35ZengInternational Union of CrystallographyActa Crystallographica Section E: Crystallographic Communications2056-98902015-03-01713o193o19410.1107/S2056989015003102zs2325Crystal structure of 2-methylpiperazine-1,4-diium bis(hydrogen maleate)Intissar Wecharine0Arto Valkonen1Mohamed Rzaigui2Wajda Smirani Sta3Laboratoire de chimie des Matériaux, Faculté des Sciences de Bizerte, Université de Carthage, 7021 Zarzouna Bizerte, TunisiaDepartment of Chemistry and Bioengineering, Tampere University of Technology, PO Box 541, 33101 Tampere, FinlandLaboratoire de chimie des Matériaux, Faculté des Sciences de Bizerte, Université de Carthage, 7021 Zarzouna Bizerte, TunisiaLaboratoire de chimie des Matériaux, Faculté des Sciences de Bizerte, Université de Carthage, 7021 Zarzouna Bizerte, TunisiaIn the title salt, C5H14N22+·2C4H3O4−, the asymmetric unit contains two independent 2-methylpiperazinium dications, which comprise a racemic pair, and four hydrogen maleate monoanions. In the roughly planar hydrogen maleate anions, intramolecular O—H...O hydrogen bonds generate S(7) rings. In the crystal, the four independent anions are linked to the 2-methylpiperazinium cations through N—H...O hydrogen bonds, forming two-dimensional layered structures lying parallel to (001).http://scripts.iucr.org/cgi-bin/paper?S2056989015003102crystal structure2-methylpiperazine-1,4-diiumhydrogen maleatehydrogen bonding |
| spellingShingle | Intissar Wecharine Arto Valkonen Mohamed Rzaigui Wajda Smirani Sta Crystal structure of 2-methylpiperazine-1,4-diium bis(hydrogen maleate) Acta Crystallographica Section E: Crystallographic Communications crystal structure 2-methylpiperazine-1,4-diium hydrogen maleate hydrogen bonding |
| title | Crystal structure of 2-methylpiperazine-1,4-diium bis(hydrogen maleate) |
| title_full | Crystal structure of 2-methylpiperazine-1,4-diium bis(hydrogen maleate) |
| title_fullStr | Crystal structure of 2-methylpiperazine-1,4-diium bis(hydrogen maleate) |
| title_full_unstemmed | Crystal structure of 2-methylpiperazine-1,4-diium bis(hydrogen maleate) |
| title_short | Crystal structure of 2-methylpiperazine-1,4-diium bis(hydrogen maleate) |
| title_sort | crystal structure of 2 methylpiperazine 1 4 diium bis hydrogen maleate |
| topic | crystal structure 2-methylpiperazine-1,4-diium hydrogen maleate hydrogen bonding |
| url | http://scripts.iucr.org/cgi-bin/paper?S2056989015003102 |
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