Synthesis and Characterization of Ni Nanoparticles via the Microemulsion Technique and Its Applications for Energy Storage Devices

Herein, a unique synthetic approach called microemulsion is used to create nickel nanoparticles (Ni-NPs). SEM, TEM, EDX, and XRD techniques were employed for the investigation of morphology and structures of the synthesized material. Electrons from electroactive components are transferred to externa...

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Main Authors: Zia Ur Rehman, Mohsan Nawaz, Hameed Ullah, Imad Uddin, Salma Shad, Elsyed Eldin, Razan A. Alshgari, Aboud Ahmed Awadh Bahajjaj, Waqas Ul Arifeen, Muhammad Sufyan Javed
Format: Article
Language:English
Published: MDPI AG 2022-12-01
Series:Materials
Subjects:
Online Access:https://www.mdpi.com/1996-1944/16/1/325
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author Zia Ur Rehman
Mohsan Nawaz
Hameed Ullah
Imad Uddin
Salma Shad
Elsyed Eldin
Razan A. Alshgari
Aboud Ahmed Awadh Bahajjaj
Waqas Ul Arifeen
Muhammad Sufyan Javed
author_facet Zia Ur Rehman
Mohsan Nawaz
Hameed Ullah
Imad Uddin
Salma Shad
Elsyed Eldin
Razan A. Alshgari
Aboud Ahmed Awadh Bahajjaj
Waqas Ul Arifeen
Muhammad Sufyan Javed
author_sort Zia Ur Rehman
collection DOAJ
description Herein, a unique synthetic approach called microemulsion is used to create nickel nanoparticles (Ni-NPs). SEM, TEM, EDX, and XRD techniques were employed for the investigation of morphology and structures of the synthesized material. Electrons from electroactive components are transferred to external circuits by Ni-NPs’ superior electrical conductivity and interconnected nanostructures, which also provide a large number of channels for ion diffusion and additional active sites. The experimental findings showed that as a positive electrode for supercapacitors (SC), Ni-NPs had an outstanding ability to store charge, with a dominant capacitive charge storage of 72.4% when measured at 10 mV/s. Furthermore, at 1 A/g, Ni-NP electrodes exhibit a maximum capacitance of 730 F/g. Further, the Ni-NP electrode retains 92.4% of its capacitance even for 5000 cycles, highlighting possible applications for it in the developing field of renewable energy. The current study provides a new method for producing high-rate next-generation electrodes for supercapacitors.
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spelling doaj.art-9244bcff87cf4e5c9733131e5cd549742023-11-16T15:50:09ZengMDPI AGMaterials1996-19442022-12-0116132510.3390/ma16010325Synthesis and Characterization of Ni Nanoparticles via the Microemulsion Technique and Its Applications for Energy Storage DevicesZia Ur Rehman0Mohsan Nawaz1Hameed Ullah2Imad Uddin3Salma Shad4Elsyed Eldin5Razan A. Alshgari6Aboud Ahmed Awadh Bahajjaj7Waqas Ul Arifeen8Muhammad Sufyan Javed9Department of Chemistry, The University of Haripur, Haripur 22620, PakistanDepartment of Chemistry, Hazara University Mansehra, Mansehra 21120, PakistanDepartment of Chemistry, Islamia College University Peshawar, Peshawar 25120, PakistanDepartment of Chemistry, The University of Haripur, Haripur 22620, PakistanDepartment of Chemistry, The University of Haripur, Haripur 22620, PakistanFaculty of Engineering and Technology, Future University in Egypt, New Cairo 11835, EgyptChemistry Department, College of Science, King Saud University, Riyadh 11451, Saudi ArabiaChemistry Department, College of Science, King Saud University, Riyadh 11451, Saudi ArabiaSchool of Mechanical Engineering, Yeungnam University, Gyeongsangbuk-do, Gyeongsan-si 38541, Republic of KoreaSchool of Physical Science and Technology, Lanzhou University, Lanzhou 730000, ChinaHerein, a unique synthetic approach called microemulsion is used to create nickel nanoparticles (Ni-NPs). SEM, TEM, EDX, and XRD techniques were employed for the investigation of morphology and structures of the synthesized material. Electrons from electroactive components are transferred to external circuits by Ni-NPs’ superior electrical conductivity and interconnected nanostructures, which also provide a large number of channels for ion diffusion and additional active sites. The experimental findings showed that as a positive electrode for supercapacitors (SC), Ni-NPs had an outstanding ability to store charge, with a dominant capacitive charge storage of 72.4% when measured at 10 mV/s. Furthermore, at 1 A/g, Ni-NP electrodes exhibit a maximum capacitance of 730 F/g. Further, the Ni-NP electrode retains 92.4% of its capacitance even for 5000 cycles, highlighting possible applications for it in the developing field of renewable energy. The current study provides a new method for producing high-rate next-generation electrodes for supercapacitors.https://www.mdpi.com/1996-1944/16/1/325supercapacitornickel nanoparticlesmicroemulsionpositive electrode
spellingShingle Zia Ur Rehman
Mohsan Nawaz
Hameed Ullah
Imad Uddin
Salma Shad
Elsyed Eldin
Razan A. Alshgari
Aboud Ahmed Awadh Bahajjaj
Waqas Ul Arifeen
Muhammad Sufyan Javed
Synthesis and Characterization of Ni Nanoparticles via the Microemulsion Technique and Its Applications for Energy Storage Devices
Materials
supercapacitor
nickel nanoparticles
microemulsion
positive electrode
title Synthesis and Characterization of Ni Nanoparticles via the Microemulsion Technique and Its Applications for Energy Storage Devices
title_full Synthesis and Characterization of Ni Nanoparticles via the Microemulsion Technique and Its Applications for Energy Storage Devices
title_fullStr Synthesis and Characterization of Ni Nanoparticles via the Microemulsion Technique and Its Applications for Energy Storage Devices
title_full_unstemmed Synthesis and Characterization of Ni Nanoparticles via the Microemulsion Technique and Its Applications for Energy Storage Devices
title_short Synthesis and Characterization of Ni Nanoparticles via the Microemulsion Technique and Its Applications for Energy Storage Devices
title_sort synthesis and characterization of ni nanoparticles via the microemulsion technique and its applications for energy storage devices
topic supercapacitor
nickel nanoparticles
microemulsion
positive electrode
url https://www.mdpi.com/1996-1944/16/1/325
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