Oxygen as a Possible Technological Adjuvant during the Crushing or the Malaxation Steps, or Both, for the Modulation of the Characteristics of Extra Virgin Olive Oil

In commercial terms, Extra Virgin Olive Oil (EVOO) is considered an exceptional food with excellent sensory and nutritional quality due to its taste, odor, and bioactive compounds; as such, it is of great health interest. This quality can be affected by the oxidative degradation, both chemical and e...

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Main Authors: Gabriel Beltrán Maza, Abraham M. Gila Beltrán, María Paz Aguilera Herrera, Antonio Jiménez Márquez, Araceli Sánchez-Ortiz
Format: Article
Language:English
Published: MDPI AG 2023-05-01
Series:Foods
Subjects:
Online Access:https://www.mdpi.com/2304-8158/12/11/2170
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author Gabriel Beltrán Maza
Abraham M. Gila Beltrán
María Paz Aguilera Herrera
Antonio Jiménez Márquez
Araceli Sánchez-Ortiz
author_facet Gabriel Beltrán Maza
Abraham M. Gila Beltrán
María Paz Aguilera Herrera
Antonio Jiménez Márquez
Araceli Sánchez-Ortiz
author_sort Gabriel Beltrán Maza
collection DOAJ
description In commercial terms, Extra Virgin Olive Oil (EVOO) is considered an exceptional food with excellent sensory and nutritional quality due to its taste, odor, and bioactive compounds; as such, it is of great health interest. This quality can be affected by the oxidative degradation, both chemical and enzymatic (the activity of oxidative, endogenous enzymes from the polyphenol oxidase and peroxidase olive fruit type), of essential components during the extraction and conservation of EVOO. In the bibliography, oxygen reduction during the malaxation process and oil storage has been studied in different ways. However, research concerning oxygen reduction in the crushing of the olive fruit or the malaxation of the paste, or both, in the “real extraction condition” is scarce. Oxygen reduction has been compared to control conditions (the concentration of atmospheric oxygen (21%)). Batches of 200 kg of the olive fruit, ‘Picual’ cultivar, were used and the following treatments were applied: Control (21% O<sub>2</sub> Mill–21% O<sub>2</sub> Mixer), “IC-NM”: Inerted crushing -Normal malaxation (6.25% O<sub>2</sub> Mill-21% O<sub>2</sub> Mixer), “NC-IM”: Normal crushing-Inerted malaxation (21% O<sub>2</sub> Mill-4.39% O<sub>2</sub> Mixer) and “IC-IM”: Inerted crushing -Inerted malaxation (5.5% O<sub>2</sub> Mill-10.5% O<sub>2</sub> Mixer). The parameters of commercial quality covered by regulation (free acidity, peroxide value and absorbency in ultra-violet (K<sub>232</sub> and K<sub>270</sub>)) did not suffer any change concerning the control, and so the oils belong to the commercial category of “Extra Virgin Olive Oil”. The phenolic compounds of the olives involved in the distinctive bitter and pungent taste, health properties, and oxidative stability are increased with the downsizing amounts of oxygen in the IC-NM, NC-IM, and IC-IM treatments with an average of 4, 10, and 20%, respectively. In contrast, the total amount of volatile compounds decreases by 10–20% in all oxygen reduction treatments. The volatile compounds arising from the lipoxygenase pathway, which are responsible for the green and fruity notes of EVOO, also decreased in concentration with the treatments by 15–20%. The results show how oxygen reduction in the milling and malaxation stages of olive fruit can modulate the content of phenols, volatile compounds, carotenoids, and chlorophyll pigments in the EVOO to avoid the degradation of the compound with sensorial and nutritional interest.
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spelling doaj.art-92f08e6441494bc78e21c778e4a6b7422023-11-18T07:51:12ZengMDPI AGFoods2304-81582023-05-011211217010.3390/foods12112170Oxygen as a Possible Technological Adjuvant during the Crushing or the Malaxation Steps, or Both, for the Modulation of the Characteristics of Extra Virgin Olive OilGabriel Beltrán Maza0Abraham M. Gila Beltrán1María Paz Aguilera Herrera2Antonio Jiménez Márquez3Araceli Sánchez-Ortiz4Andalusian Institute of Agricultural and Fisheries Research and Training (IFAPA), Agro-Industry and Food Quality Area, Center IFAPA Venta Del Llano, Mengíbar, 23620 Jaén, SpainAndalusian Institute of Agricultural and Fisheries Research and Training (IFAPA), Agro-Industry and Food Quality Area, Center IFAPA Venta Del Llano, Mengíbar, 23620 Jaén, SpainAndalusian Institute of Agricultural and Fisheries Research and Training (IFAPA), Agro-Industry and Food Quality Area, Center IFAPA Venta Del Llano, Mengíbar, 23620 Jaén, SpainAndalusian Institute of Agricultural and Fisheries Research and Training (IFAPA), Agro-Industry and Food Quality Area, Center IFAPA Venta Del Llano, Mengíbar, 23620 Jaén, SpainAndalusian Institute of Agricultural and Fisheries Research and Training (IFAPA), Agro-Industry and Food Quality Area, Center IFAPA Venta Del Llano, Mengíbar, 23620 Jaén, SpainIn commercial terms, Extra Virgin Olive Oil (EVOO) is considered an exceptional food with excellent sensory and nutritional quality due to its taste, odor, and bioactive compounds; as such, it is of great health interest. This quality can be affected by the oxidative degradation, both chemical and enzymatic (the activity of oxidative, endogenous enzymes from the polyphenol oxidase and peroxidase olive fruit type), of essential components during the extraction and conservation of EVOO. In the bibliography, oxygen reduction during the malaxation process and oil storage has been studied in different ways. However, research concerning oxygen reduction in the crushing of the olive fruit or the malaxation of the paste, or both, in the “real extraction condition” is scarce. Oxygen reduction has been compared to control conditions (the concentration of atmospheric oxygen (21%)). Batches of 200 kg of the olive fruit, ‘Picual’ cultivar, were used and the following treatments were applied: Control (21% O<sub>2</sub> Mill–21% O<sub>2</sub> Mixer), “IC-NM”: Inerted crushing -Normal malaxation (6.25% O<sub>2</sub> Mill-21% O<sub>2</sub> Mixer), “NC-IM”: Normal crushing-Inerted malaxation (21% O<sub>2</sub> Mill-4.39% O<sub>2</sub> Mixer) and “IC-IM”: Inerted crushing -Inerted malaxation (5.5% O<sub>2</sub> Mill-10.5% O<sub>2</sub> Mixer). The parameters of commercial quality covered by regulation (free acidity, peroxide value and absorbency in ultra-violet (K<sub>232</sub> and K<sub>270</sub>)) did not suffer any change concerning the control, and so the oils belong to the commercial category of “Extra Virgin Olive Oil”. The phenolic compounds of the olives involved in the distinctive bitter and pungent taste, health properties, and oxidative stability are increased with the downsizing amounts of oxygen in the IC-NM, NC-IM, and IC-IM treatments with an average of 4, 10, and 20%, respectively. In contrast, the total amount of volatile compounds decreases by 10–20% in all oxygen reduction treatments. The volatile compounds arising from the lipoxygenase pathway, which are responsible for the green and fruity notes of EVOO, also decreased in concentration with the treatments by 15–20%. The results show how oxygen reduction in the milling and malaxation stages of olive fruit can modulate the content of phenols, volatile compounds, carotenoids, and chlorophyll pigments in the EVOO to avoid the degradation of the compound with sensorial and nutritional interest.https://www.mdpi.com/2304-8158/12/11/2170carotenoid pigmentschlorophyll pigmentsextraction technologyolive oil qualityoxygenphenolic compounds
spellingShingle Gabriel Beltrán Maza
Abraham M. Gila Beltrán
María Paz Aguilera Herrera
Antonio Jiménez Márquez
Araceli Sánchez-Ortiz
Oxygen as a Possible Technological Adjuvant during the Crushing or the Malaxation Steps, or Both, for the Modulation of the Characteristics of Extra Virgin Olive Oil
Foods
carotenoid pigments
chlorophyll pigments
extraction technology
olive oil quality
oxygen
phenolic compounds
title Oxygen as a Possible Technological Adjuvant during the Crushing or the Malaxation Steps, or Both, for the Modulation of the Characteristics of Extra Virgin Olive Oil
title_full Oxygen as a Possible Technological Adjuvant during the Crushing or the Malaxation Steps, or Both, for the Modulation of the Characteristics of Extra Virgin Olive Oil
title_fullStr Oxygen as a Possible Technological Adjuvant during the Crushing or the Malaxation Steps, or Both, for the Modulation of the Characteristics of Extra Virgin Olive Oil
title_full_unstemmed Oxygen as a Possible Technological Adjuvant during the Crushing or the Malaxation Steps, or Both, for the Modulation of the Characteristics of Extra Virgin Olive Oil
title_short Oxygen as a Possible Technological Adjuvant during the Crushing or the Malaxation Steps, or Both, for the Modulation of the Characteristics of Extra Virgin Olive Oil
title_sort oxygen as a possible technological adjuvant during the crushing or the malaxation steps or both for the modulation of the characteristics of extra virgin olive oil
topic carotenoid pigments
chlorophyll pigments
extraction technology
olive oil quality
oxygen
phenolic compounds
url https://www.mdpi.com/2304-8158/12/11/2170
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