Effect of CaO-TiO<sub>2</sub>-SiO<sub>2</sub> on the Microstructure and Mechanical Properties of Ceramic Corundum Abrasives

Ceramic corundum abrasives were prepared using pseudo-boehmite as a raw material via the sol-gel method. Additives can significantly change the microscopic morphology of abrasives and improve mechanical properties. When 2 wt% CaO-TiO<sub>2</sub>-SiO<sub>2</sub> with a molar r...

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Main Authors: Quanbao Zhao, Zhihong Li, Yumei Zhu
Format: Article
Language:English
Published: MDPI AG 2023-04-01
Series:Inorganics
Subjects:
Online Access:https://www.mdpi.com/2304-6740/11/5/187
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author Quanbao Zhao
Zhihong Li
Yumei Zhu
author_facet Quanbao Zhao
Zhihong Li
Yumei Zhu
author_sort Quanbao Zhao
collection DOAJ
description Ceramic corundum abrasives were prepared using pseudo-boehmite as a raw material via the sol-gel method. Additives can significantly change the microscopic morphology of abrasives and improve mechanical properties. When 2 wt% CaO-TiO<sub>2</sub>-SiO<sub>2</sub> with a molar ratio of 3:4:9 was added, samples with the best morphology and mechanical properties were obtained. Single-particle compressive strength, density, Vickers hardness, and average grain size were 51.45 N, 3.94 g·cm<sup>−3</sup>, 16.43 GPa, and 0.98 μm, respectively. We compared the same additive system with abrasives prepared by ball milling, and found that ball milling was beneficial for obtaining denser and smaller grain size abrasives. On the other hand, abrasives obtained without ball milling had relatively higher single-particle compressive strength. Additionally, the additives are non-precious metal oxides, which can reduce the cost of the synthesis process. In addition, there has been discussion of the connection between microstructure and mechanical characteristics.
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spelling doaj.art-934318b7927c4f18bfe44b079e0d509b2023-11-18T01:48:47ZengMDPI AGInorganics2304-67402023-04-0111518710.3390/inorganics11050187Effect of CaO-TiO<sub>2</sub>-SiO<sub>2</sub> on the Microstructure and Mechanical Properties of Ceramic Corundum AbrasivesQuanbao Zhao0Zhihong Li1Yumei Zhu2Key Laboratory for Advanced Ceramics and Machining Technology of Ministry of Education, School of Materials Science and Engineering, Tianjin University, Tianjin 300072, ChinaKey Laboratory for Advanced Ceramics and Machining Technology of Ministry of Education, School of Materials Science and Engineering, Tianjin University, Tianjin 300072, ChinaKey Laboratory for Advanced Ceramics and Machining Technology of Ministry of Education, School of Materials Science and Engineering, Tianjin University, Tianjin 300072, ChinaCeramic corundum abrasives were prepared using pseudo-boehmite as a raw material via the sol-gel method. Additives can significantly change the microscopic morphology of abrasives and improve mechanical properties. When 2 wt% CaO-TiO<sub>2</sub>-SiO<sub>2</sub> with a molar ratio of 3:4:9 was added, samples with the best morphology and mechanical properties were obtained. Single-particle compressive strength, density, Vickers hardness, and average grain size were 51.45 N, 3.94 g·cm<sup>−3</sup>, 16.43 GPa, and 0.98 μm, respectively. We compared the same additive system with abrasives prepared by ball milling, and found that ball milling was beneficial for obtaining denser and smaller grain size abrasives. On the other hand, abrasives obtained without ball milling had relatively higher single-particle compressive strength. Additionally, the additives are non-precious metal oxides, which can reduce the cost of the synthesis process. In addition, there has been discussion of the connection between microstructure and mechanical characteristics.https://www.mdpi.com/2304-6740/11/5/187ceramic corundumsol-gel processadditivesstrength
spellingShingle Quanbao Zhao
Zhihong Li
Yumei Zhu
Effect of CaO-TiO<sub>2</sub>-SiO<sub>2</sub> on the Microstructure and Mechanical Properties of Ceramic Corundum Abrasives
Inorganics
ceramic corundum
sol-gel process
additives
strength
title Effect of CaO-TiO<sub>2</sub>-SiO<sub>2</sub> on the Microstructure and Mechanical Properties of Ceramic Corundum Abrasives
title_full Effect of CaO-TiO<sub>2</sub>-SiO<sub>2</sub> on the Microstructure and Mechanical Properties of Ceramic Corundum Abrasives
title_fullStr Effect of CaO-TiO<sub>2</sub>-SiO<sub>2</sub> on the Microstructure and Mechanical Properties of Ceramic Corundum Abrasives
title_full_unstemmed Effect of CaO-TiO<sub>2</sub>-SiO<sub>2</sub> on the Microstructure and Mechanical Properties of Ceramic Corundum Abrasives
title_short Effect of CaO-TiO<sub>2</sub>-SiO<sub>2</sub> on the Microstructure and Mechanical Properties of Ceramic Corundum Abrasives
title_sort effect of cao tio sub 2 sub sio sub 2 sub on the microstructure and mechanical properties of ceramic corundum abrasives
topic ceramic corundum
sol-gel process
additives
strength
url https://www.mdpi.com/2304-6740/11/5/187
work_keys_str_mv AT quanbaozhao effectofcaotiosub2subsiosub2subonthemicrostructureandmechanicalpropertiesofceramiccorundumabrasives
AT zhihongli effectofcaotiosub2subsiosub2subonthemicrostructureandmechanicalpropertiesofceramiccorundumabrasives
AT yumeizhu effectofcaotiosub2subsiosub2subonthemicrostructureandmechanicalpropertiesofceramiccorundumabrasives