Sintesis N-p-Metilbenzil-p-Kumaramida dari Asam p-Kumarat
N-p-Methylbenzyl-p-coumaramide has been synthesized from p-coumaric acid. The purpose of this study was to synthesize N-p-methylbenzyl-p-coumaramide compounds from p-coumaric acid. The N-p-methylbenzyl-p-coumaramide target compound was obtained by direct conversion method using a orthoboric acid cat...
| Main Authors: | , |
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| Format: | Article |
| Language: | English |
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Faculty of Science and Technology Alauddin State Islamic University of Makassar
2017-12-01
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| Series: | Al-Kimia |
| Subjects: | |
| Online Access: | http://journal.uin-alauddin.ac.id/index.php/al-kimia/article/view/3643 |
| Summary: | N-p-Methylbenzyl-p-coumaramide has been synthesized from p-coumaric acid. The purpose of this study was to synthesize N-p-methylbenzyl-p-coumaramide compounds from p-coumaric acid. The N-p-methylbenzyl-p-coumaramide target compound was obtained by direct conversion method using a orthoboric acid catalyst. Target compounds were identified and characterized by melting point, TLC test, FTIR, 1H-NMR, and 13C-NMR spectrometer. The results showed that N-p-methylbenzyl-p-coumaramide compound obtained was white solid (yield 75.83%) with melting point 156-158 oC and TLC (SiO2, n-hexane : chloroform = 5: 3 v/v, Rf = 0.37). |
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| ISSN: | 2302-2736 |