Sintesis N-p-Metilbenzil-p-Kumaramida dari Asam p-Kumarat
N-p-Methylbenzyl-p-coumaramide has been synthesized from p-coumaric acid. The purpose of this study was to synthesize N-p-methylbenzyl-p-coumaramide compounds from p-coumaric acid. The N-p-methylbenzyl-p-coumaramide target compound was obtained by direct conversion method using a orthoboric acid cat...
| Main Authors: | , |
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| Format: | Article |
| Language: | English |
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Faculty of Science and Technology Alauddin State Islamic University of Makassar
2017-12-01
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| Series: | Al-Kimia |
| Subjects: | |
| Online Access: | http://journal.uin-alauddin.ac.id/index.php/al-kimia/article/view/3643 |
| _version_ | 1818570696690761728 |
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| author | Nasriadi Dali Arniah Dali |
| author_facet | Nasriadi Dali Arniah Dali |
| author_sort | Nasriadi Dali |
| collection | DOAJ |
| description | N-p-Methylbenzyl-p-coumaramide has been synthesized from p-coumaric acid. The purpose of this study was to synthesize N-p-methylbenzyl-p-coumaramide compounds from p-coumaric acid. The N-p-methylbenzyl-p-coumaramide target compound was obtained by direct conversion method using a orthoboric acid catalyst. Target compounds were identified and characterized by melting point, TLC test, FTIR, 1H-NMR, and 13C-NMR spectrometer. The results showed that N-p-methylbenzyl-p-coumaramide compound obtained was white solid (yield 75.83%) with melting point 156-158 oC and TLC (SiO2, n-hexane : chloroform = 5: 3 v/v, Rf = 0.37). |
| first_indexed | 2024-12-14T13:45:20Z |
| format | Article |
| id | doaj.art-93b9c01a79be465b85d505c4255f1c6a |
| institution | Directory Open Access Journal |
| issn | 2302-2736 |
| language | English |
| last_indexed | 2024-12-14T13:45:20Z |
| publishDate | 2017-12-01 |
| publisher | Faculty of Science and Technology Alauddin State Islamic University of Makassar |
| record_format | Article |
| series | Al-Kimia |
| spelling | doaj.art-93b9c01a79be465b85d505c4255f1c6a2022-12-21T22:59:20ZengFaculty of Science and Technology Alauddin State Islamic University of MakassarAl-Kimia2302-27362017-12-015215416010.24252/al-kimia.v5i2.36433573Sintesis N-p-Metilbenzil-p-Kumaramida dari Asam p-KumaratNasriadi Dali0Arniah DaliJurusan Kimia, FMIPA, Universitas Halu OleoN-p-Methylbenzyl-p-coumaramide has been synthesized from p-coumaric acid. The purpose of this study was to synthesize N-p-methylbenzyl-p-coumaramide compounds from p-coumaric acid. The N-p-methylbenzyl-p-coumaramide target compound was obtained by direct conversion method using a orthoboric acid catalyst. Target compounds were identified and characterized by melting point, TLC test, FTIR, 1H-NMR, and 13C-NMR spectrometer. The results showed that N-p-methylbenzyl-p-coumaramide compound obtained was white solid (yield 75.83%) with melting point 156-158 oC and TLC (SiO2, n-hexane : chloroform = 5: 3 v/v, Rf = 0.37).http://journal.uin-alauddin.ac.id/index.php/al-kimia/article/view/3643AcylationAmidesAmidationAminesPcoumaric acidAcylationAmidation |
| spellingShingle | Nasriadi Dali Arniah Dali Sintesis N-p-Metilbenzil-p-Kumaramida dari Asam p-Kumarat Al-Kimia Acylation Amides Amidation Amines Pcoumaric acid Acylation Amidation |
| title | Sintesis N-p-Metilbenzil-p-Kumaramida dari Asam p-Kumarat |
| title_full | Sintesis N-p-Metilbenzil-p-Kumaramida dari Asam p-Kumarat |
| title_fullStr | Sintesis N-p-Metilbenzil-p-Kumaramida dari Asam p-Kumarat |
| title_full_unstemmed | Sintesis N-p-Metilbenzil-p-Kumaramida dari Asam p-Kumarat |
| title_short | Sintesis N-p-Metilbenzil-p-Kumaramida dari Asam p-Kumarat |
| title_sort | sintesis n p metilbenzil p kumaramida dari asam p kumarat |
| topic | Acylation Amides Amidation Amines Pcoumaric acid Acylation Amidation |
| url | http://journal.uin-alauddin.ac.id/index.php/al-kimia/article/view/3643 |
| work_keys_str_mv | AT nasriadidali sintesisnpmetilbenzilpkumaramidadariasampkumarat AT arniahdali sintesisnpmetilbenzilpkumaramidadariasampkumarat |