A rapid identification method for adulteration of microcrystalline cellulose

A rapid identification method of microcrystalline cellulose adulteration by near infrared spectroscopy was studied. Based on the near-infrared spectrum data of microcrystalline cellulose samples and adulterants (soluble starch, wheat flour), the material spectrum database and the adulterant spectrum...

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Main Authors: CHEN Xiu-ming, LIANG Hao-xin, HUANG Wei-qiang, XI Xing-lin, LI Shuang, ZHANG Jia-jun
Format: Article
Language:English
Published: Academy of National Food and Strategic Reserves Administration 2023-01-01
Series:Liang you shipin ke-ji
Subjects:
Online Access:http://lyspkj.ijournal.cn/lyspkj/article/abstract/20230124?st=article_issue
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author CHEN Xiu-ming
LIANG Hao-xin
HUANG Wei-qiang
XI Xing-lin
LI Shuang
ZHANG Jia-jun
author_facet CHEN Xiu-ming
LIANG Hao-xin
HUANG Wei-qiang
XI Xing-lin
LI Shuang
ZHANG Jia-jun
author_sort CHEN Xiu-ming
collection DOAJ
description A rapid identification method of microcrystalline cellulose adulteration by near infrared spectroscopy was studied. Based on the near-infrared spectrum data of microcrystalline cellulose samples and adulterants (soluble starch, wheat flour), the material spectrum database and the adulterant spectrum database were created respectively, and the microcrystalline cellulose classification and the adulterant models were also established. A rapid identification method for microcrystalline cellulose adulteration was established by using the Adulterant Screen algorithm technology for calculation and analysis. The minimum detected content of single component adulteration of microcrystalline fiber powder was 2% soluble starch and 1% wheat flour, and the accurate recognition rate was 100%. When the adulteration of two components (soluble starch + wheat flour) was two to ten times of the detection limit concentration of one component, the accurate recognition rate was 100%. The accurate recognition rate of unknown sample microcrystalline cellulose above the detection limit is 100%. The method is simple, rapid and reliable, and can quickly identify adulteration of microcrystalline cellulose samples. It can be effectively applied to the adulteration detection and identification of daily microcrystalline cellulose samples, which could provide technical support for the customs to crack down on tax evasion and evasion.
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spelling doaj.art-93e06e7f5d144989adb2fb744af239992023-02-24T06:44:04ZengAcademy of National Food and Strategic Reserves AdministrationLiang you shipin ke-ji1007-75612023-01-0131118118810.16210/j.cnki.1007-7561.2023.01.023A rapid identification method for adulteration of microcrystalline celluloseCHEN Xiu-ming0LIANG Hao-xin1HUANG Wei-qiang2 XI Xing-lin3LI Shuang4ZHANG Jia-jun5Guangzhou Customs Technology Center, Guangzhou, Guangdong 510623, ChinaGuangzhou Customs Technology Center, Guangzhou, Guangdong 510623, ChinaGuangzhou Customs Technology Center, Guangzhou, Guangdong 510623, ChinaGuangzhou Customs Technology Center, Guangzhou, Guangdong 510623, ChinaGuangzhou Customs Technology Center, Guangzhou, Guangdong 510623, ChinaGuangzhou Customs Technology Center, Guangzhou, Guangdong 510623, ChinaA rapid identification method of microcrystalline cellulose adulteration by near infrared spectroscopy was studied. Based on the near-infrared spectrum data of microcrystalline cellulose samples and adulterants (soluble starch, wheat flour), the material spectrum database and the adulterant spectrum database were created respectively, and the microcrystalline cellulose classification and the adulterant models were also established. A rapid identification method for microcrystalline cellulose adulteration was established by using the Adulterant Screen algorithm technology for calculation and analysis. The minimum detected content of single component adulteration of microcrystalline fiber powder was 2% soluble starch and 1% wheat flour, and the accurate recognition rate was 100%. When the adulteration of two components (soluble starch + wheat flour) was two to ten times of the detection limit concentration of one component, the accurate recognition rate was 100%. The accurate recognition rate of unknown sample microcrystalline cellulose above the detection limit is 100%. The method is simple, rapid and reliable, and can quickly identify adulteration of microcrystalline cellulose samples. It can be effectively applied to the adulteration detection and identification of daily microcrystalline cellulose samples, which could provide technical support for the customs to crack down on tax evasion and evasion.http://lyspkj.ijournal.cn/lyspkj/article/abstract/20230124?st=article_issuemicrocrystalline cellulosethe adulterationrapidlyidentification
spellingShingle CHEN Xiu-ming
LIANG Hao-xin
HUANG Wei-qiang
XI Xing-lin
LI Shuang
ZHANG Jia-jun
A rapid identification method for adulteration of microcrystalline cellulose
Liang you shipin ke-ji
microcrystalline cellulose
the adulteration
rapidly
identification
title A rapid identification method for adulteration of microcrystalline cellulose
title_full A rapid identification method for adulteration of microcrystalline cellulose
title_fullStr A rapid identification method for adulteration of microcrystalline cellulose
title_full_unstemmed A rapid identification method for adulteration of microcrystalline cellulose
title_short A rapid identification method for adulteration of microcrystalline cellulose
title_sort rapid identification method for adulteration of microcrystalline cellulose
topic microcrystalline cellulose
the adulteration
rapidly
identification
url http://lyspkj.ijournal.cn/lyspkj/article/abstract/20230124?st=article_issue
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