An assessment of magnesium AZ31 coronary stents manufacture

AZ31 magnesium coronary stents were studied through a manufacturing process chain involving laser cutting, acid pickling, and dip coating. The purpose of this study was to evaluate surface thickness and geometrical dimensions of stents after processing. Stents were dip coated in a solution using PCL...

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Main Authors: Mariana Nuñez-Nava, Elisa Vazquez, Wendy Ortega-Lara, Ciro A Rodriguez, Erika García-López
Format: Article
Language:English
Published: IOP Publishing 2021-01-01
Series:Materials Research Express
Subjects:
Online Access:https://doi.org/10.1088/2053-1591/ac16f2
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author Mariana Nuñez-Nava
Elisa Vazquez
Wendy Ortega-Lara
Ciro A Rodriguez
Erika García-López
author_facet Mariana Nuñez-Nava
Elisa Vazquez
Wendy Ortega-Lara
Ciro A Rodriguez
Erika García-López
author_sort Mariana Nuñez-Nava
collection DOAJ
description AZ31 magnesium coronary stents were studied through a manufacturing process chain involving laser cutting, acid pickling, and dip coating. The purpose of this study was to evaluate surface thickness and geometrical dimensions of stents after processing. Stents were dip coated in a solution using PCL with 1% of TiO _2 . Additionally, AZ31 coronary stents were dynamically tested using a degradation system based on peristaltic pumps. Our results indicate that coated stents degraded slower than AZ31 uncoated control stents. After 4 weeks of dynamic degradation under flowing Hank’s solution, coated stents lost only ∼9% in weight while uncoated stents lost ∼27% in weight. Stents were qualitatively evaluated after four weeks of degradation. Our results demonstrate the formation of micro-pores after one and two weeks of degradation for coated stents. Lamination was observed after three weeks of degradation, meanwhile, uncoated stents resulted with notches and an irregular surface caused by degradation.
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spelling doaj.art-949aca710e6e4c7f9026a00d538148512023-08-09T15:52:03ZengIOP PublishingMaterials Research Express2053-15912021-01-018707540310.1088/2053-1591/ac16f2An assessment of magnesium AZ31 coronary stents manufactureMariana Nuñez-Nava0Elisa Vazquez1https://orcid.org/0000-0002-1228-9636Wendy Ortega-Lara2Ciro A Rodriguez3https://orcid.org/0000-0003-2289-4239Erika García-López4https://orcid.org/0000-0002-3341-298XTecnologico de Monterrey, Escuela de Ingeniería y Ciencias, Ave. Eugenio Garza Sada 2501 Sur, Monterrey, N.L., 64849, Mexico; Laboratorio Nacional de Manufactura Aditiva y Digital MADiT, Apodaca, Nuevo León, 66628, MexicoTecnologico de Monterrey, Escuela de Ingeniería y Ciencias, Ave. Eugenio Garza Sada 2501 Sur, Monterrey, N.L., 64849, Mexico; Laboratorio Nacional de Manufactura Aditiva y Digital MADiT, Apodaca, Nuevo León, 66628, MexicoTecnologico de Monterrey, Escuela de Ingeniería y Ciencias, Ave. Eugenio Garza Sada 2501 Sur, Monterrey, N.L., 64849, MexicoTecnologico de Monterrey, Escuela de Ingeniería y Ciencias, Ave. Eugenio Garza Sada 2501 Sur, Monterrey, N.L., 64849, Mexico; Laboratorio Nacional de Manufactura Aditiva y Digital MADiT, Apodaca, Nuevo León, 66628, MexicoTecnologico de Monterrey, Escuela de Ingeniería y Ciencias, Ave. Eugenio Garza Sada 2501 Sur, Monterrey, N.L., 64849, Mexico; Laboratorio Nacional de Manufactura Aditiva y Digital MADiT, Apodaca, Nuevo León, 66628, MexicoAZ31 magnesium coronary stents were studied through a manufacturing process chain involving laser cutting, acid pickling, and dip coating. The purpose of this study was to evaluate surface thickness and geometrical dimensions of stents after processing. Stents were dip coated in a solution using PCL with 1% of TiO _2 . Additionally, AZ31 coronary stents were dynamically tested using a degradation system based on peristaltic pumps. Our results indicate that coated stents degraded slower than AZ31 uncoated control stents. After 4 weeks of dynamic degradation under flowing Hank’s solution, coated stents lost only ∼9% in weight while uncoated stents lost ∼27% in weight. Stents were qualitatively evaluated after four weeks of degradation. Our results demonstrate the formation of micro-pores after one and two weeks of degradation for coated stents. Lamination was observed after three weeks of degradation, meanwhile, uncoated stents resulted with notches and an irregular surface caused by degradation.https://doi.org/10.1088/2053-1591/ac16f2AZ31 magnesium alloyPCLdynamic degradationacid picklinglaser cutting
spellingShingle Mariana Nuñez-Nava
Elisa Vazquez
Wendy Ortega-Lara
Ciro A Rodriguez
Erika García-López
An assessment of magnesium AZ31 coronary stents manufacture
Materials Research Express
AZ31 magnesium alloy
PCL
dynamic degradation
acid pickling
laser cutting
title An assessment of magnesium AZ31 coronary stents manufacture
title_full An assessment of magnesium AZ31 coronary stents manufacture
title_fullStr An assessment of magnesium AZ31 coronary stents manufacture
title_full_unstemmed An assessment of magnesium AZ31 coronary stents manufacture
title_short An assessment of magnesium AZ31 coronary stents manufacture
title_sort assessment of magnesium az31 coronary stents manufacture
topic AZ31 magnesium alloy
PCL
dynamic degradation
acid pickling
laser cutting
url https://doi.org/10.1088/2053-1591/ac16f2
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