Microstructure Evolution of Ni-Based ODS Superalloy Powders During Horizontal Rotary Ball Milling

Microstructure evolution of Ni-based oxide dispersion-strengthened alloy powders with milling time is investigated. The elemental powders having a nominal composition of Ni-15Cr-4.5Al-4W-2.5Ti-2Mo-2Ta-0.15Zr-1.1Y2O3 in wt % were ball-milled by using horizontal rotary ball milling with the change of...

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Main Authors: Lee H.-E., Kim Y.Su., Park J.K., Oh S.-T.
Format: Article
Language:English
Published: Polish Academy of Sciences 2017-06-01
Series:Archives of Metallurgy and Materials
Subjects:
Online Access:http://www.degruyter.com/view/j/amm.2017.62.issue-2/amm-2017-0187/amm-2017-0187.xml?format=INT
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author Lee H.-E.
Kim Y.Su.
Park J.K.
Oh S.-T.
author_facet Lee H.-E.
Kim Y.Su.
Park J.K.
Oh S.-T.
author_sort Lee H.-E.
collection DOAJ
description Microstructure evolution of Ni-based oxide dispersion-strengthened alloy powders with milling time is investigated. The elemental powders having a nominal composition of Ni-15Cr-4.5Al-4W-2.5Ti-2Mo-2Ta-0.15Zr-1.1Y2O3 in wt % were ball-milled by using horizontal rotary ball milling with the change of milling velocity. Microstructure observation revealed that large aggregates were formed in the early stages of ball milling, and further milling to 5 h decreased particle size. The average crystalline size, estimated by the peak broadening of XRD, decreased from 28 nm to 15 nm with increasing milling time from 1 h to 5 h. SEM and EPMA analysis showed that the main elements of Ni and Cr were homogeneously distributed inside the powders after ball milling of 5 h.
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spelling doaj.art-95fa97e8a09b4cc0a152a01216d89d162022-12-22T03:46:53ZengPolish Academy of SciencesArchives of Metallurgy and Materials2300-19092017-06-016221253125510.1515/amm-2017-0187amm-2017-0187Microstructure Evolution of Ni-Based ODS Superalloy Powders During Horizontal Rotary Ball MillingLee H.-E.0Kim Y.Su.1Park J.K.2Oh S.-T.3Department of Materials Science and Engineering, Seoul National University of Science and Technology, Seoul01811, Korea (Republic of)Department of Materials Science and Engineering, Seoul National University of Science and Technology, Seoul01811, Korea (Republic of)Korea Sintered Metal Co. Ltd., Daegu42983, Korea (Republic of)Department of Materials Science and Engineering, Seoul National University of Science and Technology, Seoul01811, Korea (Republic of)Microstructure evolution of Ni-based oxide dispersion-strengthened alloy powders with milling time is investigated. The elemental powders having a nominal composition of Ni-15Cr-4.5Al-4W-2.5Ti-2Mo-2Ta-0.15Zr-1.1Y2O3 in wt % were ball-milled by using horizontal rotary ball milling with the change of milling velocity. Microstructure observation revealed that large aggregates were formed in the early stages of ball milling, and further milling to 5 h decreased particle size. The average crystalline size, estimated by the peak broadening of XRD, decreased from 28 nm to 15 nm with increasing milling time from 1 h to 5 h. SEM and EPMA analysis showed that the main elements of Ni and Cr were homogeneously distributed inside the powders after ball milling of 5 h.http://www.degruyter.com/view/j/amm.2017.62.issue-2/amm-2017-0187/amm-2017-0187.xml?format=INTNi-base ODS superalloyHigh energy ball millingParticle and crystalline sizeMicrostructure
spellingShingle Lee H.-E.
Kim Y.Su.
Park J.K.
Oh S.-T.
Microstructure Evolution of Ni-Based ODS Superalloy Powders During Horizontal Rotary Ball Milling
Archives of Metallurgy and Materials
Ni-base ODS superalloy
High energy ball milling
Particle and crystalline size
Microstructure
title Microstructure Evolution of Ni-Based ODS Superalloy Powders During Horizontal Rotary Ball Milling
title_full Microstructure Evolution of Ni-Based ODS Superalloy Powders During Horizontal Rotary Ball Milling
title_fullStr Microstructure Evolution of Ni-Based ODS Superalloy Powders During Horizontal Rotary Ball Milling
title_full_unstemmed Microstructure Evolution of Ni-Based ODS Superalloy Powders During Horizontal Rotary Ball Milling
title_short Microstructure Evolution of Ni-Based ODS Superalloy Powders During Horizontal Rotary Ball Milling
title_sort microstructure evolution of ni based ods superalloy powders during horizontal rotary ball milling
topic Ni-base ODS superalloy
High energy ball milling
Particle and crystalline size
Microstructure
url http://www.degruyter.com/view/j/amm.2017.62.issue-2/amm-2017-0187/amm-2017-0187.xml?format=INT
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