Effect of cobalt production method on properties of its nanopowders

The relevance of work is caused by the necessity to produce industrially cobalt nanopowders with specified properties. The aim of the research: to obtain cobalt nanopowder by plasmachemical synthesis, sol-gel and infrared pyrolysis methods; to determine and to compare their characteristics. Research...

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Main Authors: Ella Dzidziguri, Galina Karpacheva, Nikolai Perov, Andrey Samokhin, Nadezhda Shatrova
Format: Article
Language:Russian
Published: Tomsk Polytechnic University 2019-05-01
Series:Известия Томского политехнического университета: Инжиниринг георесурсов
Subjects:
Online Access:http://izvestiya-tpu.ru/archive/article/view/1322
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author Ella Dzidziguri
Galina Karpacheva
Nikolai Perov
Andrey Samokhin
Nadezhda Shatrova
author_facet Ella Dzidziguri
Galina Karpacheva
Nikolai Perov
Andrey Samokhin
Nadezhda Shatrova
author_sort Ella Dzidziguri
collection DOAJ
description The relevance of work is caused by the necessity to produce industrially cobalt nanopowders with specified properties. The aim of the research: to obtain cobalt nanopowder by plasmachemical synthesis, sol-gel and infrared pyrolysis methods; to determine and to compare their characteristics. Research methods: the X-ray phase qualitative and quantitative analysis, the average size calculation of coherent-scattering region and coherent-scattering region distribution by the sizes, the transmission and scanning electronic microscopy, the electron diffraction analysis, the calculation of the average size of particles with software, the method of low-temperature nitrogen adsorption, the mass spectrometry, the vibration magnetometry. The results: The authors have studied phase qualitative and quantitative compositions, disperse characteristics, morphology, magnetic properties of cobalt nanopowders obtained by three methods and have determined dimensional dependences of coercive force. It was ascertained that the nanopowders have similar morphology, but various qualitative and quantitative compositions, disperse characteristics and magnetic properties. It is impossible to interchange these materials technologically.
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spelling doaj.art-96c7c0794fee4bf8b625769a816b146b2023-06-03T21:08:52ZrusTomsk Polytechnic UniversityИзвестия Томского политехнического университета: Инжиниринг георесурсов2500-10192413-18302019-05-013243Effect of cobalt production method on properties of its nanopowdersElla DzidziguriGalina KarpachevaNikolai PerovAndrey SamokhinNadezhda ShatrovaThe relevance of work is caused by the necessity to produce industrially cobalt nanopowders with specified properties. The aim of the research: to obtain cobalt nanopowder by plasmachemical synthesis, sol-gel and infrared pyrolysis methods; to determine and to compare their characteristics. Research methods: the X-ray phase qualitative and quantitative analysis, the average size calculation of coherent-scattering region and coherent-scattering region distribution by the sizes, the transmission and scanning electronic microscopy, the electron diffraction analysis, the calculation of the average size of particles with software, the method of low-temperature nitrogen adsorption, the mass spectrometry, the vibration magnetometry. The results: The authors have studied phase qualitative and quantitative compositions, disperse characteristics, morphology, magnetic properties of cobalt nanopowders obtained by three methods and have determined dimensional dependences of coercive force. It was ascertained that the nanopowders have similar morphology, but various qualitative and quantitative compositions, disperse characteristics and magnetic properties. It is impossible to interchange these materials technologically.http://izvestiya-tpu.ru/archive/article/view/1322nanopowdersphase compositionmorphologydispersionmagnetic properties
spellingShingle Ella Dzidziguri
Galina Karpacheva
Nikolai Perov
Andrey Samokhin
Nadezhda Shatrova
Effect of cobalt production method on properties of its nanopowders
Известия Томского политехнического университета: Инжиниринг георесурсов
nanopowders
phase composition
morphology
dispersion
magnetic properties
title Effect of cobalt production method on properties of its nanopowders
title_full Effect of cobalt production method on properties of its nanopowders
title_fullStr Effect of cobalt production method on properties of its nanopowders
title_full_unstemmed Effect of cobalt production method on properties of its nanopowders
title_short Effect of cobalt production method on properties of its nanopowders
title_sort effect of cobalt production method on properties of its nanopowders
topic nanopowders
phase composition
morphology
dispersion
magnetic properties
url http://izvestiya-tpu.ru/archive/article/view/1322
work_keys_str_mv AT elladzidziguri effectofcobaltproductionmethodonpropertiesofitsnanopowders
AT galinakarpacheva effectofcobaltproductionmethodonpropertiesofitsnanopowders
AT nikolaiperov effectofcobaltproductionmethodonpropertiesofitsnanopowders
AT andreysamokhin effectofcobaltproductionmethodonpropertiesofitsnanopowders
AT nadezhdashatrova effectofcobaltproductionmethodonpropertiesofitsnanopowders