Facile One-Step Synthesis of PVDF Bead-on-String Fibers by Pressurized Gyration for Reusable Face Masks

Single-use face masks pose a threat to the environment and are not cost-effective, which prompts the need for developing reusable masks. In this study, pressurized gyration (PG) successfully produced bead-on-string polyvinylidene fluoride (PVDF) fibers with fiber diameters ranging from 2.3 μm to 26....

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Main Authors: Ruiran Huang, Yanqi Dai, Jubair Ahmed, Mohan Edirisinghe
Format: Article
Language:English
Published: MDPI AG 2022-10-01
Series:Polymers
Subjects:
Online Access:https://www.mdpi.com/2073-4360/14/21/4498
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author Ruiran Huang
Yanqi Dai
Jubair Ahmed
Mohan Edirisinghe
author_facet Ruiran Huang
Yanqi Dai
Jubair Ahmed
Mohan Edirisinghe
author_sort Ruiran Huang
collection DOAJ
description Single-use face masks pose a threat to the environment and are not cost-effective, which prompts the need for developing reusable masks. In this study, pressurized gyration (PG) successfully produced bead-on-string polyvinylidene fluoride (PVDF) fibers with fiber diameters ranging from 2.3 μm to 26.1 μm, and bead diameters ranging from 60.9 μm to 88.5 μm by changing the solution parameters. The effect of the solution parameters on the crystalline phase was studied by Fourier-transform infrared spectroscopy (FT-IR), where the β-phase contents of PG PVDF fibers reached over 75%. The fiber morphology and β-phase contents of PG PVDF fibers indicated the potential mechanical and electrostatic filtration efficiency of PG PVDF fibers, respectively. Additionally, the hydrophobicity was investigated by static water contact angle tests, and the PVDF fibers showed superior hydrophobicity properties (all samples above 125°) over commercial polypropylene (PP) single-use masks (approximately 107°). This study supports the notion that the PG PVDF fiber mats are a promising candidate for future reusable face masks.
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spelling doaj.art-96e36283dca34f2b843a716d438f39922023-11-24T06:27:15ZengMDPI AGPolymers2073-43602022-10-011421449810.3390/polym14214498Facile One-Step Synthesis of PVDF Bead-on-String Fibers by Pressurized Gyration for Reusable Face MasksRuiran Huang0Yanqi Dai1Jubair Ahmed2Mohan Edirisinghe3Department of Mechanical Engineering, University College London, Torrington Place, London WC1E 7JE, UKDepartment of Mechanical Engineering, University College London, Torrington Place, London WC1E 7JE, UKDepartment of Mechanical Engineering, University College London, Torrington Place, London WC1E 7JE, UKDepartment of Mechanical Engineering, University College London, Torrington Place, London WC1E 7JE, UKSingle-use face masks pose a threat to the environment and are not cost-effective, which prompts the need for developing reusable masks. In this study, pressurized gyration (PG) successfully produced bead-on-string polyvinylidene fluoride (PVDF) fibers with fiber diameters ranging from 2.3 μm to 26.1 μm, and bead diameters ranging from 60.9 μm to 88.5 μm by changing the solution parameters. The effect of the solution parameters on the crystalline phase was studied by Fourier-transform infrared spectroscopy (FT-IR), where the β-phase contents of PG PVDF fibers reached over 75%. The fiber morphology and β-phase contents of PG PVDF fibers indicated the potential mechanical and electrostatic filtration efficiency of PG PVDF fibers, respectively. Additionally, the hydrophobicity was investigated by static water contact angle tests, and the PVDF fibers showed superior hydrophobicity properties (all samples above 125°) over commercial polypropylene (PP) single-use masks (approximately 107°). This study supports the notion that the PG PVDF fiber mats are a promising candidate for future reusable face masks.https://www.mdpi.com/2073-4360/14/21/4498pressurized gyrationpolyvinylidene fluoride (PVDF)bead-on-string fiberfiber morphologyβ-phasehydrophobicity
spellingShingle Ruiran Huang
Yanqi Dai
Jubair Ahmed
Mohan Edirisinghe
Facile One-Step Synthesis of PVDF Bead-on-String Fibers by Pressurized Gyration for Reusable Face Masks
Polymers
pressurized gyration
polyvinylidene fluoride (PVDF)
bead-on-string fiber
fiber morphology
β-phase
hydrophobicity
title Facile One-Step Synthesis of PVDF Bead-on-String Fibers by Pressurized Gyration for Reusable Face Masks
title_full Facile One-Step Synthesis of PVDF Bead-on-String Fibers by Pressurized Gyration for Reusable Face Masks
title_fullStr Facile One-Step Synthesis of PVDF Bead-on-String Fibers by Pressurized Gyration for Reusable Face Masks
title_full_unstemmed Facile One-Step Synthesis of PVDF Bead-on-String Fibers by Pressurized Gyration for Reusable Face Masks
title_short Facile One-Step Synthesis of PVDF Bead-on-String Fibers by Pressurized Gyration for Reusable Face Masks
title_sort facile one step synthesis of pvdf bead on string fibers by pressurized gyration for reusable face masks
topic pressurized gyration
polyvinylidene fluoride (PVDF)
bead-on-string fiber
fiber morphology
β-phase
hydrophobicity
url https://www.mdpi.com/2073-4360/14/21/4498
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AT jubairahmed facileonestepsynthesisofpvdfbeadonstringfibersbypressurizedgyrationforreusablefacemasks
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