Study on Synthesis and Modification of Conical Ni Structures by One-Step Method
In this work the conical Ni structures were obtained from an electrolyte containing NH4Cl as a crystal modifier. This process is called one-step method and allows to cover large areas with micro- and nanostructures during a single electrodeposition. Presence of NH4Cl promotes a vertical direction of...
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Polish Academy of Sciences
2021-09-01
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Series: | Archives of Metallurgy and Materials |
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Online Access: | https://journals.pan.pl/Content/119264/PDF/AMM-2021-3-33-Skibinska.pdf |
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author | K. Skibińska S. Semeniuk D. Kutyła K. Kołczyk-Siedlecka A. Jędraczka P. Żabiński |
author_facet | K. Skibińska S. Semeniuk D. Kutyła K. Kołczyk-Siedlecka A. Jędraczka P. Żabiński |
author_sort | K. Skibińska |
collection | DOAJ |
description | In this work the conical Ni structures were obtained from an electrolyte containing NH4Cl as a crystal modifier. This process is called one-step method and allows to cover large areas with micro- and nanostructures during a single electrodeposition. Presence of NH4Cl promotes a vertical direction of structure growth in order to block a horizontal one. Additionally, this method does not require using chromic acid solution, which is dangerous for the environment. Due to the ferromagnetic properties of Ni, obtained coatings could be applied as magnetic devices. The influence of the parameters such as a preparation of copper substrate, a composition of electrolyte and electrodeposition conditions (time, the electrolyte temperature and current density) was investigated in this work. |
first_indexed | 2024-04-11T21:37:40Z |
format | Article |
id | doaj.art-9854272ec4f04c58b8ddcb13eef4cc7a |
institution | Directory Open Access Journal |
issn | 2300-1909 |
language | English |
last_indexed | 2024-04-11T21:37:40Z |
publishDate | 2021-09-01 |
publisher | Polish Academy of Sciences |
record_format | Article |
series | Archives of Metallurgy and Materials |
spelling | doaj.art-9854272ec4f04c58b8ddcb13eef4cc7a2022-12-22T04:01:42ZengPolish Academy of SciencesArchives of Metallurgy and Materials2300-19092021-09-01vol. 66No 3861869https://doi.org/10.24425/amm.2021.136391Study on Synthesis and Modification of Conical Ni Structures by One-Step MethodK. Skibińska0https://orcid.org/0000-0002-0332-7725S. Semeniuk1D. Kutyła2https://orcid.org/0000-0002-6482-0740K. Kołczyk-Siedlecka3https://orcid.org/0000-0002-8391-4603A. Jędraczka4https://orcid.org/0000-0001-5792-2063P. Żabiński5https://orcid.org/0000-0002-5085-2645AGH University of Science and Technology, Faculty of Non-Ferrous Metals, Al. Mickiewicza 30, 30-059, Krakow, PolandAGH University of Science and Technology, Faculty of Non-Ferrous Metals, Al. Mickiewicza 30, 30-059, Krakow, PolandAGH University of Science and Technology, Faculty of Non-Ferrous Metals, Al. Mickiewicza 30, 30-059, Krakow, PolandAGH University of Science and Technology, Faculty of Non-Ferrous Metals, Al. Mickiewicza 30, 30-059, Krakow, PolandAGH University of Science and Technology, Faculty of Non-Ferrous Metals, Al. Mickiewicza 30, 30-059, Krakow, PolandAGH University of Science and Technology, Faculty of Non-Ferrous Metals, Al. Mickiewicza 30, 30-059, Krakow, PolandIn this work the conical Ni structures were obtained from an electrolyte containing NH4Cl as a crystal modifier. This process is called one-step method and allows to cover large areas with micro- and nanostructures during a single electrodeposition. Presence of NH4Cl promotes a vertical direction of structure growth in order to block a horizontal one. Additionally, this method does not require using chromic acid solution, which is dangerous for the environment. Due to the ferromagnetic properties of Ni, obtained coatings could be applied as magnetic devices. The influence of the parameters such as a preparation of copper substrate, a composition of electrolyte and electrodeposition conditions (time, the electrolyte temperature and current density) was investigated in this work.https://journals.pan.pl/Content/119264/PDF/AMM-2021-3-33-Skibinska.pdfelectrodepositionone-step methodcrystal modifiernickel conesfree-standing structures |
spellingShingle | K. Skibińska S. Semeniuk D. Kutyła K. Kołczyk-Siedlecka A. Jędraczka P. Żabiński Study on Synthesis and Modification of Conical Ni Structures by One-Step Method Archives of Metallurgy and Materials electrodeposition one-step method crystal modifier nickel cones free-standing structures |
title | Study on Synthesis and Modification of Conical Ni Structures by One-Step Method |
title_full | Study on Synthesis and Modification of Conical Ni Structures by One-Step Method |
title_fullStr | Study on Synthesis and Modification of Conical Ni Structures by One-Step Method |
title_full_unstemmed | Study on Synthesis and Modification of Conical Ni Structures by One-Step Method |
title_short | Study on Synthesis and Modification of Conical Ni Structures by One-Step Method |
title_sort | study on synthesis and modification of conical ni structures by one step method |
topic | electrodeposition one-step method crystal modifier nickel cones free-standing structures |
url | https://journals.pan.pl/Content/119264/PDF/AMM-2021-3-33-Skibinska.pdf |
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