Study on Synthesis and Modification of Conical Ni Structures by One-Step Method

In this work the conical Ni structures were obtained from an electrolyte containing NH4Cl as a crystal modifier. This process is called one-step method and allows to cover large areas with micro- and nanostructures during a single electrodeposition. Presence of NH4Cl promotes a vertical direction of...

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Main Authors: K. Skibińska, S. Semeniuk, D. Kutyła, K. Kołczyk-Siedlecka, A. Jędraczka, P. Żabiński
Format: Article
Language:English
Published: Polish Academy of Sciences 2021-09-01
Series:Archives of Metallurgy and Materials
Subjects:
Online Access:https://journals.pan.pl/Content/119264/PDF/AMM-2021-3-33-Skibinska.pdf
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author K. Skibińska
S. Semeniuk
D. Kutyła
K. Kołczyk-Siedlecka
A. Jędraczka
P. Żabiński
author_facet K. Skibińska
S. Semeniuk
D. Kutyła
K. Kołczyk-Siedlecka
A. Jędraczka
P. Żabiński
author_sort K. Skibińska
collection DOAJ
description In this work the conical Ni structures were obtained from an electrolyte containing NH4Cl as a crystal modifier. This process is called one-step method and allows to cover large areas with micro- and nanostructures during a single electrodeposition. Presence of NH4Cl promotes a vertical direction of structure growth in order to block a horizontal one. Additionally, this method does not require using chromic acid solution, which is dangerous for the environment. Due to the ferromagnetic properties of Ni, obtained coatings could be applied as magnetic devices. The influence of the parameters such as a preparation of copper substrate, a composition of electrolyte and electrodeposition conditions (time, the electrolyte temperature and current density) was investigated in this work.
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spelling doaj.art-9854272ec4f04c58b8ddcb13eef4cc7a2022-12-22T04:01:42ZengPolish Academy of SciencesArchives of Metallurgy and Materials2300-19092021-09-01vol. 66No 3861869https://doi.org/10.24425/amm.2021.136391Study on Synthesis and Modification of Conical Ni Structures by One-Step MethodK. Skibińska0https://orcid.org/0000-0002-0332-7725S. Semeniuk1D. Kutyła2https://orcid.org/0000-0002-6482-0740K. Kołczyk-Siedlecka3https://orcid.org/0000-0002-8391-4603A. Jędraczka4https://orcid.org/0000-0001-5792-2063P. Żabiński5https://orcid.org/0000-0002-5085-2645AGH University of Science and Technology, Faculty of Non-Ferrous Metals, Al. Mickiewicza 30, 30-059, Krakow, PolandAGH University of Science and Technology, Faculty of Non-Ferrous Metals, Al. Mickiewicza 30, 30-059, Krakow, PolandAGH University of Science and Technology, Faculty of Non-Ferrous Metals, Al. Mickiewicza 30, 30-059, Krakow, PolandAGH University of Science and Technology, Faculty of Non-Ferrous Metals, Al. Mickiewicza 30, 30-059, Krakow, PolandAGH University of Science and Technology, Faculty of Non-Ferrous Metals, Al. Mickiewicza 30, 30-059, Krakow, PolandAGH University of Science and Technology, Faculty of Non-Ferrous Metals, Al. Mickiewicza 30, 30-059, Krakow, PolandIn this work the conical Ni structures were obtained from an electrolyte containing NH4Cl as a crystal modifier. This process is called one-step method and allows to cover large areas with micro- and nanostructures during a single electrodeposition. Presence of NH4Cl promotes a vertical direction of structure growth in order to block a horizontal one. Additionally, this method does not require using chromic acid solution, which is dangerous for the environment. Due to the ferromagnetic properties of Ni, obtained coatings could be applied as magnetic devices. The influence of the parameters such as a preparation of copper substrate, a composition of electrolyte and electrodeposition conditions (time, the electrolyte temperature and current density) was investigated in this work.https://journals.pan.pl/Content/119264/PDF/AMM-2021-3-33-Skibinska.pdfelectrodepositionone-step methodcrystal modifiernickel conesfree-standing structures
spellingShingle K. Skibińska
S. Semeniuk
D. Kutyła
K. Kołczyk-Siedlecka
A. Jędraczka
P. Żabiński
Study on Synthesis and Modification of Conical Ni Structures by One-Step Method
Archives of Metallurgy and Materials
electrodeposition
one-step method
crystal modifier
nickel cones
free-standing structures
title Study on Synthesis and Modification of Conical Ni Structures by One-Step Method
title_full Study on Synthesis and Modification of Conical Ni Structures by One-Step Method
title_fullStr Study on Synthesis and Modification of Conical Ni Structures by One-Step Method
title_full_unstemmed Study on Synthesis and Modification of Conical Ni Structures by One-Step Method
title_short Study on Synthesis and Modification of Conical Ni Structures by One-Step Method
title_sort study on synthesis and modification of conical ni structures by one step method
topic electrodeposition
one-step method
crystal modifier
nickel cones
free-standing structures
url https://journals.pan.pl/Content/119264/PDF/AMM-2021-3-33-Skibinska.pdf
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AT kkołczyksiedlecka studyonsynthesisandmodificationofconicalnistructuresbyonestepmethod
AT ajedraczka studyonsynthesisandmodificationofconicalnistructuresbyonestepmethod
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