Corn Starch-Chitosan Nanocomposite Film Containing Nettle Essential Oil Nanoemulsions and Starch Nanocrystals: Optimization and Characterization
In the current study, nanocomposite films were produced based on corn starch:chitosan (CS:CH) biopolymers and the films were reinforced with nettle essential oil nanoemulsions (NEONEs) and starch nanocrystals (SNCs) to improve their physicochemical and mechanical properties. CS: CH at 70:30, 50:50,...
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MDPI AG
2021-06-01
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author | Fatemeh Kalateh-Seifari Shima Yousefi Hamed Ahari Seyed Hedayat Hosseini |
author_facet | Fatemeh Kalateh-Seifari Shima Yousefi Hamed Ahari Seyed Hedayat Hosseini |
author_sort | Fatemeh Kalateh-Seifari |
collection | DOAJ |
description | In the current study, nanocomposite films were produced based on corn starch:chitosan (CS:CH) biopolymers and the films were reinforced with nettle essential oil nanoemulsions (NEONEs) and starch nanocrystals (SNCs) to improve their physicochemical and mechanical properties. CS: CH at 70:30, 50:50, and 30:70 (<i>w</i>/<i>w</i>) ratios; SNCs at 2, 4, and 6% (<i>w</i>/<i>w</i>), and NEONEs at 0.5, 1, and 1.5% (<i>w</i>/<i>w</i>) were selected as variables. Then the various physical and mechanical attributes of chitosan-starch blended film containing SNCs and NEONEs were optimized using response surface methodology. The desirability function technique for the second-order polynomial models revealed that the following results could be achieved as the optimized treatment: water solubility of 51.56%; water absorption capacity of 128.75%; surface color of L (89.60), a (0.96), and b (1.90); water vapor permeability of 0.335 g/s Pa m, oxygen permeability of 2.60 cm<sup>3</sup> μm/m<sup>2</sup> d kPa; thickness of 154.41 µm, elongation at break of 53.54%; and tensile strength of 0.20 MPa at CS:CH of 38:62, SNC of 6.0%, and NEONEs of 0.41%. The nanocomposite film obtained can be employed as a novel biofunctional film with boosted physical mechanical and physical characteristics for food packaging applications. |
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series | Polymers |
spelling | doaj.art-993a6020e8744d0a8941ed1c7ca46ba12023-11-22T01:58:24ZengMDPI AGPolymers2073-43602021-06-011313211310.3390/polym13132113Corn Starch-Chitosan Nanocomposite Film Containing Nettle Essential Oil Nanoemulsions and Starch Nanocrystals: Optimization and CharacterizationFatemeh Kalateh-Seifari0Shima Yousefi1Hamed Ahari2Seyed Hedayat Hosseini3Department of Agriculture and Food Science, Science and Research Branch, Islamic Azad University, Tehran 476714171, IranDepartment of Agriculture and Food Science, Science and Research Branch, Islamic Azad University, Tehran 476714171, IranDepartment of Agriculture and Food Science, Science and Research Branch, Islamic Azad University, Tehran 476714171, IranDepartment of Food Science and Technology, Shahid Beheshti University of Medical Science, Tehran 1983969411, IranIn the current study, nanocomposite films were produced based on corn starch:chitosan (CS:CH) biopolymers and the films were reinforced with nettle essential oil nanoemulsions (NEONEs) and starch nanocrystals (SNCs) to improve their physicochemical and mechanical properties. CS: CH at 70:30, 50:50, and 30:70 (<i>w</i>/<i>w</i>) ratios; SNCs at 2, 4, and 6% (<i>w</i>/<i>w</i>), and NEONEs at 0.5, 1, and 1.5% (<i>w</i>/<i>w</i>) were selected as variables. Then the various physical and mechanical attributes of chitosan-starch blended film containing SNCs and NEONEs were optimized using response surface methodology. The desirability function technique for the second-order polynomial models revealed that the following results could be achieved as the optimized treatment: water solubility of 51.56%; water absorption capacity of 128.75%; surface color of L (89.60), a (0.96), and b (1.90); water vapor permeability of 0.335 g/s Pa m, oxygen permeability of 2.60 cm<sup>3</sup> μm/m<sup>2</sup> d kPa; thickness of 154.41 µm, elongation at break of 53.54%; and tensile strength of 0.20 MPa at CS:CH of 38:62, SNC of 6.0%, and NEONEs of 0.41%. The nanocomposite film obtained can be employed as a novel biofunctional film with boosted physical mechanical and physical characteristics for food packaging applications.https://www.mdpi.com/2073-4360/13/13/2113chitosan-starch compositenettle essential oilstarch nanocrystalsoptimization |
spellingShingle | Fatemeh Kalateh-Seifari Shima Yousefi Hamed Ahari Seyed Hedayat Hosseini Corn Starch-Chitosan Nanocomposite Film Containing Nettle Essential Oil Nanoemulsions and Starch Nanocrystals: Optimization and Characterization Polymers chitosan-starch composite nettle essential oil starch nanocrystals optimization |
title | Corn Starch-Chitosan Nanocomposite Film Containing Nettle Essential Oil Nanoemulsions and Starch Nanocrystals: Optimization and Characterization |
title_full | Corn Starch-Chitosan Nanocomposite Film Containing Nettle Essential Oil Nanoemulsions and Starch Nanocrystals: Optimization and Characterization |
title_fullStr | Corn Starch-Chitosan Nanocomposite Film Containing Nettle Essential Oil Nanoemulsions and Starch Nanocrystals: Optimization and Characterization |
title_full_unstemmed | Corn Starch-Chitosan Nanocomposite Film Containing Nettle Essential Oil Nanoemulsions and Starch Nanocrystals: Optimization and Characterization |
title_short | Corn Starch-Chitosan Nanocomposite Film Containing Nettle Essential Oil Nanoemulsions and Starch Nanocrystals: Optimization and Characterization |
title_sort | corn starch chitosan nanocomposite film containing nettle essential oil nanoemulsions and starch nanocrystals optimization and characterization |
topic | chitosan-starch composite nettle essential oil starch nanocrystals optimization |
url | https://www.mdpi.com/2073-4360/13/13/2113 |
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