Microstructure and properties of C/C composites brazed with Ni-Cr-P pasty filler metal

The Ni-Cr-P metal powder was prepared by vacuum melting and inert gas atomization method, and then an organic binder was added and stirred at high speed to prepare a Ni14Cr10P paste-like filler metal. The prepared pasty filler metal was used to braze the C/C composites in a vacuum furnace. Then the...

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Main Authors: YI Zhen-hua, RAN Li-ping, YI Mao-zhong
Format: Article
Language:zho
Published: Journal of Materials Engineering 2020-05-01
Series:Cailiao gongcheng
Subjects:
Online Access:http://jme.biam.ac.cn/CN/Y2020/V48/I5/127
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author YI Zhen-hua
RAN Li-ping
YI Mao-zhong
author_facet YI Zhen-hua
RAN Li-ping
YI Mao-zhong
author_sort YI Zhen-hua
collection DOAJ
description The Ni-Cr-P metal powder was prepared by vacuum melting and inert gas atomization method, and then an organic binder was added and stirred at high speed to prepare a Ni14Cr10P paste-like filler metal. The prepared pasty filler metal was used to braze the C/C composites in a vacuum furnace. Then the shear strength of the brazed joint was tested. The interface structure of the brazed joint was analyzed by OM, SEM, EDS and XRD. The results show that the shear strength of the joint obtained at the brazing temperature of 1000℃ and the holding time of 0.5 h reaches 28.6 MPa, and then the strength of the brazed joint is decreased with the increase of the brazing temperature or the holding time. It is found that the contact area between the brazing layer and the surface of the C/C composites is increased by the pasty brazing filler metal, which is favorable for blocking the pores on the surface of the C/C composites. A staggered distribution of Cr carbide phase buffer layer is formed at the interface, so that the interface exhibits a structure with an increased thermal expansion coefficient gradient, which helps to alleviate the thermal mismatch and improve the strength of the brazed joint.
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spelling doaj.art-994f870a76f44392abead52af4ec766f2023-01-03T06:24:15ZzhoJournal of Materials EngineeringCailiao gongcheng1001-43811001-43812020-05-0148512713510.11868/j.issn.1001-4381.2019.00019520200417Microstructure and properties of C/C composites brazed with Ni-Cr-P pasty filler metalYI Zhen-hua0RAN Li-ping1YI Mao-zhong2State Key Laboratory for Powder Metallurgy, Institute of Powder Metallurgy, Central South University, Changsha 410083, ChinaState Key Laboratory for Powder Metallurgy, Institute of Powder Metallurgy, Central South University, Changsha 410083, ChinaState Key Laboratory for Powder Metallurgy, Institute of Powder Metallurgy, Central South University, Changsha 410083, ChinaThe Ni-Cr-P metal powder was prepared by vacuum melting and inert gas atomization method, and then an organic binder was added and stirred at high speed to prepare a Ni14Cr10P paste-like filler metal. The prepared pasty filler metal was used to braze the C/C composites in a vacuum furnace. Then the shear strength of the brazed joint was tested. The interface structure of the brazed joint was analyzed by OM, SEM, EDS and XRD. The results show that the shear strength of the joint obtained at the brazing temperature of 1000℃ and the holding time of 0.5 h reaches 28.6 MPa, and then the strength of the brazed joint is decreased with the increase of the brazing temperature or the holding time. It is found that the contact area between the brazing layer and the surface of the C/C composites is increased by the pasty brazing filler metal, which is favorable for blocking the pores on the surface of the C/C composites. A staggered distribution of Cr carbide phase buffer layer is formed at the interface, so that the interface exhibits a structure with an increased thermal expansion coefficient gradient, which helps to alleviate the thermal mismatch and improve the strength of the brazed joint.http://jme.biam.ac.cn/CN/Y2020/V48/I5/127active brazing fillerpasty fillerc/c composites brazingshear strengthinterface stru-cture
spellingShingle YI Zhen-hua
RAN Li-ping
YI Mao-zhong
Microstructure and properties of C/C composites brazed with Ni-Cr-P pasty filler metal
Cailiao gongcheng
active brazing filler
pasty filler
c/c composites brazing
shear strength
interface stru-cture
title Microstructure and properties of C/C composites brazed with Ni-Cr-P pasty filler metal
title_full Microstructure and properties of C/C composites brazed with Ni-Cr-P pasty filler metal
title_fullStr Microstructure and properties of C/C composites brazed with Ni-Cr-P pasty filler metal
title_full_unstemmed Microstructure and properties of C/C composites brazed with Ni-Cr-P pasty filler metal
title_short Microstructure and properties of C/C composites brazed with Ni-Cr-P pasty filler metal
title_sort microstructure and properties of c c composites brazed with ni cr p pasty filler metal
topic active brazing filler
pasty filler
c/c composites brazing
shear strength
interface stru-cture
url http://jme.biam.ac.cn/CN/Y2020/V48/I5/127
work_keys_str_mv AT yizhenhua microstructureandpropertiesofcccompositesbrazedwithnicrppastyfillermetal
AT ranliping microstructureandpropertiesofcccompositesbrazedwithnicrppastyfillermetal
AT yimaozhong microstructureandpropertiesofcccompositesbrazedwithnicrppastyfillermetal