Cooling Rate Controlled Aging of a Co-Free Fe-Ni-Cr-Mo-Ti-Al Maraging Steel

Maraging steels are high-strength steels that are hardened by the formation of precipitates during an isothermal aging heat treatment. Depending on the aging temperature and time the cooling rate after holding can play a significant factor on the development of the microstructure and mechanical prop...

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Main Authors: Stefan Zeisl, Ronald Schnitzer
Format: Article
Language:English
Published: MDPI AG 2022-03-01
Series:Metals
Subjects:
Online Access:https://www.mdpi.com/2075-4701/12/4/538
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author Stefan Zeisl
Ronald Schnitzer
author_facet Stefan Zeisl
Ronald Schnitzer
author_sort Stefan Zeisl
collection DOAJ
description Maraging steels are high-strength steels that are hardened by the formation of precipitates during an isothermal aging heat treatment. Depending on the aging temperature and time the cooling rate after holding can play a significant factor on the development of the microstructure and mechanical properties. This study seeks to show how the cooling time influences the precipitation hardening effect, austenite reversion and the development of hardness and impact toughness. The material was aged at a constant temperature using holding times of 0 h, 4 h and 15 h and cooled with different cooling rates resulting in cooling times of 7 h, 28 h and 56 h. The microstructure was characterized using a combination of electron backscatter diffraction, X-ray diffraction and atom probe tomography with cluster-based precipitate analysis. It is shown that the effect of the cooling time is strongly dependent on the holding time and that a longer cooling time can improve hardness and impact toughness.
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spelling doaj.art-997cf90dd35042fd9a118ac4ff45b17f2023-12-03T13:42:03ZengMDPI AGMetals2075-47012022-03-0112453810.3390/met12040538Cooling Rate Controlled Aging of a Co-Free Fe-Ni-Cr-Mo-Ti-Al Maraging SteelStefan Zeisl0Ronald Schnitzer1Department of Materials Science, Montanuniversität Leoben, Franz-Josef Straße 18, 8700 Leoben, AustriaDepartment of Materials Science, Montanuniversität Leoben, Franz-Josef Straße 18, 8700 Leoben, AustriaMaraging steels are high-strength steels that are hardened by the formation of precipitates during an isothermal aging heat treatment. Depending on the aging temperature and time the cooling rate after holding can play a significant factor on the development of the microstructure and mechanical properties. This study seeks to show how the cooling time influences the precipitation hardening effect, austenite reversion and the development of hardness and impact toughness. The material was aged at a constant temperature using holding times of 0 h, 4 h and 15 h and cooled with different cooling rates resulting in cooling times of 7 h, 28 h and 56 h. The microstructure was characterized using a combination of electron backscatter diffraction, X-ray diffraction and atom probe tomography with cluster-based precipitate analysis. It is shown that the effect of the cooling time is strongly dependent on the holding time and that a longer cooling time can improve hardness and impact toughness.https://www.mdpi.com/2075-4701/12/4/538maraging steelsatom probe tomographyheat treatment studyX-ray diffractionintermetallic precipitates
spellingShingle Stefan Zeisl
Ronald Schnitzer
Cooling Rate Controlled Aging of a Co-Free Fe-Ni-Cr-Mo-Ti-Al Maraging Steel
Metals
maraging steels
atom probe tomography
heat treatment study
X-ray diffraction
intermetallic precipitates
title Cooling Rate Controlled Aging of a Co-Free Fe-Ni-Cr-Mo-Ti-Al Maraging Steel
title_full Cooling Rate Controlled Aging of a Co-Free Fe-Ni-Cr-Mo-Ti-Al Maraging Steel
title_fullStr Cooling Rate Controlled Aging of a Co-Free Fe-Ni-Cr-Mo-Ti-Al Maraging Steel
title_full_unstemmed Cooling Rate Controlled Aging of a Co-Free Fe-Ni-Cr-Mo-Ti-Al Maraging Steel
title_short Cooling Rate Controlled Aging of a Co-Free Fe-Ni-Cr-Mo-Ti-Al Maraging Steel
title_sort cooling rate controlled aging of a co free fe ni cr mo ti al maraging steel
topic maraging steels
atom probe tomography
heat treatment study
X-ray diffraction
intermetallic precipitates
url https://www.mdpi.com/2075-4701/12/4/538
work_keys_str_mv AT stefanzeisl coolingratecontrolledagingofacofreefenicrmotialmaragingsteel
AT ronaldschnitzer coolingratecontrolledagingofacofreefenicrmotialmaragingsteel