Synthesis and Characterization of Molybdenum Disulfide Composite Coating on Steel Using Chemical Vapor Deposition
Molybdenum disulfide (MoS2) is one of the most widely used solid lubricants applied in different ways on the surfaces under friction. In this work, AISI 316 austenitic stainless steel was coated with MoS2, using chemical vapor deposition (CVD) at four different temperatures (400, 500, 600 and 700°C)...
| Main Authors: | , , |
|---|---|
| Format: | Article |
| Language: | English |
| Published: |
Polish Academy of Sciences
2018-06-01
|
| Series: | Archives of Metallurgy and Materials |
| Subjects: | |
| Online Access: | https://journals.pan.pl/Content/103524/PDF/AMM-2018-2-04-Zandrahimi.pdf |
| _version_ | 1811220294696697856 |
|---|---|
| author | E. Moradpour M. Akbarzadeh M. Zandrahimi |
| author_facet | E. Moradpour M. Akbarzadeh M. Zandrahimi |
| author_sort | E. Moradpour |
| collection | DOAJ |
| description | Molybdenum disulfide (MoS2) is one of the most widely used solid lubricants applied in different ways on the surfaces under friction. In this work, AISI 316 austenitic stainless steel was coated with MoS2, using chemical vapor deposition (CVD) at four different temperatures (400, 500, 600 and 700°C). Coatings properties were investigated using SEM, EDX, XRD and FTIR, Hardness Tester and Roughness tester. The results showed that with simultaneous evaporation of sulfur and molybdenum trioxide (MoO3) in the CVD chamber, a uniform coating layer containing MoS2 and MoO2 phases was formed. Increase in the substrate temperature resulted in the rise in the amount of MoS2 to MoO2 phases. The thickness, grain size and the hardness of the coating were 17-29 μm, 50-120 nm and 260-480 HV respectively. Friction tests carried out using pin-on-plate method under normal loads of 10 N under ambient conditions showed values of the friction coefficient 0.25-0.40. |
| first_indexed | 2024-04-12T07:39:01Z |
| format | Article |
| id | doaj.art-999a2b77412a4aec82fb50d687ae30e0 |
| institution | Directory Open Access Journal |
| issn | 2300-1909 |
| language | English |
| last_indexed | 2024-04-12T07:39:01Z |
| publishDate | 2018-06-01 |
| publisher | Polish Academy of Sciences |
| record_format | Article |
| series | Archives of Metallurgy and Materials |
| spelling | doaj.art-999a2b77412a4aec82fb50d687ae30e02022-12-22T03:41:51ZengPolish Academy of SciencesArchives of Metallurgy and Materials2300-19092018-06-01vol. 63No 2https://doi.org/10.24425/118974Synthesis and Characterization of Molybdenum Disulfide Composite Coating on Steel Using Chemical Vapor DepositionE. MoradpourM. AkbarzadehM. ZandrahimiMolybdenum disulfide (MoS2) is one of the most widely used solid lubricants applied in different ways on the surfaces under friction. In this work, AISI 316 austenitic stainless steel was coated with MoS2, using chemical vapor deposition (CVD) at four different temperatures (400, 500, 600 and 700°C). Coatings properties were investigated using SEM, EDX, XRD and FTIR, Hardness Tester and Roughness tester. The results showed that with simultaneous evaporation of sulfur and molybdenum trioxide (MoO3) in the CVD chamber, a uniform coating layer containing MoS2 and MoO2 phases was formed. Increase in the substrate temperature resulted in the rise in the amount of MoS2 to MoO2 phases. The thickness, grain size and the hardness of the coating were 17-29 μm, 50-120 nm and 260-480 HV respectively. Friction tests carried out using pin-on-plate method under normal loads of 10 N under ambient conditions showed values of the friction coefficient 0.25-0.40.https://journals.pan.pl/Content/103524/PDF/AMM-2018-2-04-Zandrahimi.pdfchemical vapor deposition methodsolid lubricant coatingmolybdenum disulfide |
| spellingShingle | E. Moradpour M. Akbarzadeh M. Zandrahimi Synthesis and Characterization of Molybdenum Disulfide Composite Coating on Steel Using Chemical Vapor Deposition Archives of Metallurgy and Materials chemical vapor deposition method solid lubricant coating molybdenum disulfide |
| title | Synthesis and Characterization of Molybdenum Disulfide Composite Coating on Steel Using Chemical Vapor Deposition |
| title_full | Synthesis and Characterization of Molybdenum Disulfide Composite Coating on Steel Using Chemical Vapor Deposition |
| title_fullStr | Synthesis and Characterization of Molybdenum Disulfide Composite Coating on Steel Using Chemical Vapor Deposition |
| title_full_unstemmed | Synthesis and Characterization of Molybdenum Disulfide Composite Coating on Steel Using Chemical Vapor Deposition |
| title_short | Synthesis and Characterization of Molybdenum Disulfide Composite Coating on Steel Using Chemical Vapor Deposition |
| title_sort | synthesis and characterization of molybdenum disulfide composite coating on steel using chemical vapor deposition |
| topic | chemical vapor deposition method solid lubricant coating molybdenum disulfide |
| url | https://journals.pan.pl/Content/103524/PDF/AMM-2018-2-04-Zandrahimi.pdf |
| work_keys_str_mv | AT emoradpour synthesisandcharacterizationofmolybdenumdisulfidecompositecoatingonsteelusingchemicalvapordeposition AT makbarzadeh synthesisandcharacterizationofmolybdenumdisulfidecompositecoatingonsteelusingchemicalvapordeposition AT mzandrahimi synthesisandcharacterizationofmolybdenumdisulfidecompositecoatingonsteelusingchemicalvapordeposition |