Investigation of the Multi-Scale Deterioration Mechanisms of Anhydrite Rock Exposed to Freeze–Thaw Environment

The deterioration of anhydrite rock exposed to a freeze–thaw environment is a complex process. Therefore, this paper systematically investigated the physical and mechanical evolutions of freeze–thawed anhydrite rock through a series of multi-scale laboratory tests. Meanwhile, the correlation between...

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Main Authors: Xiaoguang Jin, Chao Hou, Jie He, Daniel Dias
Format: Article
Language:English
Published: MDPI AG 2024-02-01
Series:Materials
Subjects:
Online Access:https://www.mdpi.com/1996-1944/17/3/726
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author Xiaoguang Jin
Chao Hou
Jie He
Daniel Dias
author_facet Xiaoguang Jin
Chao Hou
Jie He
Daniel Dias
author_sort Xiaoguang Jin
collection DOAJ
description The deterioration of anhydrite rock exposed to a freeze–thaw environment is a complex process. Therefore, this paper systematically investigated the physical and mechanical evolutions of freeze–thawed anhydrite rock through a series of multi-scale laboratory tests. Meanwhile, the correlation between pore structure and macroscopic mechanical parameters was discussed, and the deterioration mechanisms of anhydrite rock under freeze–thaw cycles were revealed. The results show that with the increase in freeze–thaw processes, the mechanical strength, elastic modulus, cohesion, proportions of micropores (r ≤ 0.1 μm), and PT-Ipore throat (0–0.1 μm) decrease exponentially. In comparison, the mass variation, proportions of mesopores (0.1 μm < r < 1 μm), macropores (r ≥ 1 μm), and PT-II pore throat (0.1–4 μm) increase exponentially. After 120 cycles, the mean porosity increases by 66.27%, and there is a significant honeycomb and pitted surface phenomenon. Meanwhile, as the freeze–thaw cycles increase, the frost resistance coefficient decreases, while the damage variable increases. The correlation analysis between pore structure and macroscopic mechanical parameters shows that macropores play the most significant role in the mechanical characteristic deterioration of freeze–thawed anhydrite rock. Finally, it is revealed that the water–rock expansion and water dissolution effects play a crucial role in the multi-scale damage of anhydrite rock under the freeze–thaw environment.
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spelling doaj.art-99c1a2c226e545d2becc209fceadce692024-02-09T15:17:53ZengMDPI AGMaterials1996-19442024-02-0117372610.3390/ma17030726Investigation of the Multi-Scale Deterioration Mechanisms of Anhydrite Rock Exposed to Freeze–Thaw EnvironmentXiaoguang Jin0Chao Hou1Jie He2Daniel Dias3Laboratory of New Technology for Construction of Cities in Mountain Area of the Ministry of Education, Chongqing University, Chongqing 400045, ChinaSchool of Civil Engineering and Architecture, Henan University of Science and Technology, Luoyang 471000, ChinaSchool of Civil Engineering, Chongqing University, Chongqing 400045, ChinaLaboratory 3SR, Grenoble Alpes University, CNRS UMR 5521, 38000 Grenoble, FranceThe deterioration of anhydrite rock exposed to a freeze–thaw environment is a complex process. Therefore, this paper systematically investigated the physical and mechanical evolutions of freeze–thawed anhydrite rock through a series of multi-scale laboratory tests. Meanwhile, the correlation between pore structure and macroscopic mechanical parameters was discussed, and the deterioration mechanisms of anhydrite rock under freeze–thaw cycles were revealed. The results show that with the increase in freeze–thaw processes, the mechanical strength, elastic modulus, cohesion, proportions of micropores (r ≤ 0.1 μm), and PT-Ipore throat (0–0.1 μm) decrease exponentially. In comparison, the mass variation, proportions of mesopores (0.1 μm < r < 1 μm), macropores (r ≥ 1 μm), and PT-II pore throat (0.1–4 μm) increase exponentially. After 120 cycles, the mean porosity increases by 66.27%, and there is a significant honeycomb and pitted surface phenomenon. Meanwhile, as the freeze–thaw cycles increase, the frost resistance coefficient decreases, while the damage variable increases. The correlation analysis between pore structure and macroscopic mechanical parameters shows that macropores play the most significant role in the mechanical characteristic deterioration of freeze–thawed anhydrite rock. Finally, it is revealed that the water–rock expansion and water dissolution effects play a crucial role in the multi-scale damage of anhydrite rock under the freeze–thaw environment.https://www.mdpi.com/1996-1944/17/3/726freeze–thaw cyclesphysical and mechanical propertiesmulti-scaledeterioration mechanismsanhydrite rock
spellingShingle Xiaoguang Jin
Chao Hou
Jie He
Daniel Dias
Investigation of the Multi-Scale Deterioration Mechanisms of Anhydrite Rock Exposed to Freeze–Thaw Environment
Materials
freeze–thaw cycles
physical and mechanical properties
multi-scale
deterioration mechanisms
anhydrite rock
title Investigation of the Multi-Scale Deterioration Mechanisms of Anhydrite Rock Exposed to Freeze–Thaw Environment
title_full Investigation of the Multi-Scale Deterioration Mechanisms of Anhydrite Rock Exposed to Freeze–Thaw Environment
title_fullStr Investigation of the Multi-Scale Deterioration Mechanisms of Anhydrite Rock Exposed to Freeze–Thaw Environment
title_full_unstemmed Investigation of the Multi-Scale Deterioration Mechanisms of Anhydrite Rock Exposed to Freeze–Thaw Environment
title_short Investigation of the Multi-Scale Deterioration Mechanisms of Anhydrite Rock Exposed to Freeze–Thaw Environment
title_sort investigation of the multi scale deterioration mechanisms of anhydrite rock exposed to freeze thaw environment
topic freeze–thaw cycles
physical and mechanical properties
multi-scale
deterioration mechanisms
anhydrite rock
url https://www.mdpi.com/1996-1944/17/3/726
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AT jiehe investigationofthemultiscaledeteriorationmechanismsofanhydriterockexposedtofreezethawenvironment
AT danieldias investigationofthemultiscaledeteriorationmechanismsofanhydriterockexposedtofreezethawenvironment