Direct measurement and calculation of rubber bulk modulus by piston-cylinder method using conventional mechanical testing equipment

This article describes a method to directly measure the bulk modulus of rubber using a piston-cylinder type apparatus. The function of the testing apparatus is to reliably transfer load to the water inside the vessel and allow for the accurate and continuous measurement of volumetric displacement as...

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Main Authors: Dustin T. Clelland, Ethan K. Nickerson, Daniel R. Merkel
Format: Article
Language:English
Published: Elsevier 2023-08-01
Series:Polymer Testing
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S0142941823002155
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author Dustin T. Clelland
Ethan K. Nickerson
Daniel R. Merkel
author_facet Dustin T. Clelland
Ethan K. Nickerson
Daniel R. Merkel
author_sort Dustin T. Clelland
collection DOAJ
description This article describes a method to directly measure the bulk modulus of rubber using a piston-cylinder type apparatus. The function of the testing apparatus is to reliably transfer load to the water inside the vessel and allow for the accurate and continuous measurement of volumetric displacement as the contents are compressed. During the test, load is applied to a piston-cylinder containing the rubber test sample and water using a conventional mechanical testing load frame. Load and the travel of the piston are recorded by a load cell and extensometer, respectfully. A brass or stainless steel plug of the same dimensions as the test sample is tested as a control sample to isolate the compliance of the system, including the compressibility of water and compliance of the o-rings which seal the piston-cylinder system. The results from this control test are used to decouple the compliance of the system from the sample test results. Load-linear displacement data are mathematically converted to pressure-volumetric displacement data, from which bulk modulus is calculated. The test apparatus and method are validated using the known bulk modulus of water. Finally, the bulk moduli for two similar rubbers are evaluated. The validity of the results and limitations of the device are discussed.
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spelling doaj.art-9a0f920243f54662b0c0db842af9e8002023-07-22T04:51:12ZengElsevierPolymer Testing0142-94182023-08-01125108135Direct measurement and calculation of rubber bulk modulus by piston-cylinder method using conventional mechanical testing equipmentDustin T. Clelland0Ethan K. Nickerson1Daniel R. Merkel2Corresponding author.; Pacific Northwest National Laboratory, 902 Battelle Blvd., Richland, 99352, WA, USAPacific Northwest National Laboratory, 902 Battelle Blvd., Richland, 99352, WA, USAPacific Northwest National Laboratory, 902 Battelle Blvd., Richland, 99352, WA, USAThis article describes a method to directly measure the bulk modulus of rubber using a piston-cylinder type apparatus. The function of the testing apparatus is to reliably transfer load to the water inside the vessel and allow for the accurate and continuous measurement of volumetric displacement as the contents are compressed. During the test, load is applied to a piston-cylinder containing the rubber test sample and water using a conventional mechanical testing load frame. Load and the travel of the piston are recorded by a load cell and extensometer, respectfully. A brass or stainless steel plug of the same dimensions as the test sample is tested as a control sample to isolate the compliance of the system, including the compressibility of water and compliance of the o-rings which seal the piston-cylinder system. The results from this control test are used to decouple the compliance of the system from the sample test results. Load-linear displacement data are mathematically converted to pressure-volumetric displacement data, from which bulk modulus is calculated. The test apparatus and method are validated using the known bulk modulus of water. Finally, the bulk moduli for two similar rubbers are evaluated. The validity of the results and limitations of the device are discussed.http://www.sciencedirect.com/science/article/pii/S0142941823002155Bulk modulusRubberMechanical testing
spellingShingle Dustin T. Clelland
Ethan K. Nickerson
Daniel R. Merkel
Direct measurement and calculation of rubber bulk modulus by piston-cylinder method using conventional mechanical testing equipment
Polymer Testing
Bulk modulus
Rubber
Mechanical testing
title Direct measurement and calculation of rubber bulk modulus by piston-cylinder method using conventional mechanical testing equipment
title_full Direct measurement and calculation of rubber bulk modulus by piston-cylinder method using conventional mechanical testing equipment
title_fullStr Direct measurement and calculation of rubber bulk modulus by piston-cylinder method using conventional mechanical testing equipment
title_full_unstemmed Direct measurement and calculation of rubber bulk modulus by piston-cylinder method using conventional mechanical testing equipment
title_short Direct measurement and calculation of rubber bulk modulus by piston-cylinder method using conventional mechanical testing equipment
title_sort direct measurement and calculation of rubber bulk modulus by piston cylinder method using conventional mechanical testing equipment
topic Bulk modulus
Rubber
Mechanical testing
url http://www.sciencedirect.com/science/article/pii/S0142941823002155
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AT danielrmerkel directmeasurementandcalculationofrubberbulkmodulusbypistoncylindermethodusingconventionalmechanicaltestingequipment