Experimento didático sobre cromatografia gasosa: uma abordagem analítica e ambiental Didactic experiment on gas chromatography: an environmental and analytical approach
<abstract language="eng">This paper describes an experiment to teach the principles of gas chromatography exploring the boiling points and polarities to explain the elution order of a series of alcohols, benzene and n-propanone, as well as to teach the response factor concept and the...
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Format: | Article |
Language: | English |
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Sociedade Brasileira de Química
2008-01-01
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Series: | Química Nova |
Subjects: | |
Online Access: | http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422008000800047 |
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author | José Carlos P. Penteado Dulce Magalhães Jorge C. Masini |
author_facet | José Carlos P. Penteado Dulce Magalhães Jorge C. Masini |
author_sort | José Carlos P. Penteado |
collection | DOAJ |
description | <abstract language="eng">This paper describes an experiment to teach the principles of gas chromatography exploring the boiling points and polarities to explain the elution order of a series of alcohols, benzene and n-propanone, as well as to teach the response factor concept and the internal standard addition method. Retention times and response factors are used for qualitative identification and quantitative analysis of a hypothetical contamination source in a simulated water sample. The internal standard n-propanol is further used for quantification of benzene and n-butanol in the water sample. This experiment has been taught in the instrumental analysis course offered to chemistry and oceanography students. |
first_indexed | 2024-12-23T06:25:46Z |
format | Article |
id | doaj.art-9a140ddfba884f6ea37d97b374528d12 |
institution | Directory Open Access Journal |
issn | 0100-4042 1678-7064 |
language | English |
last_indexed | 2024-12-23T06:25:46Z |
publishDate | 2008-01-01 |
publisher | Sociedade Brasileira de Química |
record_format | Article |
series | Química Nova |
spelling | doaj.art-9a140ddfba884f6ea37d97b374528d122022-12-21T17:57:05ZengSociedade Brasileira de QuímicaQuímica Nova0100-40421678-70642008-01-013182190219310.1590/S0100-40422008000800047Experimento didático sobre cromatografia gasosa: uma abordagem analítica e ambiental Didactic experiment on gas chromatography: an environmental and analytical approachJosé Carlos P. PenteadoDulce MagalhãesJorge C. Masini<abstract language="eng">This paper describes an experiment to teach the principles of gas chromatography exploring the boiling points and polarities to explain the elution order of a series of alcohols, benzene and n-propanone, as well as to teach the response factor concept and the internal standard addition method. Retention times and response factors are used for qualitative identification and quantitative analysis of a hypothetical contamination source in a simulated water sample. The internal standard n-propanol is further used for quantification of benzene and n-butanol in the water sample. This experiment has been taught in the instrumental analysis course offered to chemistry and oceanography students.http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422008000800047benzeneinternal standardcontamination |
spellingShingle | José Carlos P. Penteado Dulce Magalhães Jorge C. Masini Experimento didático sobre cromatografia gasosa: uma abordagem analítica e ambiental Didactic experiment on gas chromatography: an environmental and analytical approach Química Nova benzene internal standard contamination |
title | Experimento didático sobre cromatografia gasosa: uma abordagem analítica e ambiental Didactic experiment on gas chromatography: an environmental and analytical approach |
title_full | Experimento didático sobre cromatografia gasosa: uma abordagem analítica e ambiental Didactic experiment on gas chromatography: an environmental and analytical approach |
title_fullStr | Experimento didático sobre cromatografia gasosa: uma abordagem analítica e ambiental Didactic experiment on gas chromatography: an environmental and analytical approach |
title_full_unstemmed | Experimento didático sobre cromatografia gasosa: uma abordagem analítica e ambiental Didactic experiment on gas chromatography: an environmental and analytical approach |
title_short | Experimento didático sobre cromatografia gasosa: uma abordagem analítica e ambiental Didactic experiment on gas chromatography: an environmental and analytical approach |
title_sort | experimento didatico sobre cromatografia gasosa uma abordagem analitica e ambiental didactic experiment on gas chromatography an environmental and analytical approach |
topic | benzene internal standard contamination |
url | http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422008000800047 |
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