Experimento didático sobre cromatografia gasosa: uma abordagem analítica e ambiental Didactic experiment on gas chromatography: an environmental and analytical approach

<abstract language="eng">This paper describes an experiment to teach the principles of gas chromatography exploring the boiling points and polarities to explain the elution order of a series of alcohols, benzene and n-propanone, as well as to teach the response factor concept and the...

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Main Authors: José Carlos P. Penteado, Dulce Magalhães, Jorge C. Masini
Format: Article
Language:English
Published: Sociedade Brasileira de Química 2008-01-01
Series:Química Nova
Subjects:
Online Access:http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422008000800047
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author José Carlos P. Penteado
Dulce Magalhães
Jorge C. Masini
author_facet José Carlos P. Penteado
Dulce Magalhães
Jorge C. Masini
author_sort José Carlos P. Penteado
collection DOAJ
description <abstract language="eng">This paper describes an experiment to teach the principles of gas chromatography exploring the boiling points and polarities to explain the elution order of a series of alcohols, benzene and n-propanone, as well as to teach the response factor concept and the internal standard addition method. Retention times and response factors are used for qualitative identification and quantitative analysis of a hypothetical contamination source in a simulated water sample. The internal standard n-propanol is further used for quantification of benzene and n-butanol in the water sample. This experiment has been taught in the instrumental analysis course offered to chemistry and oceanography students.
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spelling doaj.art-9a140ddfba884f6ea37d97b374528d122022-12-21T17:57:05ZengSociedade Brasileira de QuímicaQuímica Nova0100-40421678-70642008-01-013182190219310.1590/S0100-40422008000800047Experimento didático sobre cromatografia gasosa: uma abordagem analítica e ambiental Didactic experiment on gas chromatography: an environmental and analytical approachJosé Carlos P. PenteadoDulce MagalhãesJorge C. Masini<abstract language="eng">This paper describes an experiment to teach the principles of gas chromatography exploring the boiling points and polarities to explain the elution order of a series of alcohols, benzene and n-propanone, as well as to teach the response factor concept and the internal standard addition method. Retention times and response factors are used for qualitative identification and quantitative analysis of a hypothetical contamination source in a simulated water sample. The internal standard n-propanol is further used for quantification of benzene and n-butanol in the water sample. This experiment has been taught in the instrumental analysis course offered to chemistry and oceanography students.http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422008000800047benzeneinternal standardcontamination
spellingShingle José Carlos P. Penteado
Dulce Magalhães
Jorge C. Masini
Experimento didático sobre cromatografia gasosa: uma abordagem analítica e ambiental Didactic experiment on gas chromatography: an environmental and analytical approach
Química Nova
benzene
internal standard
contamination
title Experimento didático sobre cromatografia gasosa: uma abordagem analítica e ambiental Didactic experiment on gas chromatography: an environmental and analytical approach
title_full Experimento didático sobre cromatografia gasosa: uma abordagem analítica e ambiental Didactic experiment on gas chromatography: an environmental and analytical approach
title_fullStr Experimento didático sobre cromatografia gasosa: uma abordagem analítica e ambiental Didactic experiment on gas chromatography: an environmental and analytical approach
title_full_unstemmed Experimento didático sobre cromatografia gasosa: uma abordagem analítica e ambiental Didactic experiment on gas chromatography: an environmental and analytical approach
title_short Experimento didático sobre cromatografia gasosa: uma abordagem analítica e ambiental Didactic experiment on gas chromatography: an environmental and analytical approach
title_sort experimento didatico sobre cromatografia gasosa uma abordagem analitica e ambiental didactic experiment on gas chromatography an environmental and analytical approach
topic benzene
internal standard
contamination
url http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422008000800047
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