Effect of sintering temperature on physical and structural properties of Alumino-Silicate-Fluoride glass ceramics fabricated from clam shell and soda lime silicate glass

A study on the effect of sintering temperature to the physical and structural of Alumino-Silicate-Fluoride (ASF) glass ceramics fabricated from clam shell (CS) and soda lime silicate (SLS) glass is conducted through conventional melt-quench technique. ASF glass ceramics composition with 25SLS-20CS-2...

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Main Authors: Wan Nurshamimi Wan Jusoh, Khamirul Amin Matori, Mohd Hafiz Mohd Zaid, Norhazlin Zainuddin, Mohammad Zulhasif Ahmad Khiri, Nadia Asyikin Abdul Rahman, Rohaniah Abdul Jalil, Esra Kul
Format: Article
Language:English
Published: Elsevier 2019-03-01
Series:Results in Physics
Online Access:http://www.sciencedirect.com/science/article/pii/S2211379719300804
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author Wan Nurshamimi Wan Jusoh
Khamirul Amin Matori
Mohd Hafiz Mohd Zaid
Norhazlin Zainuddin
Mohammad Zulhasif Ahmad Khiri
Nadia Asyikin Abdul Rahman
Rohaniah Abdul Jalil
Esra Kul
author_facet Wan Nurshamimi Wan Jusoh
Khamirul Amin Matori
Mohd Hafiz Mohd Zaid
Norhazlin Zainuddin
Mohammad Zulhasif Ahmad Khiri
Nadia Asyikin Abdul Rahman
Rohaniah Abdul Jalil
Esra Kul
author_sort Wan Nurshamimi Wan Jusoh
collection DOAJ
description A study on the effect of sintering temperature to the physical and structural of Alumino-Silicate-Fluoride (ASF) glass ceramics fabricated from clam shell (CS) and soda lime silicate (SLS) glass is conducted through conventional melt-quench technique. ASF glass ceramics composition with 25SLS-20CS-20P2O5-20Al2O3-15CaF2 by weight percentage is analysed by using Energy X-ray (EDX), density (ρ), linear shrinkage, X-ray Diffraction (XRD), Fourier Transforms Infrared (FTIR) and Field Emission Scanning Electron Microscopy (FESEM). High content of Ca and Si in CS and SLS glass respectively promote the use of waste materials in production of ASF composition. The density and linear shrinkage of the samples varies with sintering temperature. Besides, XRD results showed that fluorapatite (Ca5(PO4)3F) is a main phase existed in all samples meanwhile FTIR confirmed the presence of silica and also the formation of CaP phase in the composition. FESEM analysis showed the increasing of grain size and formation of needle-like microstructure known as fluorapatite when sintering temperature increase. Overall results promoted the ASF glass ceramics samples produced from waste materials as a high potential candidate for dental application. Keywords: Alumino-Silicate-Fluoride composition, Clam shell, Soda lime silicate glass, Sintering, Fluorapatite
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spelling doaj.art-9a3b768a1bbe46d992924b44885100352022-12-21T19:00:07ZengElsevierResults in Physics2211-37972019-03-011219091914Effect of sintering temperature on physical and structural properties of Alumino-Silicate-Fluoride glass ceramics fabricated from clam shell and soda lime silicate glassWan Nurshamimi Wan Jusoh0Khamirul Amin Matori1Mohd Hafiz Mohd Zaid2Norhazlin Zainuddin3Mohammad Zulhasif Ahmad Khiri4Nadia Asyikin Abdul Rahman5Rohaniah Abdul Jalil6Esra Kul7Department of Physics, Faculty of Science, Universiti Putra Malaysia, 43400 UPM Serdang, Selangor, MalaysiaDepartment of Physics, Faculty of Science, Universiti Putra Malaysia, 43400 UPM Serdang, Selangor, Malaysia; Material Synthesis and Characterization Laboratory, Institute of Advanced Technology, Universiti Putra Malaysia, 43400 UPM Serdang, Selangor, Malaysia; Corresponding author.Department of Physics, Faculty of Science, Universiti Putra Malaysia, 43400 UPM Serdang, Selangor, MalaysiaDepartment of Chemistry, Faculty of Science, Universiti Putra Malaysia, 43400 UPM Serdang, Selangor, MalaysiaMaterial Synthesis and Characterization Laboratory, Institute of Advanced Technology, Universiti Putra Malaysia, 43400 UPM Serdang, Selangor, MalaysiaDepartment of Physics, Faculty of Science, Universiti Putra Malaysia, 43400 UPM Serdang, Selangor, MalaysiaDepartment of Physics, Faculty of Science, Universiti Putra Malaysia, 43400 UPM Serdang, Selangor, MalaysiaDepartment of Prosthodontics, Faculty of Dentistry, Ataturk University, 25030 Erzurum, TurkeyA study on the effect of sintering temperature to the physical and structural of Alumino-Silicate-Fluoride (ASF) glass ceramics fabricated from clam shell (CS) and soda lime silicate (SLS) glass is conducted through conventional melt-quench technique. ASF glass ceramics composition with 25SLS-20CS-20P2O5-20Al2O3-15CaF2 by weight percentage is analysed by using Energy X-ray (EDX), density (ρ), linear shrinkage, X-ray Diffraction (XRD), Fourier Transforms Infrared (FTIR) and Field Emission Scanning Electron Microscopy (FESEM). High content of Ca and Si in CS and SLS glass respectively promote the use of waste materials in production of ASF composition. The density and linear shrinkage of the samples varies with sintering temperature. Besides, XRD results showed that fluorapatite (Ca5(PO4)3F) is a main phase existed in all samples meanwhile FTIR confirmed the presence of silica and also the formation of CaP phase in the composition. FESEM analysis showed the increasing of grain size and formation of needle-like microstructure known as fluorapatite when sintering temperature increase. Overall results promoted the ASF glass ceramics samples produced from waste materials as a high potential candidate for dental application. Keywords: Alumino-Silicate-Fluoride composition, Clam shell, Soda lime silicate glass, Sintering, Fluorapatitehttp://www.sciencedirect.com/science/article/pii/S2211379719300804
spellingShingle Wan Nurshamimi Wan Jusoh
Khamirul Amin Matori
Mohd Hafiz Mohd Zaid
Norhazlin Zainuddin
Mohammad Zulhasif Ahmad Khiri
Nadia Asyikin Abdul Rahman
Rohaniah Abdul Jalil
Esra Kul
Effect of sintering temperature on physical and structural properties of Alumino-Silicate-Fluoride glass ceramics fabricated from clam shell and soda lime silicate glass
Results in Physics
title Effect of sintering temperature on physical and structural properties of Alumino-Silicate-Fluoride glass ceramics fabricated from clam shell and soda lime silicate glass
title_full Effect of sintering temperature on physical and structural properties of Alumino-Silicate-Fluoride glass ceramics fabricated from clam shell and soda lime silicate glass
title_fullStr Effect of sintering temperature on physical and structural properties of Alumino-Silicate-Fluoride glass ceramics fabricated from clam shell and soda lime silicate glass
title_full_unstemmed Effect of sintering temperature on physical and structural properties of Alumino-Silicate-Fluoride glass ceramics fabricated from clam shell and soda lime silicate glass
title_short Effect of sintering temperature on physical and structural properties of Alumino-Silicate-Fluoride glass ceramics fabricated from clam shell and soda lime silicate glass
title_sort effect of sintering temperature on physical and structural properties of alumino silicate fluoride glass ceramics fabricated from clam shell and soda lime silicate glass
url http://www.sciencedirect.com/science/article/pii/S2211379719300804
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