CHARACTERISTIC OF PRASEODYMIUM OXIDE BASED CATALYST IN METHANATION: EFFECT CALCINATION TEMPERATURE

Methanation reaction using carbon dioxide gas is one of favorable green technology to form methane gas by converting carbon dioxide in the presence of hydrogen. This technology needs the catalyst to achieve a higher catalytic activity. Therefore, a catalyst of Ru/Mn/Pr (5:30:65)/Al2O3 (RMP, 5:30:60)...

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Main Authors: Salmiah Jamal Mat Rosid, Susilawati Toemen, Wan Azelee Wan Abu Bakar a, Sarina Mat Rosid, Wan Nazwanie Wan Abdullah, Siti Maisarah Aziz
Format: Article
Language:English
Published: Universiti Teknologi MARA, Negeri Sembilan 2021-04-01
Series:Journal of Academia
Subjects:
Online Access:https://myjms.mohe.gov.my/index.php/joa/article/view/11103
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author Salmiah Jamal Mat Rosid
Susilawati Toemen
Wan Azelee Wan Abu Bakar a
Sarina Mat Rosid
Wan Nazwanie Wan Abdullah
Siti Maisarah Aziz
author_facet Salmiah Jamal Mat Rosid
Susilawati Toemen
Wan Azelee Wan Abu Bakar a
Sarina Mat Rosid
Wan Nazwanie Wan Abdullah
Siti Maisarah Aziz
author_sort Salmiah Jamal Mat Rosid
collection DOAJ
description Methanation reaction using carbon dioxide gas is one of favorable green technology to form methane gas by converting carbon dioxide in the presence of hydrogen. This technology needs the catalyst to achieve a higher catalytic activity. Therefore, a catalyst of Ru/Mn/Pr (5:30:65)/Al2O3 (RMP, 5:30:60) was prepared via wetness impregnation method and investigated on the effect of calcination temperatures with respect to catalytic performance using FTIR analysis. The RMP (5:30:60) catalyst calcined at 800oC was chosen as an excel catalyst with 96.9% of CO2 conversion and 45.1% CH4 formation at 350oC reaction temperature. From the EDX mapping, it can be observed that the distribution of all element is homogeneous at 800oC except Ru, O and Al at 900oC and 1000oC calcination temperature. The image from FESEM also shows the presence of some crystal shape on the catalyst surface. From the FTIR analysis, the peaks stretching and bending mode of O-H bonding decreased when the calcination temperature increased.
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spelling doaj.art-9a6bc9758d7a45a395b69034e53dd8282024-04-17T16:36:02ZengUniversiti Teknologi MARA, Negeri SembilanJournal of Academia2289-63682021-04-01914955CHARACTERISTIC OF PRASEODYMIUM OXIDE BASED CATALYST IN METHANATION: EFFECT CALCINATION TEMPERATURESalmiah Jamal Mat Rosid 0Susilawati Toemen 1Wan Azelee Wan Abu Bakar a2Sarina Mat Rosid 3Wan Nazwanie Wan Abdullah 4Siti Maisarah Aziz 5Universiti Sultan Zainal AbidinUniversiti Teknologi MalaysiaUniversiti Teknologi MalaysiUniversiti Teknologi MalaysiaUniversiti Sains MalaysiaUniversiti Sultan Zainal AbidinMethanation reaction using carbon dioxide gas is one of favorable green technology to form methane gas by converting carbon dioxide in the presence of hydrogen. This technology needs the catalyst to achieve a higher catalytic activity. Therefore, a catalyst of Ru/Mn/Pr (5:30:65)/Al2O3 (RMP, 5:30:60) was prepared via wetness impregnation method and investigated on the effect of calcination temperatures with respect to catalytic performance using FTIR analysis. The RMP (5:30:60) catalyst calcined at 800oC was chosen as an excel catalyst with 96.9% of CO2 conversion and 45.1% CH4 formation at 350oC reaction temperature. From the EDX mapping, it can be observed that the distribution of all element is homogeneous at 800oC except Ru, O and Al at 900oC and 1000oC calcination temperature. The image from FESEM also shows the presence of some crystal shape on the catalyst surface. From the FTIR analysis, the peaks stretching and bending mode of O-H bonding decreased when the calcination temperature increased.https://myjms.mohe.gov.my/index.php/joa/article/view/11103calcination temperaturemethanationmorphologypraseodymium
spellingShingle Salmiah Jamal Mat Rosid
Susilawati Toemen
Wan Azelee Wan Abu Bakar a
Sarina Mat Rosid
Wan Nazwanie Wan Abdullah
Siti Maisarah Aziz
CHARACTERISTIC OF PRASEODYMIUM OXIDE BASED CATALYST IN METHANATION: EFFECT CALCINATION TEMPERATURE
Journal of Academia
calcination temperature
methanation
morphology
praseodymium
title CHARACTERISTIC OF PRASEODYMIUM OXIDE BASED CATALYST IN METHANATION: EFFECT CALCINATION TEMPERATURE
title_full CHARACTERISTIC OF PRASEODYMIUM OXIDE BASED CATALYST IN METHANATION: EFFECT CALCINATION TEMPERATURE
title_fullStr CHARACTERISTIC OF PRASEODYMIUM OXIDE BASED CATALYST IN METHANATION: EFFECT CALCINATION TEMPERATURE
title_full_unstemmed CHARACTERISTIC OF PRASEODYMIUM OXIDE BASED CATALYST IN METHANATION: EFFECT CALCINATION TEMPERATURE
title_short CHARACTERISTIC OF PRASEODYMIUM OXIDE BASED CATALYST IN METHANATION: EFFECT CALCINATION TEMPERATURE
title_sort characteristic of praseodymium oxide based catalyst in methanation effect calcination temperature
topic calcination temperature
methanation
morphology
praseodymium
url https://myjms.mohe.gov.my/index.php/joa/article/view/11103
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AT wanazeleewanabubakara characteristicofpraseodymiumoxidebasedcatalystinmethanationeffectcalcinationtemperature
AT sarinamatrosid characteristicofpraseodymiumoxidebasedcatalystinmethanationeffectcalcinationtemperature
AT wannazwaniewanabdullah characteristicofpraseodymiumoxidebasedcatalystinmethanationeffectcalcinationtemperature
AT sitimaisarahaziz characteristicofpraseodymiumoxidebasedcatalystinmethanationeffectcalcinationtemperature