An undergraduate level experiment on the synthesis of Au nanoparticles and their size-dependent optical and catalytic properties

The synthesis of gold nanoparticles (Au NPs) 15, 26, and 34 nm in diameter, followed by the investigation of their size-dependent optical and catalytic properties, is described herein as an undergraduate level experiment. The proposed experiment covers concepts on the synthesis, stabilization, and c...

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Main Authors: Anderson G. M. da Silva, Thenner S. Rodrigues, Alexandra Macedo, Rafael T. P. da Silva, Pedro H. C. Camargo
Format: Article
Language:English
Published: Sociedade Brasileira de Química 2014-01-01
Series:Química Nova
Subjects:
Online Access:http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422014001000023&lng=en&tlng=en
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author Anderson G. M. da Silva
Thenner S. Rodrigues
Alexandra Macedo
Rafael T. P. da Silva
Pedro H. C. Camargo
author_facet Anderson G. M. da Silva
Thenner S. Rodrigues
Alexandra Macedo
Rafael T. P. da Silva
Pedro H. C. Camargo
author_sort Anderson G. M. da Silva
collection DOAJ
description The synthesis of gold nanoparticles (Au NPs) 15, 26, and 34 nm in diameter, followed by the investigation of their size-dependent optical and catalytic properties, is described herein as an undergraduate level experiment. The proposed experiment covers concepts on the synthesis, stabilization, and characterization of Au NPs, their size-dependent optical and catalytic properties at the nanoscale, chemical kinetics, and the role of a catalyst. The experiment should be performed by groups of two or three students in three lab sessions of 3 h each and organized as follows: i) synthesis of Au NPs of different sizes and investigation of their optical properties; ii) evaluation of their catalytic activity; and iii) data analysis and discussion. We believe that this activity enables students to integrate these multidisciplinary concepts in a single experiment as well as to become introduced/familiarized with an active research field and current literature in the areas of nanoparticle synthesis and catalysis.
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spelling doaj.art-9ae0be7cbbd44851859a054afd11ee102022-12-22T02:54:58ZengSociedade Brasileira de QuímicaQuímica Nova1678-70642014-01-0137101716172010.5935/0100-4042.20140235S0100-40422014001000023An undergraduate level experiment on the synthesis of Au nanoparticles and their size-dependent optical and catalytic propertiesAnderson G. M. da Silva0Thenner S. Rodrigues1Alexandra Macedo2Rafael T. P. da Silva3Pedro H. C. Camargo4Universidade de São PauloUniversidade de São PauloUniversidade de São PauloUniversidade de São PauloUniversidade de São PauloThe synthesis of gold nanoparticles (Au NPs) 15, 26, and 34 nm in diameter, followed by the investigation of their size-dependent optical and catalytic properties, is described herein as an undergraduate level experiment. The proposed experiment covers concepts on the synthesis, stabilization, and characterization of Au NPs, their size-dependent optical and catalytic properties at the nanoscale, chemical kinetics, and the role of a catalyst. The experiment should be performed by groups of two or three students in three lab sessions of 3 h each and organized as follows: i) synthesis of Au NPs of different sizes and investigation of their optical properties; ii) evaluation of their catalytic activity; and iii) data analysis and discussion. We believe that this activity enables students to integrate these multidisciplinary concepts in a single experiment as well as to become introduced/familiarized with an active research field and current literature in the areas of nanoparticle synthesis and catalysis.http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422014001000023&lng=en&tlng=enlaboratory experimentundergraduate levelgold nanoparticlescatalysissize-dependent properties
spellingShingle Anderson G. M. da Silva
Thenner S. Rodrigues
Alexandra Macedo
Rafael T. P. da Silva
Pedro H. C. Camargo
An undergraduate level experiment on the synthesis of Au nanoparticles and their size-dependent optical and catalytic properties
Química Nova
laboratory experiment
undergraduate level
gold nanoparticles
catalysis
size-dependent properties
title An undergraduate level experiment on the synthesis of Au nanoparticles and their size-dependent optical and catalytic properties
title_full An undergraduate level experiment on the synthesis of Au nanoparticles and their size-dependent optical and catalytic properties
title_fullStr An undergraduate level experiment on the synthesis of Au nanoparticles and their size-dependent optical and catalytic properties
title_full_unstemmed An undergraduate level experiment on the synthesis of Au nanoparticles and their size-dependent optical and catalytic properties
title_short An undergraduate level experiment on the synthesis of Au nanoparticles and their size-dependent optical and catalytic properties
title_sort undergraduate level experiment on the synthesis of au nanoparticles and their size dependent optical and catalytic properties
topic laboratory experiment
undergraduate level
gold nanoparticles
catalysis
size-dependent properties
url http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422014001000023&lng=en&tlng=en
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