Impacts of the calcination temperature on the structural and radiation shielding properties of the NASICON compound synthesized from zircon minerals

The present work aims to fabricate Na1+xZr2SixP3-xO12 compound at various calcination temperatures based on the zircon mineral. The fabricated compound was calcinated at 250, 500, and 1000°C. The effect of calcination temperature on the structure, crystal phase, and radiation shielding properties wa...

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Main Authors: Islam G. Alhindawy, Hany Gamal, Aljawhara.H. Almuqrin, M.I. Sayyed, K.A. Mahmoud
Format: Article
Language:English
Published: Elsevier 2023-05-01
Series:Nuclear Engineering and Technology
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S1738573323000864
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author Islam G. Alhindawy
Hany Gamal
Aljawhara.H. Almuqrin
M.I. Sayyed
K.A. Mahmoud
author_facet Islam G. Alhindawy
Hany Gamal
Aljawhara.H. Almuqrin
M.I. Sayyed
K.A. Mahmoud
author_sort Islam G. Alhindawy
collection DOAJ
description The present work aims to fabricate Na1+xZr2SixP3-xO12 compound at various calcination temperatures based on the zircon mineral. The fabricated compound was calcinated at 250, 500, and 1000°C. The effect of calcination temperature on the structure, crystal phase, and radiation shielding properties was studied for the fabricated compound. The X-ray diffraction diffractometer demonstrates that, the monoclinic crystal phase appeared at a calcination temperature of 250°C and 500°C is totally transformed to a high-symmetry hexagonal crystal phase under a calcination temperature of 1000°C. The radiation shielding capacity was also qualified for the fabricated compounds using the Monte Carlo N-Particle transport code in the γ-photons energy interval between 15keV and 122keV. The impacts of calcination temperature on the γ-ray shielding behavior were clarified in the present study, where the linear attenuation coefficient was enhanced by 218% at energy of 122keV, when the calcination temperature increased from 250 to 1000°C, respectively.
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spelling doaj.art-9ae4577a3f2f445ebdb19d5fe8e11c7d2023-05-19T04:45:17ZengElsevierNuclear Engineering and Technology1738-57332023-05-0155518851891Impacts of the calcination temperature on the structural and radiation shielding properties of the NASICON compound synthesized from zircon mineralsIslam G. Alhindawy0Hany Gamal1Aljawhara.H. Almuqrin2M.I. Sayyed3K.A. Mahmoud4Nuclear Materials Authority, P.O. Box 530, El-Maadi, Cairo, Egypt; Corresponding author.Nuclear Materials Authority, P.O. Box 530, El-Maadi, Cairo, EgyptDepartment of Physics, College of Science, Princess Nourah Bint Abdulrahman University, P.O.Box 84428, Riyadh, 11671, Saudi ArabiaDepartment of Physics, Faculty of Science, Isra University, Amman, Jordan; Department of Nuclear Medicine Research, Institute for Research and Medical Consultations (IRMC), Imam Abdulrahman Bin Faisal University (IAU), P.O. Box 1982, Dammam, 31441, Saudi ArabiaNuclear Materials Authority, P.O. Box 530, El-Maadi, Cairo, Egypt; Ural Federal University, 19 Mira St, 620002, Yekaterinburg, Russia; Corresponding author. Nuclear Materials Authority, P.O. Box 530 El-Maadi, Cairo, Egypt.The present work aims to fabricate Na1+xZr2SixP3-xO12 compound at various calcination temperatures based on the zircon mineral. The fabricated compound was calcinated at 250, 500, and 1000°C. The effect of calcination temperature on the structure, crystal phase, and radiation shielding properties was studied for the fabricated compound. The X-ray diffraction diffractometer demonstrates that, the monoclinic crystal phase appeared at a calcination temperature of 250°C and 500°C is totally transformed to a high-symmetry hexagonal crystal phase under a calcination temperature of 1000°C. The radiation shielding capacity was also qualified for the fabricated compounds using the Monte Carlo N-Particle transport code in the γ-photons energy interval between 15keV and 122keV. The impacts of calcination temperature on the γ-ray shielding behavior were clarified in the present study, where the linear attenuation coefficient was enhanced by 218% at energy of 122keV, when the calcination temperature increased from 250 to 1000°C, respectively.http://www.sciencedirect.com/science/article/pii/S1738573323000864Zircon mineralNASICON compoundsCalcination temperatureRadiation shielding propertiesMonte Carlo simulation
spellingShingle Islam G. Alhindawy
Hany Gamal
Aljawhara.H. Almuqrin
M.I. Sayyed
K.A. Mahmoud
Impacts of the calcination temperature on the structural and radiation shielding properties of the NASICON compound synthesized from zircon minerals
Nuclear Engineering and Technology
Zircon mineral
NASICON compounds
Calcination temperature
Radiation shielding properties
Monte Carlo simulation
title Impacts of the calcination temperature on the structural and radiation shielding properties of the NASICON compound synthesized from zircon minerals
title_full Impacts of the calcination temperature on the structural and radiation shielding properties of the NASICON compound synthesized from zircon minerals
title_fullStr Impacts of the calcination temperature on the structural and radiation shielding properties of the NASICON compound synthesized from zircon minerals
title_full_unstemmed Impacts of the calcination temperature on the structural and radiation shielding properties of the NASICON compound synthesized from zircon minerals
title_short Impacts of the calcination temperature on the structural and radiation shielding properties of the NASICON compound synthesized from zircon minerals
title_sort impacts of the calcination temperature on the structural and radiation shielding properties of the nasicon compound synthesized from zircon minerals
topic Zircon mineral
NASICON compounds
Calcination temperature
Radiation shielding properties
Monte Carlo simulation
url http://www.sciencedirect.com/science/article/pii/S1738573323000864
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