Tapered Optical Fiber Functionalized with Palladium Nanoparticles by Drop Casting and Laser Radiation for H2 and Volatile Organic Compounds Sensing Purposes

A comparative study on the sensing properties of a tapered optical fiber pristine and functionalized with the palladium nanoparticles to hydrogen and volatile organic compounds (VOCs), is presented. The sensor response and, response/recovery times were extracted from the measurements of the transien...

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Main Authors: Nancy Elizabeth González-Sierra, Luz del Carmen Gómez-Pavón, Gerardo Francisco Pérez-Sánchez, Arnulfo Luis-Ramos, Plácido Zaca-Morán, Jesús Manuel Muñoz-Pacheco, Fernando Chávez-Ramírez
Format: Article
Language:English
Published: MDPI AG 2017-09-01
Series:Sensors
Subjects:
Online Access:https://www.mdpi.com/1424-8220/17/9/2039
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author Nancy Elizabeth González-Sierra
Luz del Carmen Gómez-Pavón
Gerardo Francisco Pérez-Sánchez
Arnulfo Luis-Ramos
Plácido Zaca-Morán
Jesús Manuel Muñoz-Pacheco
Fernando Chávez-Ramírez
author_facet Nancy Elizabeth González-Sierra
Luz del Carmen Gómez-Pavón
Gerardo Francisco Pérez-Sánchez
Arnulfo Luis-Ramos
Plácido Zaca-Morán
Jesús Manuel Muñoz-Pacheco
Fernando Chávez-Ramírez
author_sort Nancy Elizabeth González-Sierra
collection DOAJ
description A comparative study on the sensing properties of a tapered optical fiber pristine and functionalized with the palladium nanoparticles to hydrogen and volatile organic compounds (VOCs), is presented. The sensor response and, response/recovery times were extracted from the measurements of the transient response of the device. The tapered optical fiber sensor was fabricated using a single-mode optical fiber by the flame-brushing technique. Functionalization of the optical fiber was performed using an aqueous solution of palladium chloride by drop-casting technique assisted for laser radiation. The detection principle of the sensor is based on the changes in the optical properties of palladium nanoparticles when exposed to reducing gases, which causes a variation in the absorption of evanescent waves. A continuous wave laser diode operating at 1550 nm is used for the sensor characterization. The sensor functionalized with palladium nanoparticles by this technique is viable for the sensing of hydrogen and VOCs, since it shows an enhancement in sensor response and response time compared to the sensor based on the pristine optical microfiber. The results show that the fabricated sensor is competitive with other fiber optic sensors functionalized with palladium nanoparticles to the hydrogen.
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spelling doaj.art-9bcd7c2dc0dc462695270f9ac82f51022022-12-22T03:58:35ZengMDPI AGSensors1424-82202017-09-01179203910.3390/s17092039s17092039Tapered Optical Fiber Functionalized with Palladium Nanoparticles by Drop Casting and Laser Radiation for H2 and Volatile Organic Compounds Sensing PurposesNancy Elizabeth González-Sierra0Luz del Carmen Gómez-Pavón1Gerardo Francisco Pérez-Sánchez2Arnulfo Luis-Ramos3Plácido Zaca-Morán4Jesús Manuel Muñoz-Pacheco5Fernando Chávez-Ramírez6Grupo de Sistemas Fotónicos y Nanoóptica, Facultad de Ciencias de la Electrónica, Benemérita Universidad Autónoma de Puebla, CP 72570 Puebla, Pue., MexicoGrupo de Sistemas Fotónicos y Nanoóptica, Facultad de Ciencias de la Electrónica, Benemérita Universidad Autónoma de Puebla, CP 72570 Puebla, Pue., MexicoInstituto de Ciencias, Benemérita Universidad Autónoma de Puebla, CP 72050 Puebla, Pue., MexicoGrupo de Sistemas Fotónicos y Nanoóptica, Facultad de Ciencias de la Electrónica, Benemérita Universidad Autónoma de Puebla, CP 72570 Puebla, Pue., MexicoInstituto de Ciencias, Benemérita Universidad Autónoma de Puebla, CP 72050 Puebla, Pue., MexicoGrupo de Sistemas Fotónicos y Nanoóptica, Facultad de Ciencias de la Electrónica, Benemérita Universidad Autónoma de Puebla, CP 72570 Puebla, Pue., MexicoInstituto de Ciencias, Benemérita Universidad Autónoma de Puebla, CP 72050 Puebla, Pue., MexicoA comparative study on the sensing properties of a tapered optical fiber pristine and functionalized with the palladium nanoparticles to hydrogen and volatile organic compounds (VOCs), is presented. The sensor response and, response/recovery times were extracted from the measurements of the transient response of the device. The tapered optical fiber sensor was fabricated using a single-mode optical fiber by the flame-brushing technique. Functionalization of the optical fiber was performed using an aqueous solution of palladium chloride by drop-casting technique assisted for laser radiation. The detection principle of the sensor is based on the changes in the optical properties of palladium nanoparticles when exposed to reducing gases, which causes a variation in the absorption of evanescent waves. A continuous wave laser diode operating at 1550 nm is used for the sensor characterization. The sensor functionalized with palladium nanoparticles by this technique is viable for the sensing of hydrogen and VOCs, since it shows an enhancement in sensor response and response time compared to the sensor based on the pristine optical microfiber. The results show that the fabricated sensor is competitive with other fiber optic sensors functionalized with palladium nanoparticles to the hydrogen.https://www.mdpi.com/1424-8220/17/9/2039Tapered optical fiberfunctionalizedpalladium nanoparticles
spellingShingle Nancy Elizabeth González-Sierra
Luz del Carmen Gómez-Pavón
Gerardo Francisco Pérez-Sánchez
Arnulfo Luis-Ramos
Plácido Zaca-Morán
Jesús Manuel Muñoz-Pacheco
Fernando Chávez-Ramírez
Tapered Optical Fiber Functionalized with Palladium Nanoparticles by Drop Casting and Laser Radiation for H2 and Volatile Organic Compounds Sensing Purposes
Sensors
Tapered optical fiber
functionalized
palladium nanoparticles
title Tapered Optical Fiber Functionalized with Palladium Nanoparticles by Drop Casting and Laser Radiation for H2 and Volatile Organic Compounds Sensing Purposes
title_full Tapered Optical Fiber Functionalized with Palladium Nanoparticles by Drop Casting and Laser Radiation for H2 and Volatile Organic Compounds Sensing Purposes
title_fullStr Tapered Optical Fiber Functionalized with Palladium Nanoparticles by Drop Casting and Laser Radiation for H2 and Volatile Organic Compounds Sensing Purposes
title_full_unstemmed Tapered Optical Fiber Functionalized with Palladium Nanoparticles by Drop Casting and Laser Radiation for H2 and Volatile Organic Compounds Sensing Purposes
title_short Tapered Optical Fiber Functionalized with Palladium Nanoparticles by Drop Casting and Laser Radiation for H2 and Volatile Organic Compounds Sensing Purposes
title_sort tapered optical fiber functionalized with palladium nanoparticles by drop casting and laser radiation for h2 and volatile organic compounds sensing purposes
topic Tapered optical fiber
functionalized
palladium nanoparticles
url https://www.mdpi.com/1424-8220/17/9/2039
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