Reaction sintering in compacted hydrolysed carbonated calcium phosphate

The thermal behaviour of the compact of an uncalcined hydrolysed carbonated calcium phosphate powder slowly heated in air (i.e. under conditions of the reaction sintering) was studied to reveal the reactions which could influence its densification up to 1100°C. A number of different reactions were f...

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Main Authors: Zyman Zoltan, Epple Matthias, Goncharenko Anton, Tkachenko Mykola, Rokhmistrov Dmytro, Sofronov Dmytro, Orlov Herman
Format: Article
Language:English
Published: University of Novi Sad 2023-12-01
Series:Processing and Application of Ceramics
Subjects:
Online Access:https://doiserbia.nb.rs/img/doi/1820-6131/2023/1820-61312304421Z.pdf
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author Zyman Zoltan
Epple Matthias
Goncharenko Anton
Tkachenko Mykola
Rokhmistrov Dmytro
Sofronov Dmytro
Orlov Herman
author_facet Zyman Zoltan
Epple Matthias
Goncharenko Anton
Tkachenko Mykola
Rokhmistrov Dmytro
Sofronov Dmytro
Orlov Herman
author_sort Zyman Zoltan
collection DOAJ
description The thermal behaviour of the compact of an uncalcined hydrolysed carbonated calcium phosphate powder slowly heated in air (i.e. under conditions of the reaction sintering) was studied to reveal the reactions which could influence its densification up to 1100°C. A number of different reactions were found which occurred with different efficiency, but finally enabled a densification of about 94%TD of the composite with a hydroxyapatite/β-tricalcium phosphate (HA/β-TCP) ratio of 48/52. Such composites are highly perspective for further densification under the conventional or other suitable sintering methods at a desired temperature in the production of improved HA/β-TCP ceramics.
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spelling doaj.art-9c3fed27e9d14076a8e9a087be71966b2024-02-01T13:36:25ZengUniversity of Novi SadProcessing and Application of Ceramics1820-61312406-10342023-12-0117442142710.2298/PAC2304421ZReaction sintering in compacted hydrolysed carbonated calcium phosphateZyman Zoltan0Epple Matthias1Goncharenko Anton2Tkachenko Mykola3Rokhmistrov Dmytro4Sofronov Dmytro5Orlov Herman6Physics of Solids Department, V.N. Karazin Kharkiv National University, Kharkiv, UkraineInorganic Chemistry and Center for Nanointegration Duisburg-Essen (CeNIDE), University of Duisburg-Essen, Essen, GermanyPhysics of Solids Department, V.N. Karazin Kharkiv National University, Kharkiv, UkrainePhysics of Solids Department, V.N. Karazin Kharkiv National University, Kharkiv, UkrainePhysics of Solids Department, V.N. Karazin Kharkiv National University, Kharkiv, UkraineInstitute for Single Crystals of National Academy of Sciences of Ukraine, Kharkiv, UkrainePhysics of Solids Department, V.N. Karazin Kharkiv National University, Kharkiv, UkraineThe thermal behaviour of the compact of an uncalcined hydrolysed carbonated calcium phosphate powder slowly heated in air (i.e. under conditions of the reaction sintering) was studied to reveal the reactions which could influence its densification up to 1100°C. A number of different reactions were found which occurred with different efficiency, but finally enabled a densification of about 94%TD of the composite with a hydroxyapatite/β-tricalcium phosphate (HA/β-TCP) ratio of 48/52. Such composites are highly perspective for further densification under the conventional or other suitable sintering methods at a desired temperature in the production of improved HA/β-TCP ceramics.https://doiserbia.nb.rs/img/doi/1820-6131/2023/1820-61312304421Z.pdfbioceramicsbiphasic calcium phosphatesreaction sinteringdensification
spellingShingle Zyman Zoltan
Epple Matthias
Goncharenko Anton
Tkachenko Mykola
Rokhmistrov Dmytro
Sofronov Dmytro
Orlov Herman
Reaction sintering in compacted hydrolysed carbonated calcium phosphate
Processing and Application of Ceramics
bioceramics
biphasic calcium phosphates
reaction sintering
densification
title Reaction sintering in compacted hydrolysed carbonated calcium phosphate
title_full Reaction sintering in compacted hydrolysed carbonated calcium phosphate
title_fullStr Reaction sintering in compacted hydrolysed carbonated calcium phosphate
title_full_unstemmed Reaction sintering in compacted hydrolysed carbonated calcium phosphate
title_short Reaction sintering in compacted hydrolysed carbonated calcium phosphate
title_sort reaction sintering in compacted hydrolysed carbonated calcium phosphate
topic bioceramics
biphasic calcium phosphates
reaction sintering
densification
url https://doiserbia.nb.rs/img/doi/1820-6131/2023/1820-61312304421Z.pdf
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AT epplematthias reactionsinteringincompactedhydrolysedcarbonatedcalciumphosphate
AT goncharenkoanton reactionsinteringincompactedhydrolysedcarbonatedcalciumphosphate
AT tkachenkomykola reactionsinteringincompactedhydrolysedcarbonatedcalciumphosphate
AT rokhmistrovdmytro reactionsinteringincompactedhydrolysedcarbonatedcalciumphosphate
AT sofronovdmytro reactionsinteringincompactedhydrolysedcarbonatedcalciumphosphate
AT orlovherman reactionsinteringincompactedhydrolysedcarbonatedcalciumphosphate