The Effect of Polyvinyl Alcohol Concentration on the Growth Kinetics of KTiOPO4 Nanoparticles Synthesized by the Co-precipitation Method

KTiOPO4 nanoparticles are known as the best candidate to utilize for second-harmonic generation in multiphoton microscopes and bio labels. Size and shape are important and effective parameters to control the properties of nanoparticles. In this paper, we will investigate the role of capping agent co...

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Main Author: Elaheh Gharibshahian
Format: Article
Language:English
Published: Ital Publication 2020-12-01
Series:HighTech and Innovation Journal
Subjects:
Online Access:https://www.hightechjournal.org/index.php/HIJ/article/view/67
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author Elaheh Gharibshahian
author_facet Elaheh Gharibshahian
author_sort Elaheh Gharibshahian
collection DOAJ
description KTiOPO4 nanoparticles are known as the best candidate to utilize for second-harmonic generation in multiphoton microscopes and bio labels. Size and shape are important and effective parameters to control the properties of nanoparticles. In this paper, we will investigate the role of capping agent concentration on the size and shape control of KTP nanoparticles. We synthesized KTP nanoparticles by the co-precipitation method. Polyvinyl alcohol with different mole ratios to titanium ion (1:3, 1:2, 1:1) was used as a capping agent. Products were examined by X-ray diffraction patterns and scanning electron microscopy analyses. X-ray diffraction patterns confirmed the formation of the KTP structure. The biggest (56.36nm) and smallest (39.42nm) grain size were obtained by 1:3 and 1:1 mole ratios of capping agent, respectively. Dumbly, spherical and polyhedral forms of KTP nanoparticles were observed by the change in capping agent mole ratio. The narrowest size distribution of KTiOPO4 nanoparticles was obtained at 1:1 mole ratio of capping agent.   Doi: 10.28991/HIJ-2020-01-04-06 Full Text: PDF
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spelling doaj.art-9c7ba7a6b6ea430eb3e3368763c1e3722022-12-21T18:14:15ZengItal PublicationHighTech and Innovation Journal2723-95352020-12-011418719310.28991/HIJ-2020-01-04-0621The Effect of Polyvinyl Alcohol Concentration on the Growth Kinetics of KTiOPO4 Nanoparticles Synthesized by the Co-precipitation MethodElaheh Gharibshahian0Narjes Vocational college, Technical and Vocational University, Semnan,KTiOPO4 nanoparticles are known as the best candidate to utilize for second-harmonic generation in multiphoton microscopes and bio labels. Size and shape are important and effective parameters to control the properties of nanoparticles. In this paper, we will investigate the role of capping agent concentration on the size and shape control of KTP nanoparticles. We synthesized KTP nanoparticles by the co-precipitation method. Polyvinyl alcohol with different mole ratios to titanium ion (1:3, 1:2, 1:1) was used as a capping agent. Products were examined by X-ray diffraction patterns and scanning electron microscopy analyses. X-ray diffraction patterns confirmed the formation of the KTP structure. The biggest (56.36nm) and smallest (39.42nm) grain size were obtained by 1:3 and 1:1 mole ratios of capping agent, respectively. Dumbly, spherical and polyhedral forms of KTP nanoparticles were observed by the change in capping agent mole ratio. The narrowest size distribution of KTiOPO4 nanoparticles was obtained at 1:1 mole ratio of capping agent.   Doi: 10.28991/HIJ-2020-01-04-06 Full Text: PDFhttps://www.hightechjournal.org/index.php/HIJ/article/view/67co-precipitation methodnanoparticlespotassium titanyl phosphatesize controlshape control.
spellingShingle Elaheh Gharibshahian
The Effect of Polyvinyl Alcohol Concentration on the Growth Kinetics of KTiOPO4 Nanoparticles Synthesized by the Co-precipitation Method
HighTech and Innovation Journal
co-precipitation method
nanoparticles
potassium titanyl phosphate
size control
shape control.
title The Effect of Polyvinyl Alcohol Concentration on the Growth Kinetics of KTiOPO4 Nanoparticles Synthesized by the Co-precipitation Method
title_full The Effect of Polyvinyl Alcohol Concentration on the Growth Kinetics of KTiOPO4 Nanoparticles Synthesized by the Co-precipitation Method
title_fullStr The Effect of Polyvinyl Alcohol Concentration on the Growth Kinetics of KTiOPO4 Nanoparticles Synthesized by the Co-precipitation Method
title_full_unstemmed The Effect of Polyvinyl Alcohol Concentration on the Growth Kinetics of KTiOPO4 Nanoparticles Synthesized by the Co-precipitation Method
title_short The Effect of Polyvinyl Alcohol Concentration on the Growth Kinetics of KTiOPO4 Nanoparticles Synthesized by the Co-precipitation Method
title_sort effect of polyvinyl alcohol concentration on the growth kinetics of ktiopo4 nanoparticles synthesized by the co precipitation method
topic co-precipitation method
nanoparticles
potassium titanyl phosphate
size control
shape control.
url https://www.hightechjournal.org/index.php/HIJ/article/view/67
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