Investigating the effect of milling time on structural, mechanical and tribological properties of a nanostructured hiped alpha alumina for biomaterial applications
In this work was prepared α-Al2O3 alloys from laboratory aluminum oxide powder that was milled for different periods of time and sintered at a temperature of 1450 °C. The difference between the prepared samples was studied using several experimental measurement techniques, including X-ray diffractio...
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Elsevier
2023-10-01
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Series: | Arabian Journal of Chemistry |
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Online Access: | http://www.sciencedirect.com/science/article/pii/S1878535223005749 |
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author | Mamoun Fellah Naouel Hezil Dikra Bouras Alex Montagne Aleksei Obrosov Wasim Jamshed Rabha W. Ibrahim Amjad Iqbal Sayed M El Din Hamiden Abd El-Wahed Khalifa |
author_facet | Mamoun Fellah Naouel Hezil Dikra Bouras Alex Montagne Aleksei Obrosov Wasim Jamshed Rabha W. Ibrahim Amjad Iqbal Sayed M El Din Hamiden Abd El-Wahed Khalifa |
author_sort | Mamoun Fellah |
collection | DOAJ |
description | In this work was prepared α-Al2O3 alloys from laboratory aluminum oxide powder that was milled for different periods of time and sintered at a temperature of 1450 °C. The difference between the prepared samples was studied using several experimental measurement techniques, including X-ray diffraction, scanning electron microscopy and measurement of physical and mechanical properties. Moreover, the effect of milling time on the formation and sintering of alpha-alumina, by milling the mixture at different times using high energy crushing technique was studied. An influence of milling time on density, open spaces and microstructure of the samples was analyzed. The obtained results showed that longer milling duration led to alloys with higher hardness (H) and modulus of elasticity (E). This improvement is due to lower porosity and corresponding higher density at high temperatures. A noticeable decrease in the size of the particles with the increase of the milling time led to an increase in the lattice parameter accompanied by a decrease in defects and ionic voids. The percentage of pores reached 0.04 % within 24 h of grinding after it was approximately 0.20 %, while the density reached 96 % after the same highest grinding time. Tests showed that the value of friction coefficient decreases, while it increases with the increase in the applied pressure force and this was confirmed by SEM images of the samples. the main factor to reduce friction is the increase in grinding time, regardless of the value of the applied load. The results showed that the Al2O3 alloy applied to it with a load of 2 N and milled for 24 h had a minimum value of 1.94 µm3 wear volumes and a wear rate of 1.33 (µm3∙N−1∙µm−1). The sample milled for 24 h showed the best result, characterized by the lowest wear size, specific wear rate and the highest hardness with extraordinary density of 96 %, which is important in the field of biomaterials applications. |
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language | English |
last_indexed | 2024-03-12T02:06:22Z |
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spelling | doaj.art-9c812688571b478ab6ee99781f18a0552023-09-07T04:43:26ZengElsevierArabian Journal of Chemistry1878-53522023-10-011610105112Investigating the effect of milling time on structural, mechanical and tribological properties of a nanostructured hiped alpha alumina for biomaterial applicationsMamoun Fellah0Naouel Hezil1Dikra Bouras2Alex Montagne3Aleksei Obrosov4Wasim Jamshed5Rabha W. Ibrahim6Amjad Iqbal7Sayed M El Din8Hamiden Abd El-Wahed Khalifa9Mechanical Engineering Department, ABBES Laghrour-University, Khenchela, P.O 1252 40004, Algeria; Tribology and Materials Group, Laboratory of Foundry, Badji Mokhtar University, Annaba, B. O, 12 CP 23000. AlgeriaMater Sciences Department, ABBES Laghrour – University, Khenchela P.O 1252, 40004, AlgeriaLaboratoryof Active Components and Materials, Larbi Ben M′Hidi University, Oum El Bouaghi 04000, AlgeriaMechanical Engineering Department, King Fahd University of Petroleum and Minerals. Box 1180, Dhahran 31261, Saudi ArabiaDepartment of Physical Metallurgy and Materials Technology, Brandenburg Technical University, Konrad-Wachsmann Allee 17, 03046 Cottbus, GermanyDepartment of Mathematics, Capital University of Science and Technology (CUST), Islamabad 44000, Pakistan; Corresponding author.Department of Computer Science and Mathematics, Lebanese American University, 13-5053 Beirut, Lebanon; Near East University, Mathematics Research Center, Department of Mathematics, Near East Boulevard, PC:99138, Nicosia, /Mersin 10, Turkey; Information and Communication Technology Research Group, Scientific Research Center, Al-Ayen University, Thi-Qar, IraqDepartment of Materials Technologies, Faculty of Materials Engineering, Silesian University of Technology, 44-100 Gliwice, Poland; CEMMPRE—Centre for Mechanical Engineering Materials and Processes, Department of Mechanical Engineering, University of Coimbra, Rua Luı’s Reis Santos, 3030-788 Coimbra, PortugalCenter of Research, Faculty of Engineering, Future University in Egypt New Cairo 11835, EgyptDepartment of Mathematics, College of Science and Arts, Qassim University, Al-Badaya 51951, Saudi Arabia; Department of Operations and Management Reseatch, Faculty of Graduate Studies for Statistical Research, Cairo University, Giza 12613, EgyptIn this work was prepared α-Al2O3 alloys from laboratory aluminum oxide powder that was milled for different periods of time and sintered at a temperature of 1450 °C. The difference between the prepared samples was studied using several experimental measurement techniques, including X-ray diffraction, scanning electron microscopy and measurement of physical and mechanical properties. Moreover, the effect of milling time on the formation and sintering of alpha-alumina, by milling the mixture at different times using high energy crushing technique was studied. An influence of milling time on density, open spaces and microstructure of the samples was analyzed. The obtained results showed that longer milling duration led to alloys with higher hardness (H) and modulus of elasticity (E). This improvement is due to lower porosity and corresponding higher density at high temperatures. A noticeable decrease in the size of the particles with the increase of the milling time led to an increase in the lattice parameter accompanied by a decrease in defects and ionic voids. The percentage of pores reached 0.04 % within 24 h of grinding after it was approximately 0.20 %, while the density reached 96 % after the same highest grinding time. Tests showed that the value of friction coefficient decreases, while it increases with the increase in the applied pressure force and this was confirmed by SEM images of the samples. the main factor to reduce friction is the increase in grinding time, regardless of the value of the applied load. The results showed that the Al2O3 alloy applied to it with a load of 2 N and milled for 24 h had a minimum value of 1.94 µm3 wear volumes and a wear rate of 1.33 (µm3∙N−1∙µm−1). The sample milled for 24 h showed the best result, characterized by the lowest wear size, specific wear rate and the highest hardness with extraordinary density of 96 %, which is important in the field of biomaterials applications.http://www.sciencedirect.com/science/article/pii/S1878535223005749α-Al2O3Milling timeNanomaterialsParticle sizeHardnessBiomaterials |
spellingShingle | Mamoun Fellah Naouel Hezil Dikra Bouras Alex Montagne Aleksei Obrosov Wasim Jamshed Rabha W. Ibrahim Amjad Iqbal Sayed M El Din Hamiden Abd El-Wahed Khalifa Investigating the effect of milling time on structural, mechanical and tribological properties of a nanostructured hiped alpha alumina for biomaterial applications Arabian Journal of Chemistry α-Al2O3 Milling time Nanomaterials Particle size Hardness Biomaterials |
title | Investigating the effect of milling time on structural, mechanical and tribological properties of a nanostructured hiped alpha alumina for biomaterial applications |
title_full | Investigating the effect of milling time on structural, mechanical and tribological properties of a nanostructured hiped alpha alumina for biomaterial applications |
title_fullStr | Investigating the effect of milling time on structural, mechanical and tribological properties of a nanostructured hiped alpha alumina for biomaterial applications |
title_full_unstemmed | Investigating the effect of milling time on structural, mechanical and tribological properties of a nanostructured hiped alpha alumina for biomaterial applications |
title_short | Investigating the effect of milling time on structural, mechanical and tribological properties of a nanostructured hiped alpha alumina for biomaterial applications |
title_sort | investigating the effect of milling time on structural mechanical and tribological properties of a nanostructured hiped alpha alumina for biomaterial applications |
topic | α-Al2O3 Milling time Nanomaterials Particle size Hardness Biomaterials |
url | http://www.sciencedirect.com/science/article/pii/S1878535223005749 |
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