Identification by GC-MS Analysis of Organics in Manufactured Articles through a D-Optimal Design
Many manufactured articles are made of composite materials often bonded by a phenolic resin. Through a D-optimal design, we optimized a method to characterize phenolic resins after the extraction process by GC-MS analysis. The study was conducted on three different phenolic resins and four manufactu...
| Main Authors: | , , , |
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| Format: | Article |
| Language: | English |
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MDPI AG
2022-07-01
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| Series: | Applied Sciences |
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| Online Access: | https://www.mdpi.com/2076-3417/12/14/7320 |
| _version_ | 1797407517618208768 |
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| author | Monica Romagnoli Valeria Polliotto Eugenio Alladio Marco Pazzi |
| author_facet | Monica Romagnoli Valeria Polliotto Eugenio Alladio Marco Pazzi |
| author_sort | Monica Romagnoli |
| collection | DOAJ |
| description | Many manufactured articles are made of composite materials often bonded by a phenolic resin. Through a D-optimal design, we optimized a method to characterize phenolic resins after the extraction process by GC-MS analysis. The study was conducted on three different phenolic resins and four manufactured articles with the same inorganic composition and different analyzed binders. Moreover, three cardanol resins that differ in their production systems were analyzed to see if there were differences between them. Through Soxhlet extraction with dichloromethane or acetone, it is possible to differentiate the raw materials through characteristic compounds and to identify them in the manufactured articles. |
| first_indexed | 2024-03-09T03:42:38Z |
| format | Article |
| id | doaj.art-9cbfe40ccda0447382bf193e25e13603 |
| institution | Directory Open Access Journal |
| issn | 2076-3417 |
| language | English |
| last_indexed | 2024-03-09T03:42:38Z |
| publishDate | 2022-07-01 |
| publisher | MDPI AG |
| record_format | Article |
| series | Applied Sciences |
| spelling | doaj.art-9cbfe40ccda0447382bf193e25e136032023-12-03T14:37:57ZengMDPI AGApplied Sciences2076-34172022-07-011214732010.3390/app12147320Identification by GC-MS Analysis of Organics in Manufactured Articles through a D-Optimal DesignMonica Romagnoli0Valeria Polliotto1Eugenio Alladio2Marco Pazzi3Department of Chemical, Pharmaceutical and Agricultural Science, University of Ferrara, Via L. Borsari 46, 44121 Ferrara, ItalyITT Italia s.r.l., Via S. Martino 87, 12032 Barge, ItalyDepartment of Chemistry, University of Turin, Via P. Giuria 7, 10125 Turin, ItalyDepartment of Chemistry, University of Turin, Via P. Giuria 7, 10125 Turin, ItalyMany manufactured articles are made of composite materials often bonded by a phenolic resin. Through a D-optimal design, we optimized a method to characterize phenolic resins after the extraction process by GC-MS analysis. The study was conducted on three different phenolic resins and four manufactured articles with the same inorganic composition and different analyzed binders. Moreover, three cardanol resins that differ in their production systems were analyzed to see if there were differences between them. Through Soxhlet extraction with dichloromethane or acetone, it is possible to differentiate the raw materials through characteristic compounds and to identify them in the manufactured articles.https://www.mdpi.com/2076-3417/12/14/7320phenolic resincardanol resincharacterizationGC-MSD-optimal design |
| spellingShingle | Monica Romagnoli Valeria Polliotto Eugenio Alladio Marco Pazzi Identification by GC-MS Analysis of Organics in Manufactured Articles through a D-Optimal Design Applied Sciences phenolic resin cardanol resin characterization GC-MS D-optimal design |
| title | Identification by GC-MS Analysis of Organics in Manufactured Articles through a D-Optimal Design |
| title_full | Identification by GC-MS Analysis of Organics in Manufactured Articles through a D-Optimal Design |
| title_fullStr | Identification by GC-MS Analysis of Organics in Manufactured Articles through a D-Optimal Design |
| title_full_unstemmed | Identification by GC-MS Analysis of Organics in Manufactured Articles through a D-Optimal Design |
| title_short | Identification by GC-MS Analysis of Organics in Manufactured Articles through a D-Optimal Design |
| title_sort | identification by gc ms analysis of organics in manufactured articles through a d optimal design |
| topic | phenolic resin cardanol resin characterization GC-MS D-optimal design |
| url | https://www.mdpi.com/2076-3417/12/14/7320 |
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