Biodiesel production from transesterified yellow grease by ZSM-5 zeolite-supported BaO catalyst: process optimization by Taguchi’s experimental design approach
Abstract Methanolysis of yellow grease (YG) was performed to synthesize its corresponding methyl ester (YGME) using BaO loaded on ZSM-5 (BaO/ZSM-5) as a heterogeneous base catalyst that was prepared via metallic solution hydrolysis method and characterized using N2 adsorption–desorption (BET), surfa...
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| Format: | Article |
| Language: | English |
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SpringerOpen
2023-11-01
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| Series: | Materials for Renewable and Sustainable Energy |
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| Online Access: | https://doi.org/10.1007/s40243-023-00240-9 |
| _version_ | 1827581448849195008 |
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| author | Adeyinka Sikiru Yusuff Moses Oluwafemi Onibonoje |
| author_facet | Adeyinka Sikiru Yusuff Moses Oluwafemi Onibonoje |
| author_sort | Adeyinka Sikiru Yusuff |
| collection | DOAJ |
| description | Abstract Methanolysis of yellow grease (YG) was performed to synthesize its corresponding methyl ester (YGME) using BaO loaded on ZSM-5 (BaO/ZSM-5) as a heterogeneous base catalyst that was prepared via metallic solution hydrolysis method and characterized using N2 adsorption–desorption (BET), surface basicity, XRD, TGA/DTA, SEM, FTIR and Raman techniques.### The Taguchi design approach was utilized to optimize the transesterification process factors, and among the parameters studied, calcination temperature was found to have a significant influence on YGME yield. At 70 ℃ for 3 h, a YGME yield of 95.9 $$\pm 0.94$$ ± 0.94 % was obtained using a methanol/YG molar ratio of 15:1 and 1 g (2 wt.% of YG used) of BaO/ZSM-5 sample calcined at 700 ℃. The BaO/ZSM-5 catalyst was reused six times with only a 15% decrease in activity. |
| first_indexed | 2024-03-08T22:36:36Z |
| format | Article |
| id | doaj.art-9d5a0ecfa6ed45728c782e4603c7dfa2 |
| institution | Directory Open Access Journal |
| issn | 2194-1459 2194-1467 |
| language | English |
| last_indexed | 2024-03-08T22:36:36Z |
| publishDate | 2023-11-01 |
| publisher | SpringerOpen |
| record_format | Article |
| series | Materials for Renewable and Sustainable Energy |
| spelling | doaj.art-9d5a0ecfa6ed45728c782e4603c7dfa22023-12-17T12:24:58ZengSpringerOpenMaterials for Renewable and Sustainable Energy2194-14592194-14672023-11-0112319920810.1007/s40243-023-00240-9Biodiesel production from transesterified yellow grease by ZSM-5 zeolite-supported BaO catalyst: process optimization by Taguchi’s experimental design approachAdeyinka Sikiru Yusuff0Moses Oluwafemi Onibonoje1Department of Chemical and Petroleum Engineering, College of Engineering, Afe Babalola UniversityDepartment of Computer and Electrical Engineering, College of Engineering, Afe Babalola UniversityAbstract Methanolysis of yellow grease (YG) was performed to synthesize its corresponding methyl ester (YGME) using BaO loaded on ZSM-5 (BaO/ZSM-5) as a heterogeneous base catalyst that was prepared via metallic solution hydrolysis method and characterized using N2 adsorption–desorption (BET), surface basicity, XRD, TGA/DTA, SEM, FTIR and Raman techniques.### The Taguchi design approach was utilized to optimize the transesterification process factors, and among the parameters studied, calcination temperature was found to have a significant influence on YGME yield. At 70 ℃ for 3 h, a YGME yield of 95.9 $$\pm 0.94$$ ± 0.94 % was obtained using a methanol/YG molar ratio of 15:1 and 1 g (2 wt.% of YG used) of BaO/ZSM-5 sample calcined at 700 ℃. The BaO/ZSM-5 catalyst was reused six times with only a 15% decrease in activity.https://doi.org/10.1007/s40243-023-00240-9BaOZeoliteBiodieselTransesterificationTaguchi optimization |
| spellingShingle | Adeyinka Sikiru Yusuff Moses Oluwafemi Onibonoje Biodiesel production from transesterified yellow grease by ZSM-5 zeolite-supported BaO catalyst: process optimization by Taguchi’s experimental design approach Materials for Renewable and Sustainable Energy BaO Zeolite Biodiesel Transesterification Taguchi optimization |
| title | Biodiesel production from transesterified yellow grease by ZSM-5 zeolite-supported BaO catalyst: process optimization by Taguchi’s experimental design approach |
| title_full | Biodiesel production from transesterified yellow grease by ZSM-5 zeolite-supported BaO catalyst: process optimization by Taguchi’s experimental design approach |
| title_fullStr | Biodiesel production from transesterified yellow grease by ZSM-5 zeolite-supported BaO catalyst: process optimization by Taguchi’s experimental design approach |
| title_full_unstemmed | Biodiesel production from transesterified yellow grease by ZSM-5 zeolite-supported BaO catalyst: process optimization by Taguchi’s experimental design approach |
| title_short | Biodiesel production from transesterified yellow grease by ZSM-5 zeolite-supported BaO catalyst: process optimization by Taguchi’s experimental design approach |
| title_sort | biodiesel production from transesterified yellow grease by zsm 5 zeolite supported bao catalyst process optimization by taguchi s experimental design approach |
| topic | BaO Zeolite Biodiesel Transesterification Taguchi optimization |
| url | https://doi.org/10.1007/s40243-023-00240-9 |
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