Spark Plasma Sintering and Characterization of Al-TiB<sub>2</sub> Composites

In this study, Al-TiB<sub>2</sub> compacts fabricated by spark plasma sintering methods at different temperatures were characterized for densification, microstructural development, and mechanical properties. Sintering parameters used were temperatures of 500 °C and 550 °C under the press...

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Main Authors: A. Raja Annamalai, Muthe Srikanth, A. Muthuchamy, Shashank Acharya, Anup Khisti, Dinesh K. Agrawal, Chun-Ping Jen
Format: Article
Language:English
Published: MDPI AG 2020-08-01
Series:Metals
Subjects:
Online Access:https://www.mdpi.com/2075-4701/10/9/1110
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author A. Raja Annamalai
Muthe Srikanth
A. Muthuchamy
Shashank Acharya
Anup Khisti
Dinesh K. Agrawal
Chun-Ping Jen
author_facet A. Raja Annamalai
Muthe Srikanth
A. Muthuchamy
Shashank Acharya
Anup Khisti
Dinesh K. Agrawal
Chun-Ping Jen
author_sort A. Raja Annamalai
collection DOAJ
description In this study, Al-TiB<sub>2</sub> compacts fabricated by spark plasma sintering methods at different temperatures were characterized for densification, microstructural development, and mechanical properties. Sintering parameters used were temperatures of 500 °C and 550 °C under the pressure of 30 MPa. A very dense microstructure with uniform phase distribution and porosity was produced in the sample sintered at 550 °C with 2.5 wt% TiB<sub>2</sub>. The same sample exhibited excellent hardness value, and a high-tensile strength attributed to full metallurgical bonding, presence of sub-micron sized grains, and their uniform distribution. These results show that the TiB<sub>2</sub> addition enhanced the composite’s hardness, sintered density, and tensile strength. In all the sintered samples, the fractographs revealed a mixed-mode fracture (ductile and brittle).
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spelling doaj.art-9f1420e6f7934966ba2444a998603e4e2023-11-20T10:35:33ZengMDPI AGMetals2075-47012020-08-01109111010.3390/met10091110Spark Plasma Sintering and Characterization of Al-TiB<sub>2</sub> CompositesA. Raja Annamalai0Muthe Srikanth1A. Muthuchamy2Shashank Acharya3Anup Khisti4Dinesh K. Agrawal5Chun-Ping Jen6Centre for Innovative Manufacturing Research, VIT, Vellore 632014, IndiaSchool of Mechanical Engineering, VIT, Vellore 632014, IndiaDepartment of Metallurgical and Materials Engineering, NIT Tiruchirappalli, Tiruchirappalli 620015, IndiaSchool of Mechanical Engineering, VIT, Vellore 632014, IndiaSchool of Mechanical Engineering, VIT, Vellore 632014, IndiaMaterial Research Institute, Pennsylvania State University, State College, PA 16802, USADepartment of Mechanical Engineering, National Chung Cheng University, Chia-Yi 621, TaiwanIn this study, Al-TiB<sub>2</sub> compacts fabricated by spark plasma sintering methods at different temperatures were characterized for densification, microstructural development, and mechanical properties. Sintering parameters used were temperatures of 500 °C and 550 °C under the pressure of 30 MPa. A very dense microstructure with uniform phase distribution and porosity was produced in the sample sintered at 550 °C with 2.5 wt% TiB<sub>2</sub>. The same sample exhibited excellent hardness value, and a high-tensile strength attributed to full metallurgical bonding, presence of sub-micron sized grains, and their uniform distribution. These results show that the TiB<sub>2</sub> addition enhanced the composite’s hardness, sintered density, and tensile strength. In all the sintered samples, the fractographs revealed a mixed-mode fracture (ductile and brittle).https://www.mdpi.com/2075-4701/10/9/1110aluminum alloymetal matrix composites (MMCs)Al-6061TiB<sub>2</sub>spark plasma sinteringcharacterizationmicrostructure
spellingShingle A. Raja Annamalai
Muthe Srikanth
A. Muthuchamy
Shashank Acharya
Anup Khisti
Dinesh K. Agrawal
Chun-Ping Jen
Spark Plasma Sintering and Characterization of Al-TiB<sub>2</sub> Composites
Metals
aluminum alloy
metal matrix composites (MMCs)
Al-6061TiB<sub>2</sub>
spark plasma sintering
characterization
microstructure
title Spark Plasma Sintering and Characterization of Al-TiB<sub>2</sub> Composites
title_full Spark Plasma Sintering and Characterization of Al-TiB<sub>2</sub> Composites
title_fullStr Spark Plasma Sintering and Characterization of Al-TiB<sub>2</sub> Composites
title_full_unstemmed Spark Plasma Sintering and Characterization of Al-TiB<sub>2</sub> Composites
title_short Spark Plasma Sintering and Characterization of Al-TiB<sub>2</sub> Composites
title_sort spark plasma sintering and characterization of al tib sub 2 sub composites
topic aluminum alloy
metal matrix composites (MMCs)
Al-6061TiB<sub>2</sub>
spark plasma sintering
characterization
microstructure
url https://www.mdpi.com/2075-4701/10/9/1110
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